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1. 发明授权

US5319111A Preparation of tetrahydrofuran and gamma-butyrolactone 失效
标题翻译：四氢呋喃和γ-丁内酯的制备
公开(公告)号：US5319111A
公开(公告)日：1994-06-07
申请号：US931117
申请日：1992-08-17
申请人： Horst Zimmermann , Karl Brenner , Hans-Juergen Scheiper , Wolfgang Sauer , Horst Hartmann
发明人： Horst Zimmermann , Karl Brenner , Hans-Juergen Scheiper , Wolfgang Sauer , Horst Hartmann
IPC分类号： C07D307/08 , C07D307/33 , C07D315/00
CPC分类号： C07D315/00 , C07D307/08
摘要： A process for the preparation of tetrahydrofuran or tetrahydrofuran and .gamma.-butyrolactone from the product of the hydrogenation of maleic acid, succinic acid, maleic anhydride, succinic anhydride and/or fumaric acid, by treating the crude hydrogenation product, without prior work-up, at from 100.degree. to 300.degree. C. with a protic acid, and isolating pure tetrahydrofuran and .gamma.-butyrolactone from the resultant reaction mixture by distillation.
摘要翻译：马来酸，琥珀酸，马来酸酐，琥珀酸酐和/或富马酸的氢化产物中四氢呋喃或四氢呋喃和γ-丁内酯的制备方法，通过处理粗制氢化产物，无需事先处理，在100〜300℃下用质子酸，通过蒸馏从得到的反应混合物中分离纯四氢呋喃和γ-丁内酯。

2. 发明授权

US4940805A Preparation of 1,4-butanediol or tetrahydrofuran or both 失效
标题翻译： 1,4-丁二醇或四氢呋喃或二者的制备
公开(公告)号：US4940805A
公开(公告)日：1990-07-10
申请号：US230015
申请日：1988-08-08
申请人： Rolf Fischer , Hans-Juergen Gosch , Wolfgang Harder , Klaus-Dieter Malsch , Manfred Eggersdorfer , Lothar Franz , Horst Zimmermann , Karl Brenner , Klaus Halbritter , Wolfgang Sauer , Hans-Juergen Scheiper
发明人： Rolf Fischer , Hans-Juergen Gosch , Wolfgang Harder , Klaus-Dieter Malsch , Manfred Eggersdorfer , Lothar Franz , Horst Zimmermann , Karl Brenner , Klaus Halbritter , Wolfgang Sauer , Hans-Juergen Scheiper
IPC分类号： B01J27/18 , B01J27/19 , C07B61/00 , C07C27/00 , C07C29/136 , C07C29/147 , C07C29/149 , C07C29/17 , C07C29/56 , C07C31/20 , C07C67/00 , C07D307/08
CPC分类号： C07D307/08 , C07C29/177
摘要： Process for the preparation of 1,4-butanediol or tetrahydrofuran or both by the catalytic hydrogenation of maleic anhydride, succinic anhydride, maleic acid, succinic acid, fumaric acid, or the alkyl esters of these acids at temperatures of from 100.degree. C. to 350.degree. C. and pressures of from 50 bar to 350 bar over a catalyst containing cobalt as the active metal and one or both of the elements copper and phosphorus, if necessary in the presence of an aliphatic alcohol.
摘要翻译：通过马来酸酐，琥珀酸酐，马来酸，琥珀酸，富马酸或这些酸的烷基酯的催化氢化制备1,4-丁二醇或四氢呋喃或二者的方法，温度为100℃至 350℃，并且在含有钴作为活性金属的催化剂和一种或两种元素铜和磷的催化剂中，如果需要，在脂族醇的存在下，压力为50巴至350巴。

3. 发明授权

US5149884A Tube bundle reactor, use thereof in exothermic organic reactions, and preparation of ketones and aldehydes using same 失效
标题翻译：管组件反应器，在有机有机反应中使用，以及使用其制备酮和醛
公开(公告)号：US5149884A
公开(公告)日：1992-09-22
申请号：US680631
申请日：1991-04-01
申请人： Karl Brenner , Wilhelm Ruppel , Otto Woerz , Klaus Halbritter , Hans-Juergen Scheiper , Werner Aquila , Hartwig Fuchs
发明人： Karl Brenner , Wilhelm Ruppel , Otto Woerz , Klaus Halbritter , Hans-Juergen Scheiper , Werner Aquila , Hartwig Fuchs
IPC分类号： B01J8/06 , C07B61/00 , C07C45/00 , C07C45/38 , C07C45/39 , C07C47/21 , C07C67/00
CPC分类号： B01J8/067 , C07C45/38 , C07C45/39 , B01J2208/00212 , B01J2208/0053
摘要： In a tube bundle reactor for carrying out catalytic organic reactions in the gas phase, comprising reaction tubes (A) arranged between tubesheets (B), the reaction tubes have an inside diameter ranging from 0.5 to 3 cm, the ratio of reaction tube length to inside diameter ranges from 2 to 10, and the reaction tubes (A) are surrounded by a fluid heat transport medium flowing in the crosswise direction; said tube bundle reactor is useful in particular in exothermic organic reactions.
摘要翻译：在用于在气相中进行催化有机反应的管束反应器中，包括布置在管板（B）之间的反应管（A），反应管的内径范围为0.5至3cm，反应管长度与内径为2〜10，反应管（A）由沿横向流动的流体传热介质包围; 所述管束反应器尤其可用于放热有机反应中。

4. 发明授权

US4431844A Preparation of polyunsaturated ketones 失效
标题翻译：多不饱和酮的制备
公开(公告)号：US4431844A
公开(公告)日：1984-02-14
申请号：US361249
申请日：1982-03-24
申请人： Lothar Janitschke , Werner Hoffmann , Lothar Arnold , Manfred Stroezel , Hans-Juergen Scheiper
发明人： Lothar Janitschke , Werner Hoffmann , Lothar Arnold , Manfred Stroezel , Hans-Juergen Scheiper
IPC分类号： C07C45/00 , C07C45/74 , C07C49/203 , C07C67/00 , C07C45/45
CPC分类号： C07C49/203 , C07C45/74
摘要： An improved process for the preparation of unsaturated ketones of the general formula I ##STR1## where R.sup.1 is --CH.sub.3, ##STR2## and R.sup.2 and R.sup.3 are different and each is H or --CH.sub.3, by reacting an aldehyde of the general formula II ##STR3## with a molar excess of acetone or methyl ethyl ketone at an elevated temperature in the presence of an aqueous alkali metal hydroxide solution, wherein (a) all the reactants are mixed thoroughly, (b) the temperature is kept at from 10 to 120.degree. C. above the boiling point of the lowest-boiling component and (c) the pressure is kept at from p to 100 bar, where p is the vapor pressure of the mixture at the reaction temperature.The products methylpseudoionone, dimethylpseudoionone, pseudoirone, methylpseudoirone and dimethylpseudoirone are useful scents and scent intermediates. In addition, pseudoionone is an important intermediate for the industrial preparation of vitamin A, and 6-methyl-hepta-3,5-dien-2-one is a sought-after aromatic.
摘要翻译：制备通式I（I）的不饱和酮的改进方法，其中R 1为-CH 3，R 2和R 3不同，各自为H或-CH 3，通式在碱金属氢氧化物水溶液的存在下，在升高的温度下用摩尔过量的丙酮或甲基乙基酮制备式II（II）化合物，其中（a）所有反应物充分混合，（b）温度为保持在最低沸点组分的沸点以上10至120℃，和（c）压力保持在p至100巴，其中p是反应温度下混合物的蒸气压。产物甲基假ion酮，二甲基假ion酮，假呋酮，甲基假酮和二甲基假酮是有用的香味和香味中间体。此外，假雄酮是维生素A工业制备的重要中间体，6-甲基 - 庚-3,5-二烯-2-酮是一种追求的芳香族。

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