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1. 发明授权

US08304500B2 Polyglycolic acid resin particle composition and process for production thereof 有权
标题翻译：聚乙醇酸树脂颗粒组合物及其制备方法
公开(公告)号：US08304500B2
公开(公告)日：2012-11-06
申请号：US12084051
申请日：2006-10-26
申请人： Hiroyuki Sato , Fuminori Kobayashi , Fumio Akutsu , Katsushi Momose
发明人： Hiroyuki Sato , Fuminori Kobayashi , Fumio Akutsu , Katsushi Momose
IPC分类号： C08G63/08
CPC分类号： C08L67/04 , C08G63/08 , C08G63/912 , C08G2140/00 , C08L2205/02 , Y10T428/2982 , C08L2666/18
摘要： A particulate polyglycolic acid resin composition, comprising: a blend of a first particulate polyglycolic acid resin and a second particulate polyglycolic acid resin each having a moisture content of at most 110 ppm and providing a ratio of melt-viscosity (as measured at 270° C. and a shear rate of 121 sec−1; the same as hereinafter) therebetween of above 1 and at most 10. After the polymerization, the first and second particulate polyglycolic acid resins can cause change in properties before the forming (e.g., during storage); or during the forming process. However, by adequately determining the blending ratio between the resins while taking the melt-viscosities thereof into account, it becomes possible to provide a particulate polyglycolic acid resin composition showing a stable melt-formability and suitable as a starting material for various forming processes.
摘要翻译：一种颗粒状聚乙醇酸树脂组合物，其包含：第一颗粒聚乙醇酸树脂和第二颗粒状聚乙醇酸树脂的共混物，所述第二颗粒聚乙醇酸树脂的水分含量为至多110ppm，并且提供熔体粘度（在270℃下测量），剪切速率为121秒-1，下文相同）在1以上至10以下。聚合后，第一和第二颗粒状聚乙醇酸树脂在成型前会导致性能变化（例如，在储存期间）; 或在成型过程中。然而，通过充分确定树脂之间的共混比，同时考虑其熔融粘度，可以提供显示出稳定的熔融成型性的颗粒聚乙醇酸树脂组合物，并且适合作为各种成型方法的原料。

2. 发明授权

US07538179B2 Process for producing aliphatic polyester 有权
标题翻译：生产脂肪族聚酯的方法
公开(公告)号：US07538179B2
公开(公告)日：2009-05-26
申请号：US10577379
申请日：2004-11-04
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
IPC分类号： C08G63/00 , C08G63/02
CPC分类号： C08G63/785 , C08G63/06 , C08G63/78 , C08K5/005 , C08K5/29 , C08L67/04
摘要： Ring-opening polymerization of a cyclic ester is performed by using an alcohol and water positively as initiators or/and molecular weight-adjusting agents to control the initial properties and properties with time of the resultant aliphatic polyester. More specifically, an aliphatic polyester is produced by ring-opening polymerization of a cyclic ester containing water and an alcohol based on a total proton concentration and a ratio between a mol concentration of carboxyl (carboxylic acid)-source compounds including water and a mol concentration of alkoxycarbonyl (ester)-source compounds, as polymerization-controlling indexes.
摘要翻译：通过使用醇和水作为引发剂或/和分子量调节剂来进行环酯的开环聚合，以控制所得脂肪族聚酯的初始性能和时间。更具体地说，通过含有水和醇的环酯的总质子浓度和包含水的羧基（羧酸）源化合物的摩尔浓度和摩尔浓度之间的比率来制造脂肪族聚酯的烷氧基羰基（酯）源化合物，作为聚合控制指标。

3. 发明申请

US20070073032A1 Process for producing aliphatic polyester 有权
标题翻译：生产脂肪族聚酯的方法
公开(公告)号：US20070073032A1
公开(公告)日：2007-03-29
申请号：US10575468
申请日：2004-10-14
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
IPC分类号： C08G63/02
CPC分类号： C08G63/912 , C08G63/08
摘要： An aliphatic polyester improved provided by using water positively as an initiator or/and a molecular weight-adjusting agent, is improved in moisture resistance. More specifically, a cyclic ester containing proton-source compounds including more than 80 ppm of water as an initiator or/and a molecular weight-adjusting agent, is subjected to ring-opening polymerization, and the resultant aliphatic polyester is compounded with a carboxyl group-capping agent to produce such an aliphatic polyester.
摘要翻译：通过使用水作为引发剂或/和分子量调节剂而提供的脂肪族聚酯改善了耐湿性。更具体地说，将包含大于80ppm水作为引发剂的质子源化合物或/和分子量调节剂的环状酯进行开环聚合，并将所得的脂肪族聚酯与羧基包覆剂以制备这种脂族聚酯。

4. 发明申请

US20120046414A1 METHOD FOR PRODUCING SOLID POLYGLYCOLIC ACID-BASED RESIN COMPOSITION 审中-公开
标题翻译：用于生产固体多羟基酸的树脂组合物的方法
公开(公告)号：US20120046414A1
公开(公告)日：2012-02-23
申请号：US13264837
申请日：2010-03-30
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Akiko Watanabe
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Akiko Watanabe
IPC分类号： C08L67/00
CPC分类号： C08G63/08 , C08G63/90
摘要： A method for producing a solid polyglycolic acid-based resin composition, including a cooling step of cooling a polyglycolic acid-based resin composition in a molten state by an aqueous medium, wherein in the cooling step, the polyglycolic acid-based resin composition in the molten state is cooled by being brought into contact with the aqueous medium so that a sodium ion concentration in an obtained solid polyglycolic acid-based resin composition can be less than 100 ppb by mass.
摘要翻译：一种固体聚乙醇酸系树脂组合物的制造方法，其特征在于，包括通过水性介质将熔融状态的聚乙醇酸系树脂组合物冷却的冷却工序，其中，在所述冷却工序中，所述聚乙醇酸系树脂组合物为熔融状态通过与水性介质接触而冷却，使得所得固体聚乙醇酸系树脂组合物中的钠离子浓度可以小于100ppb。

5. 发明授权

US07538178B2 Process for producing aliphatic polyester 有权
标题翻译：生产脂肪族聚酯的方法
公开(公告)号：US07538178B2
公开(公告)日：2009-05-26
申请号：US10575468
申请日：2004-10-14
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
IPC分类号： C08G63/02 , C08G64/00
CPC分类号： C08G63/912 , C08G63/08
摘要： An aliphatic polyester improved provided by using water positively as an initiator or/and a molecular weight-adjusting agent, is improved in moisture resistance. More specifically, a cyclic ester containing proton-source compounds including more than 80 ppm of water as an initiator or/and a molecular weight-adjusting agent, is subjected to ring-opening polymerization, and the resultant aliphatic polyester is compounded with a carboxyl group-capping agent to produce such an aliphatic polyester.
摘要翻译：通过使用水作为引发剂或/和分子量调节剂而提供的脂肪族聚酯改善了耐湿性。更具体地说，将包含大于80ppm水作为引发剂的质子源化合物或/和分子量调节剂的环状酯进行开环聚合，并将所得的脂肪族聚酯与羧基包覆剂以制备这种脂族聚酯。

6. 发明申请

US20070073033A1 Process for producing aliphatic polyester 有权
标题翻译：生产脂肪族聚酯的方法
公开(公告)号：US20070073033A1
公开(公告)日：2007-03-29
申请号：US10577379
申请日：2004-11-04
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yasushi Okada
IPC分类号： C08G63/02
CPC分类号： C08G63/785 , C08G63/06 , C08G63/78 , C08K5/005 , C08K5/29 , C08L67/04
摘要： Ring-opening polymerization of a cyclic ester is performed by using an alcohol and water positively as initiators or/and molecular weight-adjusting agents to control the initial properties and properties with time of the resultant aliphatic polyester. More specifically, an aliphatic polyester is produced by ring-opening polymerization of a cyclic ester containing water and an alcohol based on a total proton concentration and a ratio between a mol concentration of carboxyl (carboxylic acid)-source compounds including water and a mol concentration of alkoxycarbonyl (ester)-source compounds, as polymerization-controlling indexes.
摘要翻译：通过使用醇和水作为引发剂或/和分子量调节剂来进行环酯的开环聚合，以控制所得脂肪族聚酯的初始性能和时间。更具体地说，通过含有水和醇的环酯的总质子浓度和包含水的羧基（羧酸）源化合物的摩尔浓度和摩尔浓度之间的比率来制造脂肪族聚酯的烷氧基羰基（酯）源化合物，作为聚合控制指标。

7. 发明授权

US07501464B2 Process for producing aliphatic polyester composition 失效
标题翻译：脂肪族聚酯组合物的制造方法
公开(公告)号：US07501464B2
公开(公告)日：2009-03-10
申请号：US11588341
申请日：2006-10-27
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yuki Hokari
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yuki Hokari
IPC分类号： C08K5/521 , C08G63/02
CPC分类号： C08J3/201 , C08G63/912 , C08J2367/04 , C08K5/52 , C08L67/04
摘要： For producing an aliphatic polyester resin composition containing a thermal stabilizer and a carboxyl group-capping agent, the aliphatic polyester resin is first mixed in a hot-melt state with the thermal stabilizer and then mixed in a hot-melt state with the carboxyl group-capping agent. As a result thereof, the resultant aliphatic polyester resin composition is provided with better moisture resistance and noticeably improved heat resistance (less coloring) than in the case where these additives are simultaneously added to effect the hot-melt mixing.
摘要翻译：为了制造含有热稳定剂和羧基封端剂的脂肪族聚酯树脂组合物，首先将脂族聚酯树脂与热稳定剂以热熔状态混合，然后以热熔状态与羧基 - 封端剂。其结果是，所得到的脂肪族聚酯树脂组合物与同时加入这些添加剂以实现热熔混合的情况相比，具有更好的耐湿性和显着改善的耐热性（较少着色）。

8. 发明授权

US08362158B2 Polyglycolic acid resin composition 有权
标题翻译：聚乙醇酸树脂组合物
公开(公告)号：US08362158B2
公开(公告)日：2013-01-29
申请号：US12085566
申请日：2006-11-30
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi
IPC分类号： C08G63/08
CPC分类号： C08J5/18 , C08J2367/04 , C08K5/25 , C08K5/29 , C08L67/04
摘要： A polyglycolic acid resin composition having improved moisture resistance is obtained by adding a carboxyl group-capping agent and a polymerization catalyst-deactivation agent to a polyglycolic acid resin.
摘要翻译：通过在聚乙醇酸树脂中加入羧基封端剂和聚合催化剂失活剂，得到耐湿性提高的聚乙醇酸树脂组合物。

9. 发明申请

US20090131602A1 Polyglycolic Acid Resin Particle Composition and Process for Production Thereof 有权
标题翻译：聚乙醇酸树脂颗粒组合物及其制备方法
公开(公告)号：US20090131602A1
公开(公告)日：2009-05-21
申请号：US12084051
申请日：2006-10-26
申请人： Hiroyuki Sato , Fuminori Kobayashi , Fumio Akutsu , Katsushi Momose
发明人： Hiroyuki Sato , Fuminori Kobayashi , Fumio Akutsu , Katsushi Momose
IPC分类号： C08G63/06
CPC分类号： C08L67/04 , C08G63/08 , C08G63/912 , C08G2140/00 , C08L2205/02 , Y10T428/2982 , C08L2666/18
摘要： A particulate polyglycolic acid resin composition, comprising: a blend of a first particulate polyglycolic acid resin and a second particulate polyglycolic acid resin each having a moisture content of at most 110 ppm and providing a ratio of melt-viscosity (as measured at 270° C. and a shear rate of 121 sec−1; the same as hereinafter) therebetween of above 1 and at most 10. After the polymerization, the first and second particulate polyglycolic acid resins can cause change in properties before the forming (e.g., during storage); or during the forming process. However, by adequately determining the blending ratio between the resins while taking the melt-viscosities thereof into account, it becomes possible to provide a particulate polyglycolic acid resin composition showing a stable melt-formability and suitable as a starting material for various forming processes.
摘要翻译：一种颗粒状聚乙醇酸树脂组合物，其包含：第一颗粒聚乙醇酸树脂和第二颗粒状聚乙醇酸树脂的共混物，所述第二颗粒聚乙醇酸树脂的水分含量为至多110ppm，并且提供熔体粘度（在270℃下测量），剪切速率为121秒-1，下文相同）在1以上至10以下。聚合后，第一和第二颗粒状聚乙醇酸树脂在成型前会导致性能变化（例如，在储存期间）; 或在成型过程中。然而，通过充分确定树脂之间的共混比，同时考虑其熔融粘度，可以提供显示出稳定的熔融成型性的颗粒聚乙醇酸树脂组合物，并且适合作为各种成型方法的原料。

10. 发明申请

US20070100037A1 Process for producing aliphatic polyester composition 失效
标题翻译：脂肪族聚酯组合物的制造方法
公开(公告)号：US20070100037A1
公开(公告)日：2007-05-03
申请号：US11588341
申请日：2006-10-27
申请人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yuki Hokari
发明人： Hiroyuki Sato , Fumio Akutsu , Fuminori Kobayashi , Yuki Hokari
IPC分类号： C08K5/49
CPC分类号： C08J3/201 , C08G63/912 , C08J2367/04 , C08K5/52 , C08L67/04
摘要： For producing an aliphatic polyester resin composition containing a thermal stabilizer and a carboxyl group-capping agent, the aliphatic polyester resin is first mixed in a hot-melt state with the thermal stabilizer and then mixed in a hot-melt state with the carboxyl group-capping agent. As a result thereof, the resultant aliphatic polyester resin composition is provided with better moisture resistance and noticeably improved heat resistance (less coloring) than in the case where these additives are simultaneously added to effect the hot-melt mixing.
摘要翻译：为了制造含有热稳定剂和羧基封端剂的脂肪族聚酯树脂组合物，首先将脂族聚酯树脂与热稳定剂以热熔状态混合，然后以热熔状态与羧基 - 封端剂。其结果是，所得到的脂肪族聚酯树脂组合物与同时加入这些添加剂以实现热熔混合的情况相比，具有更好的耐湿性和显着改善的耐热性（较少着色）。

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