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1. 发明授权

US07968874B2 Organic electroluminescent device material and organic electroluminescent device 有权
标题翻译：有机电致发光器件材料和有机电致发光器件
公开(公告)号：US07968874B2
公开(公告)日：2011-06-28
申请号：US12438304
申请日：2007-08-28
申请人： Hiroshi Miyazaki , Atsuhiko Katayama , Shinji Matsuo , Katsuhide Noguchi
发明人： Hiroshi Miyazaki , Atsuhiko Katayama , Shinji Matsuo , Katsuhide Noguchi
IPC分类号： H01L21/00
CPC分类号： H01L51/0081 , C07F5/069 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/186 , H01L51/0085 , H01L51/5016 , H01L2251/308
摘要： Disclosed is an organic electroluminescent device (organic EL device) that utilizes phosphorescence and is improved in luminous efficiency and fully secured of driving stability. The organic EL device comprises an anode, an organic layer containing a hole-transporting layer, a light-emitting layer, and an electron-transporting layer, and a cathode piled one upon another on a substrate while the hole-transporting layer is disposed between the light-emitting layer and the anode and the electron-transporting layer is disposed between the light-emitting layer and the cathode. The light-emitting layer comprises an aluminum heterocomplex or dimeric complex of deuterated substituted or unsubstituted 2-methyl-8-hydroxyquinoline (Me8HQ-D) in which the hydrogen atoms in the methyl group of substituted or unsubstituted 2-methyl-8-hydroxyquinoline (Me8HQ) are deuterated as a host material and an organic metal complex containing at least one metal selected from groups 7 to 11 of the periodic table as a guest material.
摘要翻译：公开了一种利用磷光的有机电致发光器件（有机EL器件），并提高发光效率并充分确保驱动稳定性。有机EL器件包括阳极，含有空穴传输层的有机层，发光层和电子传输层，以及在衬底上彼此堆叠的阴极，同时空穴传输层位于发光层和阳极以及电子传输层设置在发光层和阴极之间。发光层包括取代或未取代的2-甲基-8-羟基喹啉的甲基中的氢原子的氘代取代或未取代的2-甲基-8-羟基喹啉（Me8HQ-D）的铝异复合物或二聚体复合物（ Me8HQ）作为主体材料氘化，含有选自元素周期表第7至11族的至少一种金属的有机金属络合物作为客体材料。

2. 发明申请

US20100181553A1 ORGANIC ELECTROLUMINESCENT DEVICE MATERIAL AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：有机电致发光器件材料和有机电致发光器件
公开(公告)号：US20100181553A1
公开(公告)日：2010-07-22
申请号：US12438304
申请日：2007-08-28
申请人： Hiroshi Miyazaki , Atsuhiko Katayama , Shinji Matsuo , Katsuhide Noguchi
发明人： Hiroshi Miyazaki , Atsuhiko Katayama , Shinji Matsuo , Katsuhide Noguchi
IPC分类号： H01L51/54 , C07F5/06 , H01L51/52
CPC分类号： H01L51/0081 , C07F5/069 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/186 , H01L51/0085 , H01L51/5016 , H01L2251/308
摘要： Disclosed is an organic electroluminescent device (organic EL device) that utilizes phosphorescence and is improved in luminous efficiency and fully secured of driving stability. The organic EL device comprises an anode, an organic layer containing a hole-transporting layer, a light-emitting layer, and an electron-transporting layer, and a cathode piled one upon another on a substrate while the hole-transporting layer is disposed between the light-emitting layer and the anode and the electron-transporting layer is disposed between the light-emitting layer and the cathode. The light-emitting layer comprises an aluminum heterocomplex or dimeric complex of deuterated substituted or unsubstituted 2-methyl-8-hydroxyquinoline (Me8HQ-D) in which the hydrogen atoms in the methyl group of substituted or unsubstituted 2-methyl-8-hydroxyquinoline (Me8HQ) are deuterated as a host material and an organic metal complex containing at least one metal selected from groups 7 to 11 of the periodic table as a guest material.
摘要翻译：公开了一种利用磷光的有机电致发光器件（有机EL器件），并提高发光效率并充分确保驱动稳定性。有机EL器件包括阳极，含有空穴传输层的有机层，发光层和电子传输层，以及在衬底上彼此堆叠的阴极，同时空穴传输层位于发光层和阳极以及电子传输层设置在发光层和阴极之间。发光层包括取代或未取代的2-甲基-8-羟基喹啉的甲基中的氢原子的氘代取代或未取代的2-甲基-8-羟基喹啉（Me8HQ-D）的铝异复合物或二聚体复合物（ Me8HQ）作为主体材料氘化，含有选自元素周期表第7至11族的至少一种金属的有机金属络合物作为客体材料。

3. 发明申请

US20100148161A1 COMPOUND FOR ORGANIC ELECTROLUMINESCENT DEVICE AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：有机电致发光器件和有机电致发光器件的化合物
公开(公告)号：US20100148161A1
公开(公告)日：2010-06-17
申请号：US12600773
申请日：2008-05-28
申请人： Takahiro Kai , Masaki Komori , Toshihiro Yamamoto , Katsuhide Noguchi , Hiroshi Miyazaki
发明人： Takahiro Kai , Masaki Komori , Toshihiro Yamamoto , Katsuhide Noguchi , Hiroshi Miyazaki
IPC分类号： H01L51/54 , C07D401/04 , C07D403/04 , C07F15/00
CPC分类号： C07D487/04 , C09K11/06 , C09K2211/1029 , C09K2211/185 , H01L51/0052 , H01L51/0058 , H01L51/0067 , H01L51/0072 , H01L51/0085 , H01L51/0087 , H01L51/5012
摘要： Disclosed are an organic electroluminescent device (organic EL device) which is improved in luminous efficiency, fully secured of driving stability, and of simple constitution and a compound useful for the fabrication of said organic EL device. The compound for the organic EL device has an indolocarbazole structure or a structure similar thereto in the molecule wherein an aromatic group is bonded to the nitrogen atom in the indolocarbazole. The organic EL device has a light-emitting layer disposed between an anode and a cathode piled one upon another on a substrate and said light-emitting layer comprises a phosphorescent dopant and the aforementioned compound for an organic electroluminescent device as a host material.
摘要翻译：公开了一种提高发光效率，完全确保驱动稳定性和简单结构的有机电致发光器件（有机EL器件）和用于制造所述有机EL器件的化合物。作为有机EL元件的化合物，在分子中具有吲哚咔唑结构或其结构，其中芳族基团与吲哚咔唑中的氮原子结合。有机EL器件具有设置在基板上彼此堆叠的阳极和阴极之间的发光层，并且所述发光层包含磷光掺杂剂和上述用于有机电致发光器件的化合物作为主体材料。

4. 发明授权

US08013330B2 Compound for organic electroluminescent device and organic electroluminescent device 有权
标题翻译：用于有机电致发光器件和有机电致发光器件的化合物
公开(公告)号：US08013330B2
公开(公告)日：2011-09-06
申请号：US12600781
申请日：2008-05-23
申请人： Masaki Komori , Toshihiro Yamamoto , Takahiro Kai , Katsuhide Noguchi , Hiroshi Miyazaki
发明人： Masaki Komori , Toshihiro Yamamoto , Takahiro Kai , Katsuhide Noguchi , Hiroshi Miyazaki
IPC分类号： H01L35/24 , H01L51/00
CPC分类号： H01L51/0067 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1059 , H01L51/0052 , H01L51/0058 , H01L51/0072 , H01L51/0078 , H01L51/0085 , H01L51/0087 , H01L51/5012 , H05B33/14
摘要： Disclosed are a compound for an organic electroluminescent device (organic EL device) which is improved in luminous efficiency, fully secured of driving stability, and of simple constitution and an organic EL device using said compound. The compound for an organic EL device has two indolocarbazole skeletons each of which is bonded to an aromatic group or two skeletons similar thereto. The organic EL device comprises a light-emitting layer disposed between an anode and a cathode piled one upon another on a substrate and said light-emitting layer comprises a phosphorescent dopant and the aforementioned compound for an organic EL device as a host material.
摘要翻译：公开了一种有机电致发光器件（有机EL器件）的化合物，其发光效率得到改善，完全确保了驱动稳定性，并且构成简单，并且使用了所述化合物的有机EL器件。有机EL元件用化合物具有两个吲哚咔唑骨架，其各自与芳族基团或与其相似的两个骨架结合。有机EL器件包括设置在基板上彼此堆叠的阳极和阴极之间的发光层，并且所述发光层包含磷光掺杂剂和上述用于有机EL器件的化合物作为主体材料。

5. 发明授权

US08008657B2 Compound for organic electroluminescent device and organic electroluminescent device 有权
标题翻译：用于有机电致发光器件和有机电致发光器件的化合物
公开(公告)号：US08008657B2
公开(公告)日：2011-08-30
申请号：US12600773
申请日：2008-05-28
申请人： Takahiro Kai , Masaki Komori , Toshihiro Yamamoto , Katsuhide Noguchi , Hiroshi Miyazaki
发明人： Takahiro Kai , Masaki Komori , Toshihiro Yamamoto , Katsuhide Noguchi , Hiroshi Miyazaki
IPC分类号： H01L35/24
CPC分类号： C07D487/04 , C09K11/06 , C09K2211/1029 , C09K2211/185 , H01L51/0052 , H01L51/0058 , H01L51/0067 , H01L51/0072 , H01L51/0085 , H01L51/0087 , H01L51/5012
摘要： Disclosed are an organic electroluminescent device (organic EL device) which is improved in luminous efficiency, fully secured of driving stability, and of simple constitution and a compound useful for the fabrication of said organic EL device. The compound for the organic EL device has an indolocarbazole structure or a structure similar thereto in the molecule wherein an aromatic group is bonded to the nitrogen atom in the indolocarbazole. The organic EL device has a light-emitting layer disposed between an anode and a cathode piled one upon another on a substrate and said light-emitting layer comprises a phosphorescent dopant and the aforementioned compound for an organic electroluminescent device as a host material.
摘要翻译：公开了一种提高发光效率，完全确保驱动稳定性和简单结构的有机电致发光器件（有机EL器件）和用于制造所述有机EL器件的化合物。作为有机EL元件的化合物，在分子中具有吲哚咔唑结构或其结构，其中芳族基团与吲哚咔唑中的氮原子结合。有机EL器件具有设置在基板上彼此堆叠的阳极和阴极之间的发光层，并且所述发光层包含磷光掺杂剂和上述用于有机电致发光器件的化合物作为主体材料。

6. 发明申请

US20100148162A1 COMPOUND FOR ORGANIC ELECTROLUMINESCENT DEVICE AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：有机电致发光器件和有机电致发光器件的化合物
公开(公告)号：US20100148162A1
公开(公告)日：2010-06-17
申请号：US12600781
申请日：2008-05-23
申请人： Masaki Komori , Toshihiro Yamamoto , Takahiro Kai , Katsuhide Noguchi , Hiroshi Miyazaki
发明人： Masaki Komori , Toshihiro Yamamoto , Takahiro Kai , Katsuhide Noguchi , Hiroshi Miyazaki
IPC分类号： H01L51/54 , C07F15/00 , C07D487/04
CPC分类号： H01L51/0067 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , C09K2211/1059 , H01L51/0052 , H01L51/0058 , H01L51/0072 , H01L51/0078 , H01L51/0085 , H01L51/0087 , H01L51/5012 , H05B33/14
摘要： Disclosed are a compound for an organic electroluminescent device (organic EL device) which is improved in luminous efficiency, fully secured of driving stability, and of simple constitution and an organic EL device using said compound. The compound for an organic EL device has two indolocarbazole skeletons each of which is bonded to an aromatic group or two skeletons similar thereto. The organic EL device comprises a light-emitting layer disposed between an anode and a cathode piled one upon another on a substrate and said light-emitting layer comprises a phosphorescent dopant and the aforementioned compound for an organic EL device as a host material.
摘要翻译：公开了一种有机电致发光器件（有机EL器件）的化合物，其发光效率得到改善，完全确保了驱动稳定性，并且构成简单，并且使用了所述化合物的有机EL器件。有机EL元件用化合物具有两个吲哚咔唑骨架，其各自与芳族基团或与其相似的两个骨架结合。有机EL器件包括设置在基板上彼此堆叠的阳极和阴极之间的发光层，并且所述发光层包含磷光掺杂剂和上述用于有机EL器件的化合物作为主体材料。

7. 发明申请

US20070285008A1 Organic Electroluminescent Element 审中-公开
标题翻译：有机电致发光元件
公开(公告)号：US20070285008A1
公开(公告)日：2007-12-13
申请号：US11660673
申请日：2005-08-15
申请人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
发明人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
IPC分类号： H01J1/63
CPC分类号： H05B33/14 , C09K11/06 , C09K2211/1007 , C09K2211/1029 , C09K2211/1037 , C09K2211/1092 , C09K2211/185 , C09K2211/186 , H01L51/0081 , H01L51/0085 , H01L51/0087 , H01L51/5016
摘要： This invention relates to an organic electroluminescent element (organic EL element) utilizing phosphorescence which shows improved luminous efficiency and driving stability and has a simple structure. The organic EL element comprises an anode, organic layers containing a hole-transporting layer, a light-emitting layer, and an electron-transporting layer, and a cathode piled one upon another on a substrate with the hole-transporting layer disposed between the light-emitting layer and the anode and the electron-transporting layer disposed between the light-emitting layer and the cathode. The light-emitting layer contains a compound represented by the following general formula (I) as a guest material and an organic metal complex containing at least one metal selected from ruthenium, rhodium, palladium, silver, rhenium, osmium, iridium, platinum, and gold as a guest material; in general formula (I), R1-R6 are independently hydrogen atoms, alkyl groups, aralkyl groups, alkenyl groups, cyano groups, alkoxy groups, aromatic hydrocarbon groups, or aromatic heterocyclic groups.
摘要翻译：本发明涉及利用磷光的有机电致发光元件（有机EL元件），其显示出改善的发光效率和驱动稳定性并且具有简单的结构。有机EL元件包括阳极，含有空穴传输层的有机层，发光层和电子传输层，以及在基板上彼此堆叠的阴极，空穴传输层设置在光设置在发光层和阴极之间的阳极和电子传输层。发光层含有作为客体材料的由以下通式（I）表示的化合物和含有选自钌，铑，钯，银，铼，锇，铱，铂的至少一种金属的有机金属络合物和金作为客人材料; 在通式（I）中，R 1 -R 6独立地是氢原子，烷基，芳烷基，烯基，氰基，烷氧基，芳族烃基，或芳族杂环基。

8. 发明申请

US20070054148A1 Aluminum chelate complex for organic el material 审中-公开
标题翻译：铝螯合物用于有机材料
公开(公告)号：US20070054148A1
公开(公告)日：2007-03-08
申请号：US10566725
申请日：2004-08-06
申请人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
发明人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
IPC分类号： H01L51/54 , C09K11/06
CPC分类号： H01L51/0079 , C07F5/069 , C09K11/06 , C09K2211/1029 , C09K2211/186 , H01L51/0052 , H01L51/0059 , H01L51/0062 , H01L51/007 , H01L51/0085 , H01L51/5012 , H05B33/14
摘要： This invention provides an organic EL material useful for the emissive layer of an organic EL element which deteriorates little in luminance when operated over a prolonged period of time and shows excellent durability. The material is an aluminum chelate complex which is represented by general formula (1) in which Ar1 is a mono- or bicylic arylene group, Ar2 is a mono- or bicyclic aryl group, R1—R6 are hydrogen or hydrocarbon groups containing 1-8 carbon atoms and contains a compound represented by general formula (1) in which Ar2 is a halogen as an impurity in an amount of 350 wt ppm or less.
摘要翻译：本发明提供了一种有机EL元件，其有机EL元件的发射层在长时间操作时亮度几乎不变，并表现出优异的耐久性。该材料是由通式（1）表示的铝螯合络合物，其中Ar 1是单 - 或双 - 亚芳基，Ar 2是单 - 或二 - 双环芳基，R 1〜R 6是氢或含有1-8个碳原子的烃基，并且含有通式（1）表示的化合物，其中Ar _{2 是作为杂质的卤素，其量为350重量ppm以下。}

9. 发明申请

US20090130297A1 Organic EL Material, Organic EL Device Using the Same, and Method for Producing Organic EL Device 审中-公开
标题翻译：有机EL材料，使用其的有机EL器件以及生产有机EL器件的方法
公开(公告)号：US20090130297A1
公开(公告)日：2009-05-21
申请号：US11887250
申请日：2006-03-14
申请人： Shinji Matsuo , Hideyuki Furumi , Hiroshi Miyazaki , Kazuo Ishii , Toshinao Yuki , Tsuyoshi Naijo
发明人： Shinji Matsuo , Hideyuki Furumi , Hiroshi Miyazaki , Kazuo Ishii , Toshinao Yuki , Tsuyoshi Naijo
IPC分类号： B05D5/12
CPC分类号： C07D215/30 , C07F5/069 , C09K11/06 , C09K2211/186 , C23C14/12 , H01L51/001 , H01L51/0025 , H01L51/0081 , H01L51/0084 , H01L51/0085 , H01L51/5012 , H05B33/14
摘要： Disclosed are an aluminum chelate complex capable of stabilizing the degree of vacuum in a film-forming chamber in the vapor deposition step and producing efficiently a high-quality organic EL device which shows excellent reliability and durability in practical use and an organic EL device using the said aluminum chelate complex. The aluminum chelate complex useful as an organic EL material is represented by L1Al(L2)2, contains 0.6 mol % or less of a complex represented by Al(L2)3, and is obtained by reacting an aluminum alkoxide with a quinolinol derivative and then with a phenolic compound and purifying the resulting complex to a high degree. In the formulas, L1 denotes a phenolate ligand and L2 denotes a substituted quinolinolate ligand.
摘要翻译：公开了能够在气相沉积步骤中稳定成膜室中的真空度的铝螯合络合物，并且有效地生产在实际应用中显示出优异的可靠性和耐久性的高品质有机EL器件以及使用说铝螯合物。可用作有机EL材料的铝螯合物由L1Al（L2）2表示，含有0.6mol％以下的由Al（L2）3表示的络合物，通过使烷氧基铝与羟基喹啉衍生物反应而得到，与酚类化合物，并高度纯化所得的络合物。在该式中，L1表示酚盐配体，L2表示取代的羟基喹啉配体。

10. 发明授权

US08263770B2 Aluminum chelate complex for organic EL material 有权
标题翻译：铝螯合物用于有机EL材料
公开(公告)号：US08263770B2
公开(公告)日：2012-09-11
申请号：US12820336
申请日：2010-06-22
申请人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
发明人： Shinji Matsuo , Hiroshi Miyazaki , Taishi Tsuji
IPC分类号： C07F5/06 , C07D215/30
CPC分类号： H01L51/0079 , C07F5/069 , C09K11/06 , C09K2211/1029 , C09K2211/186 , H01L51/0052 , H01L51/0059 , H01L51/0062 , H01L51/007 , H01L51/0085 , H01L51/5012 , H05B33/14
摘要： This invention provides an organic EL material useful for the emissive layer of an organic EL element which deteriorates little in luminance when operated over a prolonged period of time and shows excellent durability. The material is an aluminum chelate complex which is represented by general formula (1) in which Ar1 is a mono- or bicylic arylene group, Ar2 is a mono- or bicyclic aryl group, R1-R6 are hydrogen or hydrocarbon groups containing 1-8 carbon atoms and contains a compound represented by general formula (1) in which Ar2 is a halogen as an impurity in an amount of 350 wt ppm or less.
摘要翻译：本发明提供了一种有机EL元件，其有机EL元件的发射层在长时间操作时亮度几乎不变，并表现出优异的耐久性。该材料是由通式（1）表示的铝螯合络合物，其中Ar 1是单或双环亚芳基，Ar 2是单或双环芳基，R 1 -R 6是氢或含1-8的烃基并且含有通式（1）表示的化合物，其中Ar 2是作为杂质的卤素，其量为350重量ppm以下。

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