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1. 发明授权

US6068697A Polysaccharide derivatives and hydraulic compositions 失效
标题翻译：多糖衍生物和水硬性组合物
公开(公告)号：US6068697A
公开(公告)日：2000-05-30
申请号：US101632
申请日：1998-07-14
申请人： Hotaka Yamamuro , Takeshi Ihara , Tomohito Kitsuki , Tetsuya Miyajima , Fujio Yamato , Makoto Kohama
发明人： Hotaka Yamamuro , Takeshi Ihara , Tomohito Kitsuki , Tetsuya Miyajima , Fujio Yamato , Makoto Kohama
IPC分类号： C04B24/16 , C04B24/24 , C04B24/38 , C04B28/02 , C04B28/14 , C08B11/04 , C08B11/12 , C08B11/193 , C08B13/00 , C08B31/12 , C08B37/00 , C12N1/21 , C04B26/28
CPC分类号： C04B28/02 , C04B24/166 , C04B24/243 , C04B24/38 , C08B11/193 , C08B13/00 , C04B2111/00129
摘要： A polysaccharide derivative prepared by replacing all or part of the hydroxyl hydrogen atoms of a polysaccharide or polysaccharide derivative by (A) a hydrophobic substituent having a C.sub.8 -C.sub.43 hydrocarbon chain as the partial structure and (B) an ionic hydrophilic substituent having at least one member selected from the group consisting of sulfonic, carboxyl phosphoric, and sulfate groups and salts thereof as the partial structure, wherein the average degree of replacement by the substituent (A) is 0.0001 or above but below 0.001 per constituent monosaccharide residue as determined by Zeisel's method or the diazomethane method and that by the substituent (B) is 0.01 to 2.0 per constituent monosaccharide residue as determined by colloidal titration. This polysaccharide derivative is useful as the admixture for hydraulic materials and can give stable hydraulic compositions excellent in dispersion.
摘要翻译： PCT No.PCT / JP97 / 04316 Sec。 371日期：1998年7月14日 102（e）日期1998年7月14日PCT 1997年11月26日PCT公布。公开号WO98 / 23647 日期1998年6月4日通过（A）具有C8-C43烃链作为部分结构的疏水性取代基取代多糖或多糖衍生物的全部或部分羟基氢原子制备的多糖衍生物，（B）离子性亲水性取代基具有选自磺酸基，羧基磷酸和硫酸根的至少一种作为部分结构，其中取代基（A）的平均取代度为0.0001以上且低于0.001，构成单糖通过Zeisel方法或重氮甲烷法测定的残留物和通过胶体滴定测定的通过取代基（B）的残基为0.01〜2.0，作为构成单糖残基。这种多糖衍生物可用作水硬性材料的混合物，并且可以得到稳定的水分分散性优良的组合物。

2. 发明授权

US5885955A Amides, method for preparing the amides, and detergent compositions containing the amides 失效
标题翻译：酰胺，制备酰胺的方法和含有酰胺的洗涤剂组合物
公开(公告)号：US5885955A
公开(公告)日：1999-03-23
申请号：US967918
申请日：1997-11-12
申请人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
发明人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
IPC分类号： A61K8/42 , A61Q5/02 , A61Q5/12 , A61Q19/00 , C07C233/05 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/30 , C07C305/06 , C07C309/15 , C11D1/52 , C11D3/32 , C11D1/04 , C11D1/28 , C11D1/62 , C11D1/66
CPC分类号： C11D3/32 , A61K8/42 , A61Q19/00 , A61Q19/10 , A61Q5/02 , C07C231/02 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/24 , C07C303/32 , C07C309/15 , C11D1/528 , A61Q5/12
摘要： An amide represented by the following formula (1): ##STR1## wherein R.sup.1 and R.sup.2 are C1-C24 alkyl, etc.; B is C2-C10 alkylene, etc.; A.sup.1 and A.sup.2 are C1-C6 alkylene, etc.; Y.sup.1 and Y.sup.2 are ##STR2## wherein R.sup.3, R.sup.4, and R.sup.5 are C1-C4 alkyl, etc., and X.sup.1 is halogen; or a salt of the amide and detergent compositions containing the amide or salt are mild to the skin or hair, provide a pleasant sensation to the skin or hair, and have excellent latherability and emulsion stability. These compounds are useful as components of various detergents and cosmetic compositions, emulsifiers, and conditioners.
摘要翻译：由下式（1）表示的酰胺：其中R 1和R 2是C 1 -C 24烷基等; B是C 2 -C 10亚烷基等; A1和A2是C1-C6亚烷基等; Y 1和Y 2是其中R 3，R 4和R 5是C 1 -C 4烷基等，且X 1是卤素; 或含有酰胺或盐的酰胺和洗涤剂组合物的盐对皮肤或毛发温和，对皮肤或毛发提供愉快的感觉，并且具有优异的起泡性和乳液稳定性。这些化合物可用作各种洗涤剂和化妆品组合物，乳化剂和调理剂的组分。

3. 发明授权

US5756784A Amides, method for preparing the amides, and detergent compositions containing the amides 失效
公开(公告)号：US5756784A
公开(公告)日：1998-05-26
申请号：US646767
申请日：1996-05-08
申请人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
发明人： Mitsuru Uno , Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita
IPC分类号： A61K8/42 , A61Q5/02 , A61Q5/12 , A61Q19/00 , C07C233/05 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/30 , C07C305/06 , C07C309/15 , C11D1/52 , C11D3/32
CPC分类号： C11D3/32 , A61K8/42 , A61Q19/00 , A61Q19/10 , A61Q5/02 , C07C231/02 , C07C233/36 , C07C233/47 , C07C303/22 , C07C303/24 , C07C303/32 , C07C309/15 , C11D1/528 , A61Q5/12
摘要： An amide represented by the following formula (1): ##STR1## wherein R.sup.1 and R.sup.2 are C1-C24 alkyl, etc.; B is C2-C10 alkylene, etc.; A.sup.1 and A.sup.2 are C1-C6 alkylene, etc.; Y.sup.1 and Y.sup.2 are ##STR2## wherein R.sup.3, R.sup.4, and R.sup.5 are C1-C4 alkyl, etc., and X.sup.1 is halogen; or a salt of the amide and detergent compositions containing the amide or salt are mild to the skin or hair, provide a pleasant sensation to the skin or hair, and have excellent latherability and emulsion stability. These compounds are useful as components of various detergents and cosmetic compositions, emulsifiers, and conditioners.

4. 发明授权

US07517534B2 Oil-in-water emulsions and process for producing the same 有权
标题翻译：水包油乳剂及其制备方法
公开(公告)号：US07517534B2
公开(公告)日：2009-04-14
申请号：US10471699
申请日：2002-03-12
申请人： Takahiro Nishizaka , Takeshi Ihara , Tomohito Kitsuki
发明人： Takahiro Nishizaka , Takeshi Ihara , Tomohito Kitsuki
IPC分类号： A61K8/02
CPC分类号： A61K8/731 , A61K8/062 , A61K8/85 , A61K8/86 , A61Q19/00 , B01F17/0028 , B01F17/005 , Y10S514/938
摘要： A process for the preparation of an o/w emulsion, which comprises mixing together a high molecular compound carrying at least on side chains thereof groups represented by the following formula (1): —(OX)n-E2-R (1) wherein n “X”s may be the same or different and each independently represents a linear or branched, divalent, saturated C1-6 hydrocarbon group, n stands for a number of from 5 to 300, E2 represents an ether bond or an oxycarbonyl group (—OCO— or —COO—), and R represents a linear or branched, C4-30 alkyl group which may be substituted by hydroxyl group(s), an aqueous solution of a water-soluble polyol, and a hydrophobic compound, and diluting a resulting mixture with water, and the o/w emulsion obtained by the preparation process. The emulsion according to the present invention is excellent in touch feeling to the skin and is good in stability.
摘要翻译：一种制备o / w乳液的方法，其包括将至少在其侧链上携带下列通式（1）表示的基团的高分子化合物混合在一起：<？in-line-formula description =“In-line 公式“end =”lead“？> - （OX）n-E2-R（1）<？in-line-formula description =”In-line Formulas“end =”tail“？>其中n”X“ 相同或不同，并且各自独立地表示直链或支链的二价饱和C 1-6烃基，n表示5至300的数，E2表示醚键或氧羰基（-OCO-或-COO - ），R表示可以被羟基取代的直链或支链的C 4-30烷基，水溶性多元醇的水溶液和疏水性化合物，并用水稀释得到的混合物，和通过制备方法获得的o / w乳液。本发明的乳液对皮肤的触感良好，稳定性好。

5. 发明授权

US06541614B1 Polysaccharide derivative 有权
标题翻译：多糖衍生物
公开(公告)号：US06541614B1
公开(公告)日：2003-04-01
申请号：US09926688
申请日：2001-12-03
申请人： Atsushi Nagasawa , Tomohito Kitsuki , Takeshi Ihara
发明人： Atsushi Nagasawa , Tomohito Kitsuki , Takeshi Ihara
IPC分类号： C07H1508
CPC分类号： C08B37/00 , A61K8/73 , A61Q5/02 , A61Q19/00 , A61Q19/10 , C08B11/00 , C08B11/08 , C08B11/20 , C08B31/00 , C08B31/08 , C08B31/12 , C08B31/125
摘要： Polysaccharide derivatives derived from a polysaccharide or a derivative thereof by substituting a part or all of the hydrogen atoms of the hydroxyl groups of the polysaccharide or the derivative thereof with the groups represented by the following formula (1): —E1—(OA)n—E2—R (1) wherein E1 represents a divalent saturated C1-6 hydrocarbon group which may be substituted with one or more hydroxyl groups or oxo groups, n stands for a number of from 8 to 300, n numbers of As may be the same or different and each independently represent a divalent saturated C1-6 hydrocarbon group, E2 represents an ether bond or an oxycarbonyl group, and R represents a C4-30 alkyl group which may be substituted with one or more hydroxyl groups, in which the H(s) of one or more hydroxy groups in each of said groups (1) may be further substituted with the groups (1); thickeners and emulsifiers comprising these polysaccharide derivatives; as well as aqueous compositions containing said polysaccharide derivatives. The polysaccharide derivatives of the present invention are excellent in water solubility and have such a rheological characteristic that the viscosity thereof increases at high temperatures, whereby they are very useful as a thickener exhibiting an excellent handling property at low temperatures and a sufficient thickening effect at high temperatures, as an emulsifier exhibiting an excellent emulsifying action allowing hydrophobic compounds to exist very stably in water, and also as a thickening and stabilizing agent for various toiletry products such as viscous bath preparations, massaging cosmetic preparations, shower preparations, skin care preparations, hair washing preparations, body washing preparations, garment detergents, garment finishing agents and hard surface cleaning agents.
摘要翻译：通过用下述式（1）表示的基团代替多糖或其衍生物的羟基的部分或全部的氢原子的一部分或全部来自多糖或其衍生物的多糖衍生物：其中E1表示二价饱和C1 可以被一个或多个羟基或氧代基取代的烃基，n表示数量为8至300，n数可以相同或不同，并且各自独立地表示二价饱和C 1-6烃基团，E2表示醚键或氧羰基，R表示可被一个或多个羟基取代的C4-30烷基，其中每个所述基团中的一个或多个羟基的H（s）（1）可以进一步被基团（1）取代; 包含这些多糖衍生物的增稠剂和乳化剂; 以及含有所述多糖衍生物的含水组合物。本发明的多糖衍生物具有优异的水溶性，并且具有其粘度在高温下增加的流变特性，因此它们作为显示出优异处理性能的增稠剂是非常有用的在低温下和在高温下具有充分的增稠效果，作为表现出优异的乳化作用的乳化剂，使疏水性化合物在水中非常稳定地存在，以及作为用于各种化妆品的增稠和稳定剂，例如粘稠浴剂，按摩化妆品制剂，沐浴用品，护肤品，洗发剂，洗身剂，衣物洗涤剂，服装整理剂和硬表面清洁剂。

6. 发明授权

US5891450A Polysaccharide derivative, and preparation process and use thereof 失效
标题翻译：多糖衍生物及其制备方法及用途
公开(公告)号：US5891450A
公开(公告)日：1999-04-06
申请号：US773533
申请日：1996-12-23
申请人： Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita , Hiroshi Kamitani , Kazuhiro Yamaki
发明人： Tetsuya Miyajima , Tomohito Kitsuki , Katsumi Kita , Hiroshi Kamitani , Kazuhiro Yamaki
IPC分类号： A61K8/06 , A61K8/73 , A61Q1/02 , A61Q1/06 , A61Q17/04 , A61Q19/00 , C08B11/193 , C08B13/00 , A61K7/48
CPC分类号： C08B13/00 , A61K8/06 , A61K8/73 , A61K8/731 , A61K8/732 , A61K8/737 , A61Q19/00 , C08B11/193 , A61Q1/02 , A61Q17/04 , Y10S514/844 , Y10S514/937
摘要： Disclosed herein are a polysaccharide derivative obtainable by substituting a part or the whole of hydrogen atoms of hydroxyl groups in a polysaccharide or a derivative thereof by the following substituents (A) and (B):(A) a hydrophobic group containing a C.sub.10 -C.sub.40 alkyl, alkenyl or acyl group which may be substituted by an --OH group or into which an oxycarbonyl group (--COO-- or --OCO--) may be introduced; and(B) a C.sub.1 -C.sub.5 sulfoalkyl group which may be substituted by an --OH group, or a salt thereof, wherein average degrees of substitution by the substituents (A) and (B) per monosaccharide residue are 0.001-1.0 and 0.01-2.0, respectively; a preparation process thereof; and use of the polysaccharide derivative for a thickener for cosmetic compositions.
摘要翻译：本文公开了通过以下取代基（A）和（B）将多糖或其衍生物中的羟基的一部分或全部氢原子取代得到的多糖衍生物：（A）含有C10-C40的疏水基团可以被-OH基取代的烷基，烯基或酰基，或可以引入氧羰基（-COO-或-OCO-）; 和（B）可以被-OH基取代的C1-C5磺基烷基或其盐，其中每个单糖残基的取代基（A）和（B）的平均取代度为0.001-1.0和0.011- 2.0; 其制备方法; 以及多糖衍生物用于化妆品组合物的增稠剂的用途。

7. 发明申请

US20060252946A1 Production process for glycidyl ether adduct and catalyst used for the process 审中-公开
标题翻译：用于该方法的缩水甘油醚加合物和催化剂的制备方法
公开(公告)号：US20060252946A1
公开(公告)日：2006-11-09
申请号：US11482749
申请日：2006-07-10
申请人： Atsushi Nagasawa , Mitsuru Uno , Tomohito Kitsuki
发明人： Atsushi Nagasawa , Mitsuru Uno , Tomohito Kitsuki
IPC分类号： C07D301/27 , C07H1/00
CPC分类号： C11D1/72 , B01J21/10 , B01J23/002 , B01J23/06 , B01J2523/00 , B01J2523/22 , B01J2523/31 , B01J2523/27
摘要： Provided is a catalyst for adding a glycidyl ether to an active hydrogen-containing organic compound, comprising a complex oxide of magnesium and at least one element other than magnesium selected from the group consisting of the elements in the third period and the fourth period in the periodic table. Also provided is a process for producing a glycidyl ether adduct, which comprises subjecting an active hydrogen-containing organic compound and a glycidyl ether to an addition reaction in the presence of the above-mentioned catalyst. In the addition reaction between the active hydrogen-containing organic compound and the glycidyl ether, use of the catalyst of the present invention enables inhibition of an excess addition reaction of the glycidyl ether which is a successive reaction, and a mono- or di-(alkyl, alkenyl or phenyl) ether product in which one or two glycidyl ethers are added is selectively produced by adjusting the mole ratio of the active hydrogen-containing organic compound to the glycidyl ether to a specific range. Accordingly, the mono- or di-(alkyl, alkenyl or phenyl) ether product can be obtained at a high productivity with a high purity.
摘要翻译：提供了一种用于向含活性氢的有机化合物中加入缩水甘油醚的催化剂，其包含镁和至少一种除镁以外的元素的复合氧化物，所述复合氧化物选自第三周期和第四周期中的元素组周期表。还提供了一种制备缩水甘油醚加合物的方法，其包括在上述催化剂存在下使含活性氢的有机化合物和缩水甘油醚进行加成反应。在含活性氢的有机化合物和缩水甘油醚之间的加成反应中，使用本发明的催化剂可以抑制作为连续反应的缩水甘油醚的过量加成反应，以及单 - 或二烷基，烯基或苯基）醚产物，其中加入一个或两个缩水甘油醚是通过将含活性氢的有机化合物与缩水甘油醚的摩尔比调整到特定范围来选择性地制备的。因此，可以以高纯度的高生产率获得单 - 或二 - （烷基，烯基或苯基）醚产物。

8. 发明授权

US5714457A 2-hydroxypropanediamine derivative and detergent composition containing the same 失效
标题翻译： 2-羟基丙二胺衍生物和含有它们的洗涤剂组合物
公开(公告)号：US5714457A
公开(公告)日：1998-02-03
申请号：US569128
申请日：1996-01-11
申请人： Tomohito Kitsuki , Mitsuru Uno , Katsumi Kita , Yoshiaki Fujikura , Akiko Nakano , Masaki Tosaka , Kazuyuki Yahagi , Shigeru Tamura , Kazunari Maruta
发明人： Tomohito Kitsuki , Mitsuru Uno , Katsumi Kita , Yoshiaki Fujikura , Akiko Nakano , Masaki Tosaka , Kazuyuki Yahagi , Shigeru Tamura , Kazunari Maruta
IPC分类号： A61K8/41 , A61K8/44 , A61K8/68 , A61Q5/00 , A61Q5/02 , A61Q19/00 , C07C229/12 , C07C229/16 , C07C233/18 , C07C233/20 , C07C233/36 , C07C233/38 , C07C235/08 , C07C235/10 , C07C305/06 , C07C309/13 , C07C309/14 , C07C309/17 , C11D1/02 , C11D1/10 , C11D1/28 , C11D1/92
CPC分类号： A61Q19/00 , A61K8/41 , A61K8/416 , A61K8/44 , A61K8/68 , A61Q5/00 , C07C229/12 , C07C229/16 , C07C233/18 , C07C233/20 , C07C233/36 , C07C233/38 , C07C235/08 , C07C235/10 , C07C305/06 , C07C309/14 , C07C309/17 , C11D1/10 , C11D1/28 , C11D3/0094 , A61K2800/75 , A61Q19/10 , A61Q5/02
摘要： The present invention relates to a 2-hydroxypropanediamine derivative represented by the following general formula (1): ##STR1## wherein R.sup.1 and R.sup.2 mean individually a linear or branched C.sub.6 -C.sub.36 alkyl or alkenyl group, X denotes a C.sub.1 -C.sub.6 alkylene or alkenylene group which may be substituted by at least one hydroxyl, sulfonic or carboxyl group and has 1-6 carbon atoms, y.sup.1 is a sulfonic group, a sulfuric acid residue or a carboxyl group, y.sup.2 means a hydroxyl group, a sulfuric acid residue or ##STR2## and n stands for 0 or 1, or a salt or quaternized product thereof, and a detergent composition containing such a compound. This compound is low in irritativeness to the skin and hair and excellent in foamability, and can give a pleasant feeling to the user's skin and the like.
摘要翻译： PCT No.PCT / JP94 / 01129 Sec。 371日期1996年1月11日 102（e）日期1996年1月11日PCT提交1994年7月11日PCT公布。出版物WO95 / 01955 日本1 9月19日本发明涉及由以下通式（1）表示的2-羟基丙二胺衍生物：其中R 1和R 2分别表示直链或支链C 6 -C 36烷基或链烯基，X 表示可以被至少一个羟基，磺酸或羧基取代并具有1-6个碳原子的C1-C6亚烷基或亚烯基，y1是磺酸基，硫酸残基或羧基，y2表示羟基基团，硫酸残基或，n表示0或1，或其盐或季铵化物，以及含有该化合物的洗涤剂组合物。该化合物对皮肤和头发的刺激性低，起泡性优异，并且可以给使用者的皮肤等提供愉快的感觉。

9. 发明授权

US08436165B2 Process for producing noncrystalline cellulose 有权
标题翻译：非晶纤维素的制造方法
公开(公告)号：US08436165B2
公开(公告)日：2013-05-07
申请号：US12527047
申请日：2008-02-15
申请人： Naoki Nojiri , Masahiro Umehara , Tomohito Kitsuki , Munehisa Okutsu , Keiichiro Tomioka
发明人： Naoki Nojiri , Masahiro Umehara , Tomohito Kitsuki , Munehisa Okutsu , Keiichiro Tomioka
IPC分类号： C07H1/00 , C08B1/00
CPC分类号： C08B1/00 , C08B15/08 , C08H8/00
摘要： The present invention relates to a process for producing a decrystallized cellulose having a reduced cellulose I-type crystallinity from a cellulose-containing raw material in an efficient manner with an excellent productivity. In accordance with the present invention, there is provided a process for producing a decrystallized cellulose from a raw material comprising at least 20% by weight, based on the weight of the raw material excluding water contained therein, of a cellulose having a cellulose I-type crystallinity of more than 33% as calculated from the following formula: Cellulose I-type Crystallinity (%)=[(I22.6−I18.5)/I22.6]×100 wherein I22.6 is a diffraction intensity of a lattice plane (002 plane) as measured at a diffraction angle 2θ of 22.6° in X-ray diffraction analysis; and I18.5 is a diffraction intensity of an amorphous moiety as measured at a diffraction angle 2θ of 18.5° in X-ray diffraction analysis, the process including the step of treating the cellulose-containing raw material using a media-type mill to reduce the cellulose I-type crystallinity of the cellulose to 33% or less, wherein the cellulose-containing raw material has a bulk density of from 100 to 500 kg/m3.
摘要翻译：本发明涉及一种以有效的方式从含纤维素原料生产具有降低的纤维素I型结晶度的脱结晶纤维素的方法，该方法具有优异的生产率。根据本发明，提供了一种从原料生产去结晶纤维素的方法，该方法包含至少20重量％，基于其中所含的不含水的原料的重量，具有纤维素I- 型结晶度大于33％，如下式所示：纤维素I型结晶度（％）= [（I22.6-I18.5）/ I22.6]×100其中，I22.6为衍射强度在X射线衍射分析中在衍射角2θ为22.6°时测得的晶格面（002平面）; I18.5是在X射线衍射分析中在衍射角2θ为18.5°测定的非晶部分的衍射强度，该方法包括使用介质型磨机处理含纤维素原料的步骤以减少纤维素的纤维素I型结晶度为33％以下，其中，所述含纤维素原料的体积密度为100〜500kg / m 3。

10. 发明授权

US5136112A Process for preparing 2-hydroxy-2 5, 5, 9-tetramethyldecalyl ethanol 失效
标题翻译：制备2-羟基-5,5,9-四甲基乙基醚的方法
公开(公告)号：US5136112A
公开(公告)日：1992-08-04
申请号：US736927
申请日：1991-07-29
申请人： Tomohito Kitsuki , Yoshiaki Fujikura
发明人： Tomohito Kitsuki , Yoshiaki Fujikura
IPC分类号： C07C29/149 , C07C29/147 , C07C29/94 , C07C35/23 , C07C35/36
CPC分类号： C07C35/36 , C07C29/147 , C07C2102/28
摘要： A process for preparing 2-hydroxy-2, 5, 5, 9-tetramethyldecalyl ethanol of formula (II): ##STR1## which comprises reducing 3a, 6, 6, 9a-tetramethyldecahydro-naphto[2, 1-b]furan-2(1H)-one of formula (I): ##STR2## with an alkali metal boron hydride in the presence of a hydroxyl ether compound.

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