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1. 发明授权

US4294808A Production of anticorrosive pigments containing phosphorus 失效
标题翻译：生产含磷的防锈颜料
公开(公告)号：US4294808A
公开(公告)日：1981-10-13
申请号：US76307
申请日：1979-09-17
申请人： Horst-Dieter Wasel-Nielen , Renate Adrian , Herbert Panter , Gero Heymer , Alexander Maurer , Raban von Schenck
发明人： Horst-Dieter Wasel-Nielen , Renate Adrian , Herbert Panter , Gero Heymer , Alexander Maurer , Raban von Schenck
IPC分类号： C23C22/08 , C01B25/163 , C01B25/165 , C01B25/26 , C01B25/32 , C01B25/34 , C01B25/37 , C09D5/08 , C01B25/36
CPC分类号： C09D5/084 , C01B25/163 , C01B25/165 , C01B25/265 , C01B25/325 , C01B25/34 , C01B25/37
摘要： The invention relates to a process for making phosphorus-containing anticorrosive pigments having a size of at most 20 microns by reacting one or more compounds of magnesium, calcium, strontium, barium, zinc, aluminum, iron, chromium or manganese with an oxygen acid of phosphorus or its alkali metal or ammonium salts at temperatures within the range 10.degree. to 100.degree. C. More particularly pigments consisting to an extent of at least 90% of particles with a size between 0.05 and 8 microns are produced by introducing an aqueous suspension or solution of the reactants into a dispersing means rotating at a speed of 3000 to 10,000 rpm, reacting the reactants by intimately mixing them, and separating and drying precipitated pigment.
摘要翻译：本发明涉及一种通过使一种或多种镁，钙，锶，钡，锌，铝，铁，铬或锰的化合物与氧酸的氧酸反应制备尺寸至多为20微米的含磷防腐颜料的方法磷或其碱金属或铵盐。更具体地说，通过将水性悬浮液或水溶性悬浮液引入至少90％的尺寸为0.05至8微米的颗粒的程度，将反应物溶解在以3000至10,000rpm的速度旋转的分散装置中，通过将它们紧密混合使反应物反应，并分离和干燥沉淀的颜料。

2. 发明授权

US4394358A Production of granular alkali metal diphosphates or triphosphates 失效
标题翻译：生产颗粒状碱金属二磷酸盐或三磷酸盐
公开(公告)号：US4394358A
公开(公告)日：1983-07-19
申请号：US303100
申请日：1981-09-17
申请人： Alexander Maurer , Renate Adrian , Herbert Panter , Gero Heymer , Dieter Nolker
发明人： Alexander Maurer , Renate Adrian , Herbert Panter , Gero Heymer , Dieter Nolker
IPC分类号： C01B25/41 , C01B25/42 , C11D3/06 , C01B25/30
CPC分类号： C01B25/418 , C01B25/425 , C11D3/062
摘要： The invention relates to a process for making granulated, partially or completely hydrated alkali metal diphosphates or triphosphates. To this end, the invention provides for alkali metal diphosphates or triphosphates which consist to an extent of at least 20% of particles with a size of less than 0.045 mm and are hydrated to an extent of less than 90%, based on the phosphates' theoretical content of water of hydration, to be intensively mixed and granulated in the presence of water and an ammonium polyphosphate, this latter being used in a proportion of about 0.5 to 50 weight %, based on the quantity of water used.
摘要翻译：本发明涉及制备颗粒状，部分或完全水合的碱金属二磷酸盐或三磷酸盐的方法。为此，本发明提供碱金属二磷酸盐或三磷酸盐，其碱度至少为20％，其尺寸小于0.045mm，并且基于磷酸盐的水合物水合至小于90％的程度，在水和多磷酸铵的存在下，水合的水的理论含量将被浓缩混合和造粒，后者基于所用的水量以约0.5至50重量％的比例使用。

3. 发明授权

US3943231A Process for making condensed aluminum phosphates 失效
标题翻译：制备浓缩磷酸铝的方法
公开(公告)号：US3943231A
公开(公告)日：1976-03-09
申请号：US370626
申请日：1973-06-18
申请人： Horst-Dieter Wasel-Nielen , Gero Heymer , Peter Wirtz
发明人： Horst-Dieter Wasel-Nielen , Gero Heymer , Peter Wirtz
IPC分类号： C04B28/26 , C01B25/36 , C01B25/38 , C04B22/16 , C01B15/16 , C01B25/26
CPC分类号： C01B25/38 , C04B22/16
摘要： The invention provides condensed aluminum phosphates which contain P.sub.2 O.sub.5 and Al.sub.2 O.sub.3 in a molar ratio equal to or greater than 1.5:1, are X-ray amorphous and have an apparent density between 50 and 200 grams/liter.They are made by spray-drying an aluminum orthophosphate solution or suspension containing P.sub.2 O.sub.5 and Al.sub.2 O.sub.3 in the molar ratio desired in the final product, in a spray tower at temperatures higher thana 250.degree.C to effect direct transformation into condensed aluminum phosphates.
摘要翻译：本发明提供含有摩尔比等于或大于1.5:1的P 2 O 5和Al 2 O 3的浓缩磷酸铝，是X射线无定形的，表观密度在50-200克/升之间。

4. 发明授权

US4042324A Process for inhibiting the corrosions and deposition of boiler scale in water-conveying systems 失效
标题翻译：防止锅炉水垢在水输送系统中的腐蚀和沉积的过程
公开(公告)号：US4042324A
公开(公告)日：1977-08-16
申请号：US654885
申请日：1976-02-03
申请人： Theodor Auel , Hannsjorg Ulrich , Horst-Dieter Wasel-Nielen , Gero Heymer
发明人： Theodor Auel , Hannsjorg Ulrich , Horst-Dieter Wasel-Nielen , Gero Heymer
IPC分类号： C02F5/14 , C07F9/38 , C23F11/167 , C02B5/06 , C23F11/16
CPC分类号： C23F11/1676 , C02F5/14 , C07F9/3808 , C23F11/167
摘要： Corrosion and deposition of boiler scale in water-conveying systems are inhibited. To this end the water is admixed with at least one carboxy-alkane compound of phosphorus of the general formula: ##STR1## in which each of the substituents R.sup.1, R.sup.2, R.sup.3, and R.sup.4 stands for hydrogen or an alkyl group having from 1 to 4 carbon atoms, R.sup.5 stands for hydrogen, an OH-group or an alkyl group having from 1 to 3 carbon atoms, and n stands for 0 or 1, or with at least one water-soluble salt thereof.
摘要翻译：锅炉秤在输水系统中的腐蚀和沉积受到抑制。为此，将水与至少一种以下通式的磷的羧基烷烃化合物混合：其中每个取代基R 1，R 2，R 3和R 4代表氢或具有1至 4个碳原子，R5代表氢，OH-基团或具有1至3个碳原子的烷基，n代表0或1，或其至少一种水溶性盐。

5. 发明授权

US4346065A Process for the manufacture of finely dispersed sparingly soluble salts of oxyacids of phosphorus 失效
标题翻译：用于制造磷的含氧酸的微细分散的微溶盐的方法
公开(公告)号：US4346065A
公开(公告)日：1982-08-24
申请号：US222079
申请日：1981-01-02
申请人： Alexander Maurer , Renate Adrian , Gero Heymer
发明人： Alexander Maurer , Renate Adrian , Gero Heymer
IPC分类号： C01B25/16 , C01B25/163 , C01B25/26 , C01B25/32 , C01B25/34 , C01B25/37 , C01B25/42 , C09D5/08 , C01B15/16 , C04B11/22
CPC分类号： C01B25/322 , C01B25/16 , C01B25/163 , C01B25/265 , C01B25/34 , C01B25/37 , C01B25/377 , C01B25/42 , C09D5/084
摘要： The invention relates to a process for making a finely dispersed, sparingly soluble salt of an oxyacid of phosphorus, having a maximum particle size of 20 .mu.m, by reacting a compound of a divalent metal with the oxyacid of phosphorus or an alkali metal or ammonium salt thereof. More particularly, finely dispersed salt consisting to an extent of at least 90% of particles with a size between 0.05 and 7 .mu.m is made. To this end, an at least 5% by weight aqueous solution or suspension of a compound of a divalent metal selected from the group Mg, Ca, Sr, Ba, Mn, Zn, Cu, Cd, Pb, Sn, Co and Ni is reacted, while maintaining a pH range of between 3 and 9 and while stirring, with an at least 2 mol % solution of at least one trivalent metal selected from the group Al, Fe and Cr in the oxyacid of phosphorus and, optionally, with an aqueous solution of an alkali metal or ammonium salt of the oxyacid of phosphorus, and the precipitated salt is separated off and dried.
摘要翻译：本发明涉及通过使二价金属的化合物与磷或碱金属或铵的含氧酸反应来制造磷的含氧酸的微细分散，微溶的最大粒度为20μm的盐的方法的盐。更具体地说，制备了至少90％粒度在0.05和7μm之间的颗粒的程度的精细分散的盐。为此，选自Mg，Ca，Sr，Ba，Mn，Zn，Cu，Cd，Pb，Sn，Co和Ni中的二价金属的化合物的至少5重量％的水溶液或悬浮液是反应，同时保持pH范围在3和9之间并在搅拌的同时，使用至少2mol％的选自Al，Fe和Cr中的至少一种选自Al，Fe和Cr的三价金属的溶液在磷的含氧酸中，并且任选地与将磷酸的含氧酸的碱金属或铵盐的水溶液分离出来并干燥。

6. 发明授权

US4294621A Production of an anticorrosive pigment on phosphate basis 失效
标题翻译：以磷酸盐为基础生产防腐颜料
公开(公告)号：US4294621A
公开(公告)日：1981-10-13
申请号：US141135
申请日：1980-04-16
申请人： Alexander Maurer , Renate Adrian , Klaus Hestermann , Gero Heymer
发明人： Alexander Maurer , Renate Adrian , Klaus Hestermann , Gero Heymer
IPC分类号： C09D5/08 , C01B25/32 , C09C1/00 , C09C1/02 , C08K3/10
CPC分类号： C01B25/322 , C01B25/325 , C09C1/02 , C01P2004/61 , C01P2006/12
摘要： The invention relates to the production of phosphorus-containing anticorrosive pigments with a particle size of at most 20 microns by reacting one or more calcium or magnesium compounds with phosphoric acid or acid alkali metal or ammonium phosphates by intimately mixing an aqueous suspension or solution of the reactants inside a dispersing means rotating at a speed of 3000 to 10,000 rpm. More particularly, fine pulverulent calcium and magnesium compounds are converted, with agitation, together with water and, if desired, a water-soluble alkanol to a homogeneous suspension or solution. The suspension or solution is intimately mixed, inside the dispersing means at 0.degree. to 40.degree. C. and in an approximately stoichiometric ratio, with the phosphoric acid or acid phosphate solution. Resulting and precipitated pigment is separated and dried under mild conditions while maintaining its content of water of crystallization. The anticorrosive pigment is comprised of a homogeneous mixture and/or mixed crystals of which 10 to 95 mol % is calcium hydrogen phosphate dihydrate, the balance being magnesium hydrogen phosphate trihydrate. An at least 55 weight % proportion consists of particles with a size of up to 5 microns with a BET-surface of at least 1 m.sup.2 /g.
摘要翻译：本发明涉及通过使一种或多种钙或镁化合物与磷酸或酸性碱金属或铵磷酸盐反应，通过将下列物质的水性悬浮液或溶液紧密混合，从而生产粒径至多为20微米的含磷防腐颜料分散装置内的反应物以3000至10,000rpm的速度旋转。更具体地，精细的粉末状钙和镁化合物在搅拌下与水一起转化，如果需要，将水溶性链烷醇转化成均匀的悬浮液或溶液。悬浮液或溶液在分散装置内在0℃至40℃下以大约化学计量比与磷酸或酸式磷酸盐溶液紧密混合。将所得沉淀的颜料分离并在温和条件下干燥，同时保持其结晶水含量。防腐颜料由均匀的混合物和/或其中10〜95摩尔％为磷酸氢钙二水合物的混合晶体组成，余量为磷酸氢二氢钙三水合物。至少55重量％的比例由尺寸高达5微米，BET表面至少为1m 2 / g的颗粒组成。

7. 发明授权

US4396586A Process for making long-chain ammonium polyphosphate 失效
标题翻译：制造长链多磷酸铵的方法
公开(公告)号：US4396586A
公开(公告)日：1983-08-02
申请号：US309902
申请日：1981-10-09
申请人： Alexander Maurer , Jurgen Stenzel , Gero Heymer
发明人： Alexander Maurer , Jurgen Stenzel , Gero Heymer
IPC分类号： C09K21/02 , C01B25/40 , C09K21/12 , C01B25/28
CPC分类号： C01B25/405
摘要： The invention relates to a process for making long chain ammonium polyphosphate consisting essentially of crystalline modification II. To this end, a mixture of phosphorus pentoxide and ammonium orthophosphate in a molar ratio of 1:0.9 to 1:1.1 is reacted with 0.1 to 15 mol % of melamine or its condensation products selected from melam, melem or mellon, calculated as melamine, at a temperature within the range 50.degree. to 150.degree. C. in the presence of an excess of ammonia and the reaction product is heat-treated at temperatures within the range 200.degree. to 400.degree. C.
摘要翻译：本发明涉及一种制备基本上由结晶改性II组成的长链多磷酸铵的方法。为此，以摩尔比1:0.9至1:1.1的五氧化二磷和正磷酸铵的混合物与0.1至15mol％的三聚氰胺或其选自蜜胺，蜜胺或梅隆的缩合产物以三聚氰胺计算，在过量氨的存在下，在50〜150℃的温度范围内，将反应产物在200〜400℃的温度范围内进行热处理。

8. 发明授权

US4279878A Process for freeing phosphoric acid from organic contaminants 失效
标题翻译：从有机污染物中释放磷酸的方法
公开(公告)号：US4279878A
公开(公告)日：1981-07-21
申请号：US131234
申请日：1980-03-17
申请人： Alexander Maurer , Klaus Schrodter , Gero Heymer
发明人： Alexander Maurer , Klaus Schrodter , Gero Heymer
IPC分类号： C01B25/237 , B01J23/00 , C01B25/235 , C01B25/16
CPC分类号： C01B25/235
摘要： The invention relates to a process for freeing aqueous phosphoric acid solutions from organic contaminants. To this end, the solutions are admixed and reacted with hydrogen peroxide in the presence of a catalyst consisting of a noble metal or metal oxide being inert with respect to phosphoric acid or of a mixture of said noble metal and metal oxide.
摘要翻译：本发明涉及从有机污染物中释放磷酸水溶液的方法。为此，在由相对于磷酸或所述贵金属和金属氧化物的混合物呈惰性的贵金属或金属氧化物组成的催化剂存在下，将溶液混合并与过氧化氢反应。

9. 发明授权

US4399114A Process for the dearsenification of polyphosphoric acid 失效
标题翻译：多磷酸脱砷方法
公开(公告)号：US4399114A
公开(公告)日：1983-08-16
申请号：US402941
申请日：1982-07-29
申请人： Alexander Maurer , Gero Heymer , Markus Erpenbach
发明人： Alexander Maurer , Gero Heymer , Markus Erpenbach
IPC分类号： C01B25/24 , C01B25/16
CPC分类号： C01B25/24
摘要： The disclosure relates to a process for the continuous dearsenification of polyphosphoric acid with the aid of hydrogen sulfide in a gas admission zone. To this end, the disclosure provides for the acid to be dearsenified in a gas admission zone subdivided so as to comprise at least two separate liquid matter-receiving zones, each zone being separated from the other by means of a separate gas zone; for the liquid in each of the liquid matter-receiving zones to be maintained at a level 0.1 up to 10 cm high, without admission of gas; for hydrogen sulfide which remained unreacted in the individual liquid matter-receiving zones to be collected in the respective gas zone and for it to be finely redispersed in the liquid matter-receiving zone directly upstream of the respective gas zone by allowing the hydrogen sulfide to flow through a plurality of openings into the acid, the latter being delivered from the respective liquid-matter-receiving zone into the next downstream liquid-matter-receiving zone, and introduced thereinto directly below the liquid matter level therein; for precipitated arsenic sulfide to be separated from the acid coming from the lower end of the gas admission zone, and for the filtrate obtained to be freed from gaseous hydrogen sulfide in excess.
摘要翻译：本公开涉及在气体入口区借助硫化氢连续脱砷多磷酸的方法。为此，本公开内容提供了在气体进入区域中进行脱砷的酸，其被细分为包括至少两个分离的液体物质接收区域，每个区域通过单独的气体区域与另一个区域分离; 使每个液体物质接收区域中的液体保持在0.1至10厘米高的水平，而不允许气体; 对于在各个液体物质接收区中保持未反应的硫化氢，其被收集在各个气体区中，并且通过允许硫化氢流动直接在各个气体区的上游被精细地再分散在液体物质接收区中通过多个开口进入酸，后者从相应的液体接收区输送到下一个下游液体接收区，并直接在其中引入液体物质的下方; 使沉淀的硫化砷与气体入口区的下端的酸分离，得到的过滤得到的无水硫化氢的滤液。

10. 发明授权

US4705529A Process for reducing the reactivity and improving the flow behavior of phosphorus pentoxide 失效
标题翻译：减少五氧化二磷的反应活性和改善流动行为的方法
公开(公告)号：US4705529A
公开(公告)日：1987-11-10
申请号：US818719
申请日：1986-01-14
申请人： Gunther Schimmel , Werner Kowalski , Gero Heymer , Reinhard Gradl
发明人： Gunther Schimmel , Werner Kowalski , Gero Heymer , Reinhard Gradl
IPC分类号： C01B25/12
CPC分类号： C01B25/12
摘要： The reactivity of phosphorus pentoxide is reduced and its flow behavior improved. To this end, phosphorus pentoxide in the form of its hexagonal modification is annealed over a period of 0.5 to 8 hours at temperatures of 200.degree. to 390.degree. C.
摘要翻译：五氧化二磷的反应性降低，流动性提高。为此，以六角形改性形式的五氧化二磷在200〜390℃的温度下退火0.5〜8小时。

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