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1. 发明授权

US5208325A Cationic 1,3,4-thiadiazole dyestuffs 失效
公开(公告)号：US5208325A
公开(公告)日：1993-05-04
申请号：US805147
申请日：1991-12-11
申请人： Horst Berneth , Klaus Leverenz
发明人： Horst Berneth , Klaus Leverenz
IPC分类号： C09B44/20 , C07D285/12 , C07D285/135 , C09B44/10 , C09D11/00 , C09D11/02 , D06P1/08 , D06P3/76 , D21H21/28
CPC分类号： C07D285/135 , C09B44/107
摘要： Cationic 1,3,4-thiadiazole dyestuff of the formula ##STR1##in whichR.sup.1 and R.sup.2, independently of one another, denote hydrogen, alkyl, alkenyl, cycloalkyl, aralkyl, aryl, a heterocycle, said heterocycle having a direct bond to the nitrogen atom, or being bound through a methylene or ethylene group, or R.sup.1 and R.sup.2, together with the nitrogen atom to which they are attached form a heterocycle,R.sup.3 denotes alkyl, alkenyl or aralkyl,R.sup.4 denotes hydrogen or alkyl,R.sup.5 denotes acyl,R.sup.6 and R.sup.7, independently of one another, denote hydrogen, alkyl, alkoxy, aryloxy or halogen andR.sup.8 and R.sup.9, independently of one another, denote hydrogen, alkyl, alkenyl, cycloalkyl, aralkyl, aryl, a heterocycle, said heterocycle having a direct bond to the nitrogen atom, or being bound through a methylene or ethylene group, or R.sup.8 and R.sup.9, together with the nitrogen atom to which they are attached form a heterocycle, orR.sup.6 and R.sup.8 together with the nitrogen to which R.sup.8 is attached completes a heterocyclic, said R.sup.6 and R.sup.8 having a total of from 2 to 4 atoms, one of which can be oxygen or nitrogen, said heterocyclic being either unsubstituted or substituted with from 1 to 3 alkyl groups orR.sup.7 and R.sup.9, together with the nitrogen to which R.sup.9 is bound completes a heterocyclic, said R.sup.7 and R.sup.9 having a total of from 2 to 4 atoms, one of which may be oxygen or nitrogen, said heterocyclic being either unsubstituted or substituted with from 1 to 3 alkyl groups, andX.sup.e denotes an anion andin which all alkyl, alkenyl, cycloalkyl, aralkyl, aryl, alkoxy and heterocyclic radicals present may be substituted by nonionic substitutents, carboxyl groups, ammonium groups and/or pyridinium groups wherein the nonionic substituents are substituents selected from the group consisting of cyano, hydroxyl, fluorine, chlorine, bromine, nitro, alkyl, monoalkylamino, dialkylamino, alkoxy, phenyl, acyloxy, acylamino, alkoxycarbonyl and alkoxycarbonyloxy.

2. 发明授权

US4250089A Process for diazotizing aromatic amines 失效
标题翻译：芳胺重氮化方法
公开(公告)号：US4250089A
公开(公告)日：1981-02-10
申请号：US674930
申请日：1976-04-08
申请人： Klaus Leverenz
发明人： Klaus Leverenz
IPC分类号： C09B29/00 , C09B29/01 , C09B29/08 , C09B29/085 , C09B29/20 , C09B29/42 , C09B41/00 , C09B44/04 , C07C113/04 , C09B29/18 , C09B29/26
CPC分类号： C09B29/363 , C09B29/0003 , C09B29/08 , C09B29/0803 , C09B29/0809 , C09B29/20 , C09B41/00 , C09B44/04
摘要： The invention relates to a process for diazotizing aromatic amines which are not diazotizable, or only incompletely diazotizable, in aqueous media containing mineral acid. It is characterized in that the diazotization is effected by means of nitrosyl compounds in organic, dipolar, aprotic solvents which do not undergo a chemical reaction with the diazonium salts of the aromatic amines. The new process is distinguished by less contamination of the effluent.
摘要翻译：本发明涉及一种在含有无机酸的含水介质中重氮化芳族胺的方法，该方法不能重氮化，或仅不完全重氮化。其特征在于重氮化通过与芳族胺的重氮盐发生化学反应的有机，偶极，非质子溶剂中的亚硝基化合物进行。新工艺的特点是废水污染少。

3. 发明授权

US4810783A Process for the preparation of azo dyestuffs having an aniline-type coupler by aminolysis of the appropriate ether group-containing compounds 失效
标题翻译：通过合适的含醚基化合物的氨解制备具有苯胺型成色剂的偶氮染料的方法
公开(公告)号：US4810783A
公开(公告)日：1989-03-07
申请号：US21285
申请日：1987-03-03
申请人： Klaus Leverenz
发明人： Klaus Leverenz
IPC分类号： C07D275/04 , C09B29/09 , C09B29/12 , C09B43/44 , D06P3/36 , C09B29/045 , C09B29/26 , D06P3/54
CPC分类号： C09B43/44 , Y10S534/02
摘要： An azo dyestuff of the formula ##STR1## wherein D=a diazo component,R.sub.1 and R.sub.2 =alkyl or aralkyl,R.sub.3 =H, R or OR.sub.1 andR.sub.4 =a hydrocarbon radical or acyl,which are prepared in a simple manner by aminolysis with ammonia or an amine of the formula ##STR2## of an azo compound of the formula ##STR3## these dyestuffs dye polyester fibres in blue-green to green shades with good fastness to light.
摘要翻译：其中D =重氮组分，R1和R2 =烷基或芳烷基，R3 = H，R或OR1，R4 =烃基或酰基，其以D =重氮组分的偶氮染料，其以简单的方式通过氨解与氨或下式的偶氮化合物的“IMAGE”的胺，这些染料以蓝绿色至绿色的色调染色具有良好的耐光牢度的聚酯纤维。

4. 发明授权

US3962209A Process for preparing azo dyestuffs with ortho-azo cyano groups by cyano exchange of metal cyanides and halo dyestuffs 失效
标题翻译：通过CYANO交换金属氰化物和HALO DYESTUFFS制备具有OROO-AZO CYANO组的AZO DYESTUFFS的方法
公开(公告)号：US3962209A
公开(公告)日：1976-06-08
申请号：US361603
申请日：1973-05-18
申请人： Alois Gotteschlich , Klaus Leverenz
发明人： Alois Gotteschlich , Klaus Leverenz
IPC分类号： C09B29/08 , C09B43/42 , C09B43/00 , D06P1/18 , D06P3/26 , D06P3/54
CPC分类号： C09B29/0809 , C09B29/08 , C09B43/42
摘要： Azo dyestuffs having the formula ##EQU1## in which A is an aromatic carbocyclic radical containing the CN substituent in the o-position to the azo group and K is the radical of a coupling component as well as the process for their production are disclosed. The process involves cyano exchange between a metal cyanide, e.g. CuCN and the corresponding dyestuff containing Cl or Br instead of CN, in an organic solvent particularly polar aprotic organic solvents, e.g. dimethyl sulfoxide. The dyestuffs are suitable for dyeing a variety of fiber materials such as cotton, wool, silk as well as snythetic materials such as polyamide and polyethylene terphthalate to give dyeings which are characterized by great clearness and good general fastness properties.

5. 发明授权

US4083846A Process for the preparation of azo dyestuffs 失效
标题翻译：偶氮染料的制备方法
公开(公告)号：US4083846A
公开(公告)日：1978-04-11
申请号：US674929
申请日：1976-04-08
申请人： Klaus Leverenz
发明人： Klaus Leverenz
IPC分类号： C09B41/00 , C09B43/40 , C09B43/42 , C09B43/00 , C09B29/08 , C09B29/26
CPC分类号： C09B41/002 , C09B43/40 , C09B43/405 , C09B43/42
摘要： The invention relates to the preparation of azo dyestuffs which are free from sulphonic acid groups by diazotization, coupling and subsequent nucleophilic exchange of a halogen atom of the diazo component is in the o-position relative to the azo group. The process is characterized in that all the reaction steps are carried out in a neutral organic dipolar solvent, with the proviso that when using diazo components which are not diazotizable, or only incompletely diazotizable, in dilute aqueous mineral acids, the diazotization medium employed consists of aprotic solvents which do not undergo any chemical reaction with the diazonium salt of this component. The new process is distinguished by less contamination of the effluent.
摘要翻译：本发明涉及通过重氮化，偶联和随后的重氮组分的卤素原子的亲核交换在相对于偶氮基的o位置中不含磺酸基团的偶氮染料的制备。该方法的特征在于所有的反应步骤都是在中性有机偶极溶剂中进行的，条件是当使用稀有的无机酸水溶液中使用不能重氮化或不完全重氮化的重氮组分时，所用的重氮化介质包括不与该组分的重氮盐发生化学反应的非质子溶剂。新工艺的特点是废水污染少。

6. 发明授权

US3968099A Process for the preparation of azo dyestuffs containing cyano groups 失效
标题翻译：制备含氰基的偶氮染料的方法
公开(公告)号：US3968099A
公开(公告)日：1976-07-06
申请号：US542051
申请日：1975-01-17
申请人： Klaus Leverenz
发明人： Klaus Leverenz
IPC分类号： C09B43/42 , C09B43/00
CPC分类号： C09B43/42
摘要： The invention relates to the preparation of ortho-cyano azo dyestuffs by conversion of azo dyestuffs of the formula ##EQU1## wherein A is an aromatic-carbocyclic radical,K is the radical of a component andX is a chlorine, bromine or iodine atom which is in the o-position to the azo groupWith CuCN or CuCN-forming compounds in polar organic sovents in the presence of azoles.
摘要翻译：本发明涉及通过转化式X | AN = NK的偶氮染料制备邻氰基偶氮染料，其中A是芳族 - 碳环基团，K是组分的基团，X是氯，溴或碘在偶氮基存在下，在极性有机溶剂中与CuCN或CuCN形成化合物位于偶氮基的o位置的原子。

7. 发明授权

US4773915A Benzisothiazole azo dye for synthetic fibers 失效
标题翻译：用于合成纤维的苯并异噻唑偶氮染料
公开(公告)号：US4773915A
公开(公告)日：1988-09-27
申请号：US1266
申请日：1987-01-07
申请人： Winfried Kruckenberg , Klaus Leverenz , Hans-Gunter Otten
发明人： Winfried Kruckenberg , Klaus Leverenz , Hans-Gunter Otten
IPC分类号： C09B29/039 , C09B29/00 , C09B67/00 , C09B67/48 , D06P1/18 , D06P3/48
CPC分类号： C09B29/0081 , C09B67/0029 , Y10S8/922
摘要： Azo dyestuffs of the formula ##STR1## wherein R.sub.1 denotes hydrogen, C.sub.1 -C.sub.4 -alkoxy or C.sub.1 -C.sub.4 -alkoxyethoxy andX denotes acyl,are distinguished by good levelling properties and good allround fastness properties. They dye polyester fibres in a bright blue shade.
摘要翻译：其中R1表示氢，C1-C4-烷氧基或C1-C4-烷氧基乙氧基并且X表示酰基的式“IMAGE”的偶氮染料的特征在于良好的流平性和良好的全能牢度性质。他们在明亮的蓝色阴影下染色聚酯纤维。

8. 发明授权

US4424156A Halo-substituted amino-and substituted-sulphonamido-containing azo dyestuffs 失效
标题翻译：卤代氨基和取代磺酰氨基偶氮染料
公开(公告)号：US4424156A
公开(公告)日：1984-01-03
申请号：US185660
申请日：1980-09-10
申请人： Rainer Hamprecht , Klaus Leverenz
发明人： Rainer Hamprecht , Klaus Leverenz
IPC分类号： C09B29/08 , C09B29/036 , C09B29/039 , C09B29/085 , C09B29/09
CPC分类号： C09B29/0833 , Y10S534/02
摘要： An azo dyestuff suited for dyeing polyester, of the formula ##STR1## in which Hal is F, Cl, Br or I, R.sub.1 is a C.sub.1 -C.sub.10 -aliphatic hydrocarbyl or a C.sub.5 -C.sub.8 -cycloalkyl radical optionally substituted by OH, halogen, alkoxy, aryloxy or acyloxy, R.sub.2 is an optionally substituted aliphatic hydrocarbyl, aryl or hetaryl radical, R.sub.1 and R.sub.2 being free from --SO.sub.3 H and/or --COOH radicals, Z.sub.1 to Z.sub.4 each independently is hydrogen, alkyl, cycloalkyl, aralkyl, halogen, --CN, --NO.sub.2, --CF.sub.3, --SO.sub.2 Q, --SO.sub.2 NVW, --COW, --CONVW, --CO.sub.2 W, --OQ, --NVW, --NWCOW, --NWSO.sub.2 Q or --NHCO.sub.2 Q, or Z.sub.2 may also be arylazo, and Z.sub.3 may also be ##STR2## and Z.sub.3 and Z.sub.4 together can be ##STR3## Q is alkyl, aralykl or aryl, U is alkyl, V is H, alkyl or aralkyl, and W is V or aryl.
摘要翻译：适用于染色聚酯的偶氮染料，其中Hal为F，Cl，Br或I的式为“IMAGE”，R1为任选被OH，卤素取代的C 1 -C 10 - 脂族烃基或C 5 -C 8环烷基，烷氧基，芳氧基或酰氧基，R2是任选取代的脂族烃基，芳基或杂芳基，R1和R2不含-SO3H和/或-COOH基团，Z1至Z4各自独立地为氢，烷基，环烷基，芳烷基，卤素， -CN，-NO 2，-CF 3，-SO 2 Q，-SO 2 N V W，-COW，-CONVW，-CO 2 W，-OQ，-NVW，-NWCOW，-NWSO 2 Q或-NHCO 2 Q，或Z 2也可以是芳基偶氮，Z 3也可以并且Z 3和Z 4可以一起作为Q是烷基，芳烷基或芳基，U是烷基，V是H，烷基或芳烷基，W是V或芳基。

9. 发明授权

US4237048A Monoazo dyestuff containing di-cyano substituents ortho to the azo group 失效
标题翻译：含偶氮基团的二氰基取代基的单偶氮染料
公开(公告)号：US4237048A
公开(公告)日：1980-12-02
申请号：US649253
申请日：1976-01-15
申请人： Alois Gottschlich , Klaus Leverenz
发明人： Alois Gottschlich , Klaus Leverenz
IPC分类号： C09B29/08 , C09B43/42 , C09B29/26 , C09B29/36
CPC分类号： C09B43/42 , C09B29/08
摘要： Azo dyestuff having the formula ##STR1## in which A is an aromatic carbocyclic radical containing a CN substituent in the o-position to the azo group and K is the radical of a coupling component as well as the process for their production are disclosed. The process involves cyano exchange between a metal cyanide, e.g. CuCN and the corresponding dyestuff containing Cl or Br instead of CN, in an organic solvent particularly polar aprotic organic solvents, e.g. dimethyl sulfoxide. The dyestuffs are suitable for dyeing a variety of fiber material such as cotton, wool, silk as well as synthetic materials such as polyamide and polyethylene terephthalate to give dyeings which are characterized by great clearness and good general fastness properties.
摘要翻译：公开了具有式“IMAGE”的偶氮染料，其中A是在与偶氮基相邻的位置上含有CN取代基的芳族碳环基团，K是偶合组分的基团及其生产方法。该方法包括金属氰化物之间的氰基交换。 CuCN和相应的含有Cl或Br的染料代替CN，在有机溶剂中，特别是极性非质子有机溶剂，例如，二甲基亚砜。该染料适用于染色各种纤维材料如棉，羊毛，丝绸以及合成材料如聚酰胺和聚对苯二甲酸乙二醇酯，得到染色，其特征是具有很好的清晰度和良好的耐牢度。

10. 发明授权

US3954395A Mixtures of dyestuffs 失效
标题翻译：染料混合物
公开(公告)号：US3954395A
公开(公告)日：1976-05-04
申请号：US378810
申请日：1973-07-13
申请人： Klaus Leverenz
发明人： Klaus Leverenz
IPC分类号： C09B29/08 , C09B67/22 , D06P1/18 , D06P1/62 , D06P3/56 , C09B27/00 , C09B45/48 , D06P1/00 , D06P3/00
CPC分类号： C09B67/0051 , D06P1/625 , D06P3/56 , Y10S534/01 , Y10S8/922
摘要： Dyestuff mixtures of at least two different dyestuffs of the general formula ##SPC1##In whichX = cn, no.sub.2 or alkylsulphonylY = hydrogen, methyl, ethoxy or methoxyR.sub.1 = hydrogen or alkylR.sub.2 = c.sub.1 -c.sub.4 -alkyl or an optionally substituted phenyl radical or phenylalkyl radicalAc = acyl.Using these mixtures for dyeing of polyester fibres deep clear blue dyeings with good general fastness properties are obtained.
摘要翻译：至少两种不同的通式为：X = CN，NO 2或烷基磺酰基Y =氢，甲基，乙氧基或甲氧基的化合物的染料混合物R1 =氢或烷基R2 = C1-C4-烷基或任意取代的苯基或苯基烷基 Ac =酰基。

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