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1. 发明授权

US08765857B2 Particulate water retaining material for cultivating plant having water absorbent resin as main component 有权
标题翻译：用于培养具有吸水性树脂作为主要成分的植物的颗粒保水材料
公开(公告)号：US08765857B2
公开(公告)日：2014-07-01
申请号：US10581343
申请日：2004-12-06
申请人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
发明人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
IPC分类号： C08K3/26 , C08K3/22 , C08F220/06 , A01G7/00
CPC分类号： A01G24/00 , A01G24/35
摘要： A particulate water retaining material for cultivating plant comprising (A) a carboxyl group-containing water-insoluble water absorbent resin and (B) a polyvalent metal compound, by having the compound (B) deposited on the rerin (A), it is made possible to possess an outstanding water absorbing property without impairing the growth of a plant.
摘要翻译：一种含有（A）含羧基的水不溶性吸水性树脂和（B）多价金属化合物的用于培养植物的颗粒状保水材料，通过使化合物（B）沉积在芦丁（A）上，制成可能具有优异的吸水性，而不损害植物的生长。

2. 发明申请

US20070101644A1 Particulate water retaining material for cultivating plant having water absorbent resin as main component 有权
标题翻译：用于培养具有吸水性树脂作为主要成分的植物的颗粒保水材料
公开(公告)号：US20070101644A1
公开(公告)日：2007-05-10
申请号：US10581343
申请日：2004-12-06
申请人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
发明人： Hirotama Fujimaru , Yorimichi Dairoku , Kunihiko Ishizaki , Yoshifumi Adachi , Nobuyuki Harada
IPC分类号： A01G7/00
CPC分类号： A01G24/00 , A01G24/35
摘要： A particulate water retaining material for cultivating plant comprising (A) a carboxyl group-containing water-insoluble water absorbent resin and (B) a polyvalent metal compound, by having the compound (B) deposited on the the rerin (A), it is made possible to possess an outstanding water absorbing property without impairing the growth of a plant.
摘要翻译：含有（A）含羧基的水不溶性吸水性树脂和（B）多价金属化合物的栽培植物用颗粒状保水材料，通过使化合物（B）沉积在rerin（A）上，是使得具有优异的吸水性而不损害植物的生长成为可能。

3. 发明授权

US08481664B2 Particulate water absorbing agent including polyacrylic acid (polyacrylate) based water absorbing resin as a principal component, method for production thereof, water-absorbent core and absorbing article in which the particulate water absorbing agent is used 有权
标题翻译：以聚丙烯酸（聚丙烯酸酯）系吸水性树脂为主要成分的颗粒状吸水剂，其制造方法，吸水性芯和使用该颗粒状吸水剂的吸收性物品
公开(公告)号：US08481664B2
公开(公告)日：2013-07-09
申请号：US11911169
申请日：2006-04-11
申请人： Yorimichi Dairoku , Hirotama Fujimaru , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Hirotama Fujimaru , Kunihiko Ishizaki
IPC分类号： C08F20/06 , A61F13/15 , A61F13/20
CPC分类号： A61L15/60 , A61L15/24 , B01J2220/68 , C08L33/02
摘要： As a characteristic that had not been known conventionally at all, “permeability potential under pressure (PPUP)” of a particulate water absorbing agent is regulated, and further, “range of particle size distribution” and “coloring” are concomitantly regulated. The present invention is directed to a particulate water absorbing agent having the following (a) to (c): (a) permeability potential under pressure (PPUP) being 50 to 100%; (b) yellowness index (YI) being 0 to 10, and rate of change of yellowness index (ΔYI) being 100 to 150% following a coloring acceleration test for 14 days at 70±1° C. and the relative humidity of 95±1%; and (c) particles of smaller than 150 μm specified by standard sieve classification accounting for 0 to 5% by weight, weight average particle diameter (D50) being 200 to 550 μm, and logarithmic standard deviation (σζ) of particle size distribution being 0.20 to 0.40.
摘要翻译：作为传统上已知的特征，调节了颗粒状吸水剂的“压力下的渗透势（PPUP）”，并且进一步调节“粒度分布范围”和“着色”。本发明涉及具有以下（a）至（c）的颗粒状吸水剂：（a）压力下的渗透势（PPUP）为50〜100％（b）在70±1℃下，着色加速试验14天，黄色指数（YI）为0〜10，黄色指数变化率（ΔYI）为100〜150％，相对湿度为95± 1％; 和（c）通过标准筛分类而规定的小于150μm的颗粒，其重量平均粒径（D50）为0-5重量％，平均粒径（D50）为200-550μm，粒度分布的对数标准偏差（sigmazeta）为0.20 至0.40。

4. 发明申请

US20090318885A1 Particulate Water Absorbing Agent Including Polyacrylic Acid (Polyacrylate) Based Water Absorbing Resin as a Principal Component, Method for Production Thereof, Water-Absorbent Core and Absorbing Article in Which the Particulate Water Absorbing Agent is Used 有权
标题翻译：包含聚丙烯酸（聚丙烯酸酯）基吸水树脂作为主要成分的颗粒吸水剂，其制造方法，吸水芯和吸收性物质，其中使用颗粒吸水剂
公开(公告)号：US20090318885A1
公开(公告)日：2009-12-24
申请号：US11911169
申请日：2006-04-11
申请人： Yorimichi Dairoku , Hirotama Fujimaru , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Hirotama Fujimaru , Kunihiko Ishizaki
IPC分类号： A61F13/53 , C08F20/06 , B01J20/26 , C08F263/02
CPC分类号： A61L15/60 , A61L15/24 , B01J2220/68 , C08L33/02
摘要： As a characteristic that had not been known conventionally at all, “permeability potential under pressure (PPUP)” of a particulate water absorbing agent is regulated, and further, “range of particle size distribution” and “coloring” are concomitantly regulated. The present invention is directed to a particulate water absorbing agent having the following (a) to (c): (a) permeability potential under pressure (PPUP) being 50 to 100%; (b) yellowness index (YI) being 0 to 10, and rate of change of yellowness index (ΔYI) being 100 to 150% following a coloring acceleration test for 14 days at 70±1° C. and the relative humidity of 95±1%; and (c) particles of smaller than 150 μm specified by standard sieve classification accounting for 0 to 5% by weight, weight average particle diameter (D50) being 200 to 550 μm, and logarithmic standard deviation (σζ) of particle size distribution being 0.20 to 0.40.
摘要翻译：作为传统上已知的特征，调节了颗粒状吸水剂的“压力下的渗透势（PPUP）”，并且进一步调节“粒度分布范围”和“着色”。本发明涉及具有以下（a）至（c）的颗粒状吸水剂：（a）压力下的渗透势（PPUP）为50〜100％（b）在70±1℃下，着色加速试验14天，黄色指数（YI）为0〜10，黄色指数变化率（ΔYI）为100〜150％，相对湿度为95± 1％; 和（c）通过标准筛分类而规定的小于150μm的颗粒，其重量平均粒径（D50）为0-5重量％，平均粒径（D50）为200-550μm，粒度分布的对数标准偏差（sigmazeta）为0.20 至0.40。

5. 发明授权

US06992144B2 Water-absorbent agent, method for production thereof, and water-absorbent composition 失效
标题翻译：吸水剂，其制造方法和吸水性组合物
公开(公告)号：US06992144B2
公开(公告)日：2006-01-31
申请号：US10229111
申请日：2002-08-28
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08F8/32
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

6. 发明申请

US20060025536A1 Absorbent resin composition 有权
标题翻译：吸收性树脂组合物
公开(公告)号：US20060025536A1
公开(公告)日：2006-02-02
申请号：US11228332
申请日：2005-09-19
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08F120/02 , C08F120/62
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

7. 发明授权

US07250459B2 Absorbent resin composition 有权
标题翻译：吸收性树脂组合物
公开(公告)号：US07250459B2
公开(公告)日：2007-07-31
申请号：US11228332
申请日：2005-09-19
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： C08K5/09
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14 , C08L33/02
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力在20g / cm 2以下的负载不小于30（ml / g），残留量为不大于2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

8. 发明授权

US5610208A Water-absorbent agent, method for production thereof, and water-absorbent composition 失效
标题翻译：吸水剂，其制造方法和吸水性组合物
公开(公告)号：US5610208A
公开(公告)日：1997-03-11
申请号：US388838
申请日：1995-02-15
申请人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
发明人： Yorimichi Dairoku , Kinya Nagasuna , Yoshihiko Masuda , Nobuyuki Harada , Yoshihiro Motono , Kunihiko Ishizaki
IPC分类号： A61L15/24 , A61L15/60 , C08J3/24 , C08F8/14
CPC分类号： C08J3/245 , A61L15/24 , A61L15/60 , C08F220/06 , C08J2300/14
摘要： A method for the production of a water-absorbent agent comprises mixing an absorbent resin containing a carboxyl group with an additive soluble in the aqueous solution of at least one member selected from the group consisting of inorganic acids, organic acids, and polyamino acids and a cross-linking agent capable of reacting with the carboxyl group. A water-absorbent agent obtained by adding from 0.005 to 8 parts by weight of an epoxy compound to 100 parts by weight of a water-absorbent resin, exhibiting an absorption capacity without load of at least 45 (g/g), an absorption capacity under load of 20 g/cm.sup.2 of not less than 30 (ml/g) and having a residue amount of an epoxy compound of not more than 2 ppm. A water-absorbent composition comprises a polyamino acid (salt) and a water-absorbent resin containing a carboxyl group.
摘要翻译：制造吸水剂的方法包括将含羧基的吸收性树脂与可溶于选自无机酸，有机酸和聚氨基酸中的至少一种的水溶液中的添加剂混合，以及能够与羧基反应的交联剂。通过将0.005〜8重量份的环氧化合物与100重量份的吸水性树脂相加而获得的吸水剂，其表现出无负载的吸收能力为至少45（g / g），吸收能力负荷为20g / cm 2以下，不低于30（ml / g），残留量不超过2ppm的环氧化合物。吸水性组合物包含聚氨基酸（盐）和含有羧基的吸水性树脂。

9. 发明授权

US06444744B1 Hydrophilic resin, absorbent article, and acrylic acid for polymerization 有权
标题翻译：亲水性树脂，吸收性物品和丙烯酸进行聚合
公开(公告)号：US06444744B1
公开(公告)日：2002-09-03
申请号：US09258503
申请日：1999-02-27
申请人： Hirotama Fujimaru , Kunihiko Ishizaki , Nobuyuki Harada , Sei Nakahara
发明人： Hirotama Fujimaru , Kunihiko Ishizaki , Nobuyuki Harada , Sei Nakahara
IPC分类号： C08F2006
CPC分类号： C08F20/06 , A61L15/24 , A61L15/60 , C08L33/02
摘要： The invention provides a hydrophilic resin and an absorbent article, both of which display still less coloring and discoloring when preserved for a long time. The hydrophilic resin is any one of: 1) a hydrophilic resin, obtained by a process including the step of polymerizing a monomer component including a major proportion of either one or both of acrylic acid and its salt which merely have a content of at most 0.20 ppm in total of hydroquinone and benzoquinone; 2) a hydrophilic resin, comprising a major proportion of an acrylic polymer and a minor proportion of either one or both of hydroquinone and benzoquinone, with the hydrophilic resin further comprising a quinhydronation inhibitor of 10˜1,000,000 times the total weight of hydroquinone and benzoquinone; 3) a hydrophilic resin, comprising a major proportion of an acrylic polymer and merely having a coloring degree (YI) of at most 20 after being left under conditions of the open system, 70° C., 65% RH for 1 week; and 4) a hydrophilic resin, which is a water-absorbent resin and is surface-crosslinked or surface-impregnated with a polyhydric alcohol and displays pH of 5.5 or less in a physiological salt solution and has an absorption capacity of 20 g/g or more for a physiological salt solution under a load of 50 g/cm2. In addition, the absorbent article comprises the above hydrophilic resin.
摘要翻译：本发明提供一种亲水性树脂和吸收性物品，两者在长期保存时都显示出较少的着色和变色。亲水性树脂是以下中的任何一种：1）亲水性树脂，其通过包括以下步骤的方法获得，所述方法包括使仅含有至多0.20的含量的丙烯酸及其盐中的一种或两种以上的主要部分对苯二酚和苯醌总共ppm; 2）亲水性树脂，其中主要部分为丙烯酸类聚合物和少量氢醌和苯醌中的一种或两种，亲水性树脂还含有氢醌和苯醌总重量的10〜1,000,000倍的醌氢醌抑制剂; 3）亲水性树脂，其包含主要部分的丙烯酸类聚合物，并且仅在开放系统的条件下，70℃，65％RH下仅具有至多20的着色度（YI）1周; 和4）作为吸水性树脂的表面交联或表面浸渍多元醇的亲水性树脂，在生理盐溶液中显示出pH5.5以下的吸收能力，吸收容量为20g / g，更多的是在50g / cm 2的负荷下的生理盐溶液。另外，吸收性物品包含上述亲水性树脂。

10. 发明授权

US06187872B1 Water-absorbent agent and method for manufacturing the same 失效
标题翻译：吸水剂及其制造方法
公开(公告)号：US06187872B1
公开(公告)日：2001-02-13
申请号：US09051313
申请日：1998-04-06
申请人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
发明人： Toru Yanase , Kazuki Kimura , Shin-ichi Fujino , Kinya Nagasuna , Kunihiko Ishizaki , Hirotama Fujimaru , Nobuyuki Harada
IPC分类号： C08F812
CPC分类号： A61L15/60 , B01J20/26 , C08F8/00 , C08F8/44 , C08F2800/20 , C08F2810/20 , C08F220/06
摘要： A hydrogel polymer obtained by polymerizing a monomer component including acrylic acid (salt) is post-neutralized so that each of polymer particles derived from a polymer produced by neutralizing the hydrogel polymer has an allowable neutralization ratio. The polymer as obtained by neutralizing the hydrogel polymer is reacted with a crosslinking agent reactive to a functional group of the polymer. The allowable neutralization ratio, for example, is a neutralization ratio which is not lower, by not less than 20 mole percent, or more than, at least 55 mole percent, than an average neutralization ratio of a mass of the polymer particles, and the post-neutralization is carried out so that a number of polymer particles having a non-allowable neutralization ratio outside the allowable neutralization range is not more than 10 in 200 polymer particles, thus obtaining a water-absorbent agent having high absorbency under no applied pressure and high pressure wherein the amount of water soluble component is lower compared with the conventional water-absorbent agent and a change in pH of a swollen gel is small.
摘要翻译：通过使包含丙烯酸（盐）的单体组分聚合而获得的水凝胶聚合物被后中和，使得通过中和水凝胶聚合物产生的聚合物衍生的各聚合物颗粒具有允许的中和比。通过中和水凝胶聚合物获得的聚合物与与聚合物的官能团反应的交联剂反应。例如，容许的中和比例是中和比，其比不到聚合物颗粒的质量的平均中和比不低于20摩尔％，或至多55摩尔％，而且进行中和后，使得在200个聚合物粒子中，许多中和比例不超过允许中和比例的聚合物颗粒数不超过10个，从而获得在无施加压力下具有高吸收性的吸水剂，其中水溶性成分的量与常规吸水剂相比较低，并且溶胀凝胶的pH变化很小。

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