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1. 发明授权

US4808719A 1H-imidazo[2,3-a]indol-2-ones as color-forming agents 失效
标题翻译： 1H-咪唑并[2,3-a]吲哚-2-酮作为着色剂
公开(公告)号：US4808719A
公开(公告)日：1989-02-28
申请号：US60189
申请日：1987-06-09
申请人： Hubertus Psaar , Roderich Raue
发明人： Hubertus Psaar , Roderich Raue
IPC分类号： B41M5/136 , B41M5/323 , C07D487/04 , C09B23/10 , C09B23/14
CPC分类号： C09B23/105 , C09B23/145
摘要： Compounds of the general formula ##STR1## wherein R represents hydrogen or alkyl andA represents a radical of the formula ##STR2## wherein the rings D can carry up to 4 alkyl radicals,R.sup.1 and R.sup.2 independently of one another represent alkyl, alkenyl, cycloalkyl, aryl or aralkyl andR.sup.3 represents hydrogen, alkyl or aryl,and the said cyclic and acyclic radicals and the rings B and C may carry nonionic substituents, are used as color-forming agents.
摘要翻译：通式（Ⅰ）的化合物，其中R表示氢或烷基，A表示下式的基团：其中环D可携带至 4个烷基，R 1和R 2彼此独立地表示烷基，烯基，环烷基，芳基或芳烷基，R 3表示氢，烷基或芳基，所述环状和非环状基团和环B和C可以带有非离子取代基作为成色剂。

2. 发明授权

US4849306A Dry toners containing methinefanal pigments 失效
标题翻译：含有次甲醛颜料的干性调色剂
公开(公告)号：US4849306A
公开(公告)日：1989-07-18
申请号：US158520
申请日：1988-02-22
申请人： Roderich Raue , Hubertus Psaar , Horst Berneth
发明人： Roderich Raue , Hubertus Psaar , Horst Berneth
IPC分类号： G03G9/097 , C09B23/00 , C09B55/00 , G03G9/09
CPC分类号： G03G9/0916 , G03G9/0922
摘要： Dry toners for developing latent electrostatic images in electrostatic recording and printing methods contain, as charge-control substance, a pigment of the formulaF.sup.+ A.sup.- (I)in whichF represent a cationic radical of a methine dyestuff andA.sup.- represents an anion of a heteropolyacid based on tungsten and/or molybdenum with phosphorus, silicon, vanadium, cobalt, aluminum, manganese, chromium and/or nickel or a copper(I) hexacyanoferrate anion.
摘要翻译：用于在静电记录和印刷方法中显影静电潜像的干性调色剂含有作为电荷控制物质的式F + A-（I）的颜料，其中F表示次甲基染料的阳离子基团，A-表示阴离子基于钨和/或钼与磷，硅，钒，钴，铝，锰，铬和/或镍或铜（I）六氰基铁酸盐阴离子的杂多酸。

3. 发明授权

US4145537A Cationic dyestuffs 失效
标题翻译：阳离子染料
公开(公告)号：US4145537A
公开(公告)日：1979-03-20
申请号：US514999
申请日：1974-10-15
申请人： Hubertus Psaar , Roderich Raue
发明人： Hubertus Psaar , Roderich Raue
IPC分类号： C09B23/00 , C09B23/01 , C09B23/10 , D06P1/42 , D06P3/02 , C07D417/06
CPC分类号： D06P1/42 , C09B23/005 , C09B23/0058 , C09B23/105 , D06P3/022
摘要： Dyestuffs of the formula ##STR1## IN WHICH R denotes hydrogen, alkyl, alkenyl, cycloalkyl, aralkyl, aryl, alkoxy, aralkoxy, aryloxy, alkylamino, aralkylamino, arylamino, acylamino, carboxylic acid ester, carbonamido, acyl, halogen or nitrile, R.sub.1 denotes hydrogen, alkyl or aralkyl, R.sub.2 denotes hydrogen, alkyl, alkenyl, carbonamide or nitrile, R.sub.3 denotes alkyl, alkenyl or aralkyl, R.sub.4 denotes hydrogen, alkyl, alkenyl, aralkyl, alkoxy or aralkoxy, alkylamino, aralkylamino, acylamino, carbonamido, nitrile, nitro or halogen, R.sub.5 and R.sub.6 denote hydrogen, alkyl, aralkyl or a cycloaliphatic 5-membered or 6-membered ring, or R.sub.6 together with R.sub.1 forms a hydroaromatic 6-membered ring and An.sup.(-) represents an anion, and Processes for their preparation and their use for dyeing and printing natural and synthetic materials.
摘要翻译：式中，R表示氢，烷基，烯基，环烷基，芳烷基，芳基，烷氧基，芳烷氧基，芳氧基，烷基氨基，芳烷基氨基，芳基氨基，酰氨基，羧酸酯，碳酰氨基，酰基，卤素或腈，R1 表示氢，烷基或芳烷基，R2表示氢，烷基，烯基，碳酰胺或腈，R3表示烷基，烯基或芳烷基，R4表示氢，烷基，烯基，芳烷基，烷氧基或芳烷氧基，烷基氨基，芳烷基氨基，酰氨基，，硝基或卤素，R 5和R 6表示氢，烷基，芳烷基或脂环族5元或6元环，或者R 6与R 1一起形成水合芳族六元环，并且An（ - ）表示阴离子，而PROCESSES FOR 他们的制备及其用于染色和印刷天然和合成材料的使用。

4. 发明授权

US4869989A Dry toners containing fanal pigments based on cationic dyes 失效
标题翻译：含有基于阳离子染料的粉末颜料的干性调色剂
公开(公告)号：US4869989A
公开(公告)日：1989-09-26
申请号：US180418
申请日：1988-04-12
申请人： Roderich Raue , Hubertus Psaar
发明人： Roderich Raue , Hubertus Psaar
IPC分类号： C09B67/20 , C09B69/06 , G03G9/09
CPC分类号： C09B69/06 , G03G9/0914
摘要： A dry toner for developing latent electrostatic images in electrostatic recording and printing methods contains, as charge-control substance, a pigment of the formula ##STR1## in which A.sup.- represents an anion of a heteropolyacid based on tungsten and/or molybdenum with phosphorus, vanadium, cobalt, aluminium, manganese, chromium and/or nickel or a copper(I) hexacyanoferrate anion,R.sup.1 and R.sup.3, independently of one another, represent hydrogen, alkyl or aralkyl,R.sup.2 and R.sup.4 independently of one another, represent hydrogen, alkyl, aralkyl or aryl, orR.sup.1, R.sup.2, R.sup.3 and R.sup.4, independently of one another, through linking to the o-position of the benzene ring, represent members of a five- or six-membered ring, orR.sup.1 and R.sup.2 or R.sup.3 and R.sup.4 together represent members of a five- or six-membered ring,B represents oxygen or N-R,R represents hydrogen, alkyl or aryl andD represents CH or C-CN,in which the two benzene rings may be fused to a further benzene ring and then hydrogen can also replace NR.sup.3 R.sup.4 and D can also denote N, and in which the cyclic and acyclic radicals and the benzene rings may be substituted by nonionic radicals which are conventional in dyestuffs chemistry.
摘要翻译：用于在静电记录和印刷方法中显影静电潜像的干燥调色剂包含作为电荷控制物质的式I的颜料，其中A-代表基于钨和/或钼与磷的杂多酸的阴离子与磷，钒，钴，铝，锰，铬和/或镍或六氰基铁酸铜（I），R1和R3彼此独立地表示氢，烷基或芳烷基，R2和R4 + L彼此独立地表示，代表氢，烷基，芳烷基或芳基，或R 1，R 2，R 3和R 4彼此独立地通过连接到苯环的邻位，表示五元或六元环的成员，或者R1和 R2或R3和R4一起表示五元或六元环的成员，B表示氧或NR，R表示氢，烷基或芳基，D表示CH或C-CN，其中两个苯环可以稠合至另外苯环然后氢也可以代替NR3R4 nd D也可以表示N，其中环状和非环状基团和苯环可以被染料化学中常规的非离子基取代。

5. 发明授权

US4847177A Fanal pigments of closed-ring dry toners containing indamine-and diphenylmethane dyestuffs 失效
标题翻译：含有吲哚胺和二苯基甲烷染料的封闭式干性调色剂的粉末颜料
公开(公告)号：US4847177A
公开(公告)日：1989-07-11
申请号：US180402
申请日：1988-04-12
申请人： Roderich Raue , Hubertus Psaar
发明人： Roderich Raue , Hubertus Psaar
IPC分类号： C09B67/20 , C09B69/06 , G03G9/09
CPC分类号： G03G9/0914 , C09B69/06
摘要： A dry toner for developing latent electrostatic images in electrostatic copying and printing processes contains, as charge-control substance, a pigment of the formula ##STR1## in which A.sup.- represents a silicomolybdate anion,R.sup.1 and R.sup.3 represent, independently of each other, hydrogen, alkyl or aralkyl,R.sup.2 and R.sup.4 represent, independently of each other, hydrogen, alkyl, aralkyl or aryl, orR.sup.1, R.sup.2, R.sup.3 and R.sup.4 represent, independently of each other, members of a five- or six-membered ring produced by linkage with the o-position of the benzene ring orR.sup.1 and R.sup.2 or R.sup.3 and R.sup.4 jointly represent members of a five- or six-membered ring,B represents oxygen, sulphur or N--R,R represents hydrogen, alkyl or aryl andD represents CH, C--CN or N,in which the two benzene rings may be fused with a further benzene ring and then NR.sup.3 R.sup.4 may also be replaced by hydrogen, and in which the cyclic and acyclic radicals and the benzene rings may be substituted by nonionic radicals usual in dyestuff chemistry.
摘要翻译：在静电复印和印刷方法中用于显影静电潜像的干燥调色剂包含作为电荷控制物质的式I的颜料，其中A-表示硅钼酸盐阴离子，R 1和R 3彼此独立地表示，氢，烷基或芳烷基，R 2和R 4彼此独立地表示氢，烷基，芳烷基或芳基，或者R 1，R 2，R 3和R 4彼此独立地表示五或六元环的成员通过与苯环的邻位连接或R 1和R 2或R 3和R 4共同表示五元或六元环的成员，B表示氧，硫或NR，R表示氢，烷基或芳基，D表示 CH，C-CN或N，其中两个苯环可以与另外的苯环稠合，然后NR 3 R 4也可以被氢代替，并且其中环状和非环状基团和苯环可以被非离子基团取代通常在染料化学中。

6. 发明授权

US4211436A Pressure-sensitive recording material 失效
标题翻译：压敏记录材料
公开(公告)号：US4211436A
公开(公告)日：1980-07-08
申请号：US958609
申请日：1978-11-08
申请人： Hans-Peter Kuhlthau , Hubertus Psaar , Roderich Raue
发明人： Hans-Peter Kuhlthau , Hubertus Psaar , Roderich Raue
IPC分类号： B41M5/136 , B41M5/323 , C09B11/00 , C09B11/04 , C09B11/26 , B41M5/16 , B41M5/22
CPC分类号： C09B11/26 , B41M5/136 , B41M5/323 , C09B11/04 , B41M5/1366 , Y10S428/914
摘要： A pressure-sensitive and heat-sensitive recording material contains color-forming agents of the formula ##STR1## wherein R.sub.1 denotes hydrogen or a non-ionic radical which is free from amino groups,R.sub.2 denotes hydroxyl, alkylamino, dialkylamino, acylamino, aralkylamino, arylamino, a saturated heterocyclic radical, alkoxy, alkenyloxy, aralkoxy, cycloalkoxy, aryloxy, acyloxy or a direct bond to R.sub.4,R.sub.3 denotes hydroxyl, alkoxy, aralkoxy, alkenyloxy, cycloalkoxy, aryloxy, alkylthio, arylthio or a radical of the formula ##STR2## wherein R.sub.5 and R.sub.6 independently of one another denote hydrogen, alkyl, aralkyl, cyloalkyl or aryl or, together with the nitrogen atom, form a ring, or R.sub.5 forms a ring with the ring B in the o-position relative to the nitrogen atom, andR.sub.4 denotes an aryl radical which is free from amino groups or a heterocyclic radical.
摘要翻译：压敏和热敏记录材料包含下式的成色剂：其中R1表示氢或不含氨基的非离子基，R2表示羟基，烷基氨基，二烷基氨基，酰氨基，芳烷基氨基，芳基氨基，饱和杂环基，烷氧基，烯氧基，芳烷氧基，环烷氧基，芳氧基，酰氧基或与R4的直接键，R3表示羟基，烷氧基，芳烷氧基，烯氧基，环烷氧基，芳氧基，烷硫基，芳硫基或式其中R 5和R 6彼此独立地表示氢，烷基，芳烷基，环烷基或芳基，或者与氮原子一起形成环，或者R5与相对于氮原子的o位置的环B形成环 R 4表示不含氨基或杂环基的芳基。

7. 发明授权

US4897223A Tri-phenyl methyl color-forming agents 失效
标题翻译：三苯基甲基成色剂
公开(公告)号：US4897223A
公开(公告)日：1990-01-30
申请号：US162531
申请日：1988-03-01
申请人： Udo Eckstein , Hubertus Psaar , Roderich Raue
发明人： Udo Eckstein , Hubertus Psaar , Roderich Raue
IPC分类号： B41M5/00 , B41M5/132 , B41M5/136 , B41M5/20 , B41M5/30 , B41M5/323 , B41M5/34 , C07C255/58 , C07C255/59 , C07D215/14 , C07D241/42 , C07D295/135 , C09B11/00 , C09B11/04 , C09B11/12
CPC分类号： C07D295/135 , B41M5/1366 , B41M5/20 , B41M5/323 , C07C255/00 , C07D215/14 , C07D241/42
摘要： Color-forming agents of the general formula ##STR1## wherein X denotes hydroxyl, alkoxy, alkenyloxy, aralkoxy, cycloalkoxy, aryloxy, acyloxy, alkoxycarbonyloxy, alkylamino, dialkylamino, acylamino, aralkylamino or arylamino,Q denotes cyano, alkoxycarbonyl, aryloxycarbonyl, aralkoxycarbonyl, carbamoyl, N-alkylcarbamoyl, N,N-dialkylcarbamoyl, N-alkyl-N-aryl-carbamoyl, acyl, alkoxysulphonyl, aralkoxysulphonyl, sulphamoyl, N-alkylsulphamoyl, N,N-dialkylsulphamoyl, alkylsulphonyl, arylsulphonyl or aralkylsulphonyl andR denotes alkyl, alkenyl or aralkyl,further isocyclic or heterocyclic rings can be fused on to the rings A, B, C and D, and the cyclic and acyclic radicals and the rings A, B, C and D can carry further substituents, are used for the preparation of pressure-sensitive recording materials.
摘要翻译：通式为（I）的成色剂，其中X表示羟基，烷氧基，烯氧基，芳烷氧基，环烷氧基，芳氧基，酰氧基，烷氧基羰基氧基，烷基氨基，二烷基氨基，酰氨基，芳烷基氨基或芳氨基，Q表示氰基，烷氧基羰基，，芳烷氧基羰基，氨基甲酰基，N-烷基氨基甲酰基，N，N-二烷基氨基甲酰基，N-烷基-N-芳基 - 氨基甲酰基，酰基，烷氧基磺酰基，芳烷基磺酰基，氨磺酰基，N-烷基氨磺酰基，N，N-二烷基氨磺酰基，烷基磺酰基，芳基磺酰基或芳烷基磺酰基和R 表示烷基，烯基或芳烷基，进一步的环或杂环可以稠合在环A，B，C和D上，并且环和无环基和环A，B，C和D可以携带另外的取代基用于制备压敏记录材料。

8. 发明授权

US4513142A Preparation of cationic methine dyestuffs 失效
标题翻译：阳离子次甲基染料的制备
公开(公告)号：US4513142A
公开(公告)日：1985-04-23
申请号：US412644
申请日：1982-08-30
申请人： Roderich Raue , Volker Huhne , Hans-Peter Kuhlthau
发明人： Roderich Raue , Volker Huhne , Hans-Peter Kuhlthau
IPC分类号： C09B23/00 , C09B23/06 , C09B23/10 , C09B23/14
CPC分类号： C09B23/06 , C09B23/105 , C09B23/145
摘要： A method of preparation of cationic dyestuffs having the formula ##STR1## wherein A, B, R, and R.sup.1 are defined in the specification carried out in the substantial absence of solvent and removing water formed in the reaction.
摘要翻译：具有式“IMAGE”的阳离子染料的制备方法，其中A，B，R和R 1在本说明书中定义，基本上不存在溶剂并除去反应中形成的水。

9. 发明授权

US4496719A 3H-Indol-2-yl cationic hydrazone dyestuffs 失效
标题翻译： 3H-吲哚-2-基阳离子腙染料
公开(公告)号：US4496719A
公开(公告)日：1985-01-29
申请号：US466709
申请日：1983-02-15
申请人： Roderich Raue
发明人： Roderich Raue
IPC分类号： C09B26/02 , C09B26/04 , C07D209/12 , C07D403/12
CPC分类号： C09B26/04
摘要： Hydrazone dyestuffs of the formula ##STR1## in which R denotes optionally substituted alkyl,R.sup.1 denotes alkyl and the two radicals can form a closed ring,R.sup.2 denotes optionally substituted alkyl,R.sup.3 denotes alkyl, alkoxy or halogen,R.sup.4 denotes alkyl, halogen, alkoxy, phenoxy, benzyloxy, benzyl, carboxyl, alkyl carboxylate, carboxamide, sulphonamide, alkylsulphonyl, phenylsulphonyl, cyano, nitro, trifluoromethyl, acetyl or benzoyl,B denotes ##STR2## D denotes alkylene, phenylene or naphthylene, E denotes halogen, hydroxyl, alkoxy or ##STR3## Z and Z.sup.1 denote hydrogen or --Y--Z.sup.2, Y denotes alkylene,Z.sup.2 denotes hydrogen, hydroxyl, pyridinium, ##STR4## Z.sup.3, Z.sup.4 and Z.sup.5 denote hydrogen or optionally substituted alkyl,Z.sup.3 also denotes phenyl, benzyl or ##STR5## Y.sup.1 denotes alkylene and s denotes 1-8, orZ and Z.sup.1 as well as Z.sup.3 and Z.sup.4 form a closed ring,G denotes alkylene, phenylene orG denotes alkylene, phenylene or ##STR6## m and n denote 0, 1 or 2 and X.sup.(-) denotes an anion,are used in particular for dyeing paper.
摘要翻译：其中R表示任选取代的烷基，R 1表示烷基且两个基团可以形成闭环，R 2表示任选取代的烷基，R 3表示烷基，烷氧基或卤素，R 4表示烷基，，卤素，烷氧基，苯氧基，苄氧基，苄基，羧基，羧酸烷基酯，甲酰胺，磺酰胺，烷基磺酰基，苯基磺酰基，氰基，硝基，三氟甲基，乙酰基或苯甲酰基，B表示亚烷基，亚苯基或亚萘基，E表示卤素，羟基，烷氧基或Z表示氢或-Y-Z2，Y表示亚烷基，Z2表示氢，羟基，吡啶鎓，Z3，Z4和Z5表示氢或任选取代的烷基 Z3也表示苯基，苄基或Y1表示亚烷基，s表示1-8或Z和Z1以及Z3和Z4形成闭环，G表示亚烷基，亚苯基或G表示亚烷基，亚苯基或 m和n表示0,1或2，X（ - ）表示阴离子特别用于染色纸。

10. 发明授权

US4419511A Process for the preparation of trimethine dyestuffs 失效
标题翻译：三甲基染料的制备方法
公开(公告)号：US4419511A
公开(公告)日：1983-12-06
申请号：US344262
申请日：1982-01-28
申请人： Roderich Raue
发明人： Roderich Raue
IPC分类号： C09B23/00 , C09B23/06
CPC分类号： C09B23/06
摘要： To prepare trimethine dyestuffs of the general formula ##STR1## wherein R represents a C.sub.1 - to C.sub.4 -alkyl radical,R.sup.1 represents hydrogen, C.sub.1 - to C.sub.4 -alkyl, benzyl, cyclohexyl, C.sub.1 - to C.sub.4 -alkoxy, benzyloxy, phenoxy, halogen, trifluoromethyl, acetylamino, carboxylic acid C.sub.1 - to C.sub.4 -alkyl esters, carbonamide which may be substituted by C.sub.1 - to C.sub.4 -alkyl and/or phenyl, C.sub.1 - to C.sub.4 -alkylsulphonyl, phenylsulphonyl, cyano, nitro, benzoxazol-2-yl, benzimidazol-2-yl, benzthiazol-2-yl and sulphonamide which may be monosubstituted or disubstituted by C.sub.1 - to C.sub.4 -alkyl, or two radicals R.sup.1 represent a fused benzene ring,n denotes 1 to 4 andA.sup.- denotes an anionic radical, first an alkali metal salt of formic acid is reacted with a mixture of acetic acid and acetic anhydride and the product is then reacted with indoline compounds of the general formula ##STR2## in which R, R.sup.1 and n have the abovementioned meaning.
摘要翻译：为了制备通式“IMAGE”的三甲基染料，其中R表示C 1〜C 4 - 烷基，R 1表示氢，C 1至C 4 - 烷基，苄基，环己基，C 1至C 4 - 烷氧基，苄氧基，苯氧基，卤素三氟甲基，乙酰氨基，羧酸C 1至C 4烷基酯，可被C 1至C 4 - 烷基和/或苯基取代的碳酰胺，C 1至C 4 - 烷基磺酰基，苯基磺酰基，氰基，硝基，苯并恶唑-2-基苯并咪唑-2-基，苯并噻唑-2-基和磺酰胺，其可以被C 1 -C 4烷基单取代或二取代，或两个基团R 1表示稠合苯环，n表示1至4，A-表示阴离子基团首先将甲酸的碱金属盐与乙酸和乙酸酐的混合物反应，然后使产物与其中R，R 1和n具有上述含义的通式为“IMAGE”的二氢吲哚化合物反应。

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