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1. 发明授权

US07425583B2 Ion exchanger 有权
公开(公告)号：US07425583B2
公开(公告)日：2008-09-16
申请号：US11301122
申请日：2005-12-12
申请人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
发明人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
IPC分类号： C08J5/20
CPC分类号： B01J47/08 , B01D61/48 , B01J20/28033 , B01J20/28054 , B01J20/28069 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J39/26 , B01J41/20 , B01J47/014 , B01J2220/52 , C02F1/42 , C02F1/469
摘要： A porous ion exchanger includes an open cell structure including interconnected macropores and mesopores whose average diameter is in a range of 1 to 1000 μm existing on walls of the macropores. Moreover, a total pore volume is in a range of 1 to 50 ml/g, ion exchange groups are uniformly distributed, and an ion exchange capacity is not less than 0.5 mg equivalent/g of dry porous ion exchanger. The porous ion exchanger can be used as an ion exchanger filled into a deionization module of an electrodeionization water purification device, solid acid catalyst, adsorbent, and filler for chromatography.

2. 发明申请

US20070175329A1 Chemical filter 审中-公开
标题翻译：化学过滤器
公开(公告)号：US20070175329A1
公开(公告)日：2007-08-02
申请号：US10553871
申请日：2004-04-22
申请人： Hiroshi Inoue , Koji Yamanaka , Akiko Yoshida , Kazuhiko Kawada , Yukiko Toriyama
发明人： Hiroshi Inoue , Koji Yamanaka , Akiko Yoshida , Kazuhiko Kawada , Yukiko Toriyama
IPC分类号： B01D53/02
CPC分类号： B01D53/02 , B01D2253/20 , B01D2253/206 , B01D2253/306 , B01D2253/308 , B01D2253/311 , B01D2256/26 , B01D2258/0216 , B01D2259/4533 , B01J20/28054 , B01J20/28083 , B01J20/28085 , B01J39/18 , B01J41/12
摘要： A chemical filter, characterized in that it uses, as an adsorption layer, an organic porous ion exchanger which has an open pore structure wherein a meso pore having an average diameter of 5 to 1,000 μm is formed in the wall between a macro pore and a macro pore connected with each other, has a total pore volume of 1 to 50 ml/g, has ion-exchange groups being uniformly distributed, and has an ion-exchange capacity of 3.0 mg equivalent/g-dry porous material or more. The chemical filter can maintain the capacity of adsorbing and removing a gaseous contaminant even at an enhanced gas transmission rate, and can remove also a trace amount of a gaseous contaminant.
摘要翻译：一种化学过滤器，其特征在于，其使用具有开孔结构的有机多孔离子交换剂作为吸附层，其中在大孔和微孔之间的壁中形成平均直径为5至1,000μm的中孔大孔相互连接，总孔体积为1〜50ml / g，离子交换基团均匀分布，离子交换容量为3.0mg当量/ g-干多孔材料以上。化学过滤器即使在增强的气体传输速率下也能保持吸附和除去气态污染物的能力，并且还可以除去微量的气态污染物。

3. 发明授权

US07078441B2 Organic porous material, process for manufacturing the same, and organic porous ion exchanger 有权
公开(公告)号：US07078441B2
公开(公告)日：2006-07-18
申请号：US10929523
申请日：2004-08-31
申请人： Hiroshi Inoue , Koji Yamanaka
发明人： Hiroshi Inoue , Koji Yamanaka
IPC分类号： C08J9/28
CPC分类号： B01J20/28085 , B01J20/28014 , B01J20/28069 , B01J20/28076 , B01J20/28078 , B01J20/28083 , B01J20/28092 , B01J39/20 , B01J41/14
摘要： An organic porous material having a continuous pore structure, which comprises interconnected macropores and mesopores with a radius of 0.01 to 100 μm in the walls of the macropores, having a total pore volume of 1 to 50 ml/g and having pore distribution curve characteristics wherein the value obtained by dividing the half-width of the pore distribution curve at the main peak by the radius at the main peak is 0.5 or less. The organic porous material is useful as an adsorbent having high physical strength and excelling in adsorption amount and adsorption speed, an ion exchanger excelling in durability against swelling and shrinkage, and a filler for chromatography exhibiting high separation capability.

4. 发明申请

US20060154997A1 Ion exchanger 有权
公开(公告)号：US20060154997A1
公开(公告)日：2006-07-13
申请号：US11301122
申请日：2005-12-12
申请人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
发明人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
IPC分类号： C08J5/20
CPC分类号： B01J47/08 , B01D61/48 , B01J20/28033 , B01J20/28054 , B01J20/28069 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J39/26 , B01J41/20 , B01J47/014 , B01J2220/52 , C02F1/42 , C02F1/469
摘要： A porous ion exchanger includes an open cell structure including interconnected macropores and mesopores whose average diameter is in a range of 1 to 1000 μm existing on walls of the macropores. Moreover, a total pore volume is in a range of 1 to 50 ml/g, ion exchange groups are uniformly distributed, and an ion exchange capacity is not less than 0.5 mg equivalent/g of dry porous ion exchanger. The porous ion exchanger can be used as an ion exchanger filled into a deionization module of an electrodeionization water purification device, solid acid catalyst, adsorbent, and filler for chromatography.

5. 发明授权

US07393445B2 Ion exchanger 有权
标题翻译：离子交换器
公开(公告)号：US07393445B2
公开(公告)日：2008-07-01
申请号：US11299586
申请日：2005-12-12
申请人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
发明人： Hiroshi Inoue , Koji Yamanaka , Makio Tamura , Shusaku Yoshida , Hideo Nakamura
IPC分类号： B01D61/48
CPC分类号： B01J47/08 , B01D61/48 , B01J20/28033 , B01J20/28054 , B01J20/28069 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J39/26 , B01J41/20 , B01J47/014 , B01J2220/52 , C02F1/42 , C02F1/469
摘要： A porous ion exchanger includes an open cell structure including interconnected macropores and mesopores whose average diameter is in a range of 1 to 1000 μm existing on walls of the macropores. Moreover, a total pore volume is in a range of 1 to 50 ml/g, ion exchange groups are uniformly distributed, and an ion exchange capacity is not less than 0.5 mg equivalent/g of dry porous ion exchanger. The porous ion exchanger can be used as an ion exchanger filled into a deionization module of an electrodeionization water purification device, solid acid catalyst, adsorbent, and filler for chromatography.
摘要翻译：多孔离子交换器包括开孔结构，其包含互连的大孔和介孔，其平均直径在大孔壁上存在1〜1000μm的范围。此外，总孔体积在1〜50ml / g的范围内，离子交换基团均匀分布，离子交换容量不小于0.5mg当量/ g干式多孔离子交换剂。多孔离子交换剂可用作填充在电去离子水净化装置，固体酸催化剂，吸附剂和色谱填料的去离子模块中的离子交换剂。

6. 发明授权

US07119164B2 Method for preparing sulfonated organic porous material 失效
标题翻译：磺化有机多孔材料的制备方法
公开(公告)号：US07119164B2
公开(公告)日：2006-10-10
申请号：US10651951
申请日：2003-09-02
申请人： Hiroshi Inoue , Koji Yamanaka , Akiko Yoshida , Yusaku Suenaga
发明人： Hiroshi Inoue , Koji Yamanaka , Akiko Yoshida , Yusaku Suenaga
IPC分类号： C08F12/08 , C08F8/36
CPC分类号： B01J20/265 , B01J20/26 , B01J20/321 , B01J20/3251 , B01J39/20 , C08F8/36 , C08F2800/10 , C08F2800/20 , C08F212/08
摘要： A sulfonated organic porous material in which at least 0.5 mg-equivalent/g (on a dry basis) of sulfonic acid groups has been introduced can be obtained by causing a gaseous substance containing sulfuric anhydride to come in contact with an organic porous material having mesopores existing on the walls of interconnected macropores and having a median radius of 0.01–100 μm and a total pore volume of 1–50 ml/g. This preparation method can ensure the introduction of a large amount of sulfonic acid groups into an organic porous material in a short period of time.
摘要翻译：可以通过使含有硫酸酐的气态物质与具有中孔的有机多孔材料接触而获得至少0.5mg当量/ g（基于干基）的磺酸基团）的磺化有机多孔材料存在于相互连接的大孔的壁上，中间半径为0.01-100μm，总孔体积为1-50ml / g。该制备方法可以确保在短时间内将大量的磺酸基团引入有机多孔材料中。

7. 发明申请

US20080308482A1 Electric Deionized Water Production Apparatus 有权
标题翻译：电去离子水生产设备
公开(公告)号：US20080308482A1
公开(公告)日：2008-12-18
申请号：US11994506
申请日：2005-07-20
申请人： Naoyuki Tajima , Koji Yamanaka , Hiroshi Inoue , Akira Nakamura
发明人： Naoyuki Tajima , Koji Yamanaka , Hiroshi Inoue , Akira Nakamura
IPC分类号： C02F1/469
CPC分类号： B01J20/28042 , B01D61/48 , B01D61/485 , B01J47/018 , B01J47/08 , C02F1/441 , C02F1/4695 , C02F5/00 , C02F2201/4611 , C02F2201/46115 , C02F2201/4617
摘要： An electric deionized water production apparatus in which a direct current field is applied to a deionizing chamber packed with an ion-exchange material such that ions to be discharged are allowed to migrate in the direction identical or opposite to the direction of the water flow in the ion-exchange material, whereby ionic impurities adsorbed in the ion-exchange material are discharged from the system, the ion-exchange material being a mixture of a monolith-shaped organic porous ion-exchange material and ion-exchange resin particles. The electric deionized water production apparatus has a simple structure that can reduce material cost, process cost, and assembly cost, capable of accelerating migration of the adsorbed ionic impurities to facilitate discharge of the adsorbed ions and free from a deflected flow due to swelling or shrinkage accompanying an ion-exchanging reaction, and from poor contact with an ion-exchange membrane.
摘要翻译：一种电去离子水生产装置，其中直流电场施加到装有离子交换材料的去离子室，使得排出的离子允许沿与水流中的水流方向相同或相反的方向迁移离子交换材料，其中吸附在离子交换材料中的离子杂质从系统中排出，离子交换材料是整料形有机多孔离子交换材料和离子交换树脂颗粒的混合物。电去离子水生产设备具有简单的结构，其可以降低材料成本，工艺成本和组装成本，能够加速吸附的离子杂质的迁移，以促进吸附的离子的排出并且由于膨胀或收缩而没有偏转的流动伴随着离子交换反应，并且与离子交换膜接触不良。

8. 发明授权

US07294265B2 Ion adsorption module and method for water treatment 有权
标题翻译：离子吸附模块及水处理方法
公开(公告)号：US07294265B2
公开(公告)日：2007-11-13
申请号：US10510964
申请日：2003-04-14
申请人： Akiko Yoshida , Koji Yamanaka , Hiroshi Inoue
发明人： Akiko Yoshida , Koji Yamanaka , Hiroshi Inoue
IPC分类号： B01D24/00
CPC分类号： B01J20/28083 , B01J20/28054 , B01J20/28085 , B01J39/20 , B01J41/14 , B01J47/00 , B01J47/028 , C02F1/42 , C02F2001/422 , C02F2001/425
摘要： An ion adsorption module comprises a container with at least an opening into which feed water flows, and an organic porous ion exchange material having a three-dimensional reticular structure filled into the container, which has a continuous pore structure comprising macropores and mesopores, the macropores being interconnected with each other forming mesopores with an average diameter of 1-1,000 μm in the interconnected parts, has a total pore volume of 1-50 ml/g, contains uniformly distributed ion exchange groups, and has an ion exchange capacity of 0.5 mg equivalent/g or more of the porous material on a dry basis. The ion adsorption module can be extremely easily filled with the ion exchange material, and the packed layer does not move even if the layer is placed in an upward flow. The ion adsorption module and the water processing method using the ion exchange material are extremely useful.
摘要翻译：离子吸附模块包括至少具有进料水流过的开口的容器和填充到容器中的具有三维网状结构的有机多孔离子交换材料，其具有包含大孔和介孔的连续孔结构，大孔彼此相互连接，在相互连接的部分中形成平均直径为1-1000μm的介孔，总孔体积为1-50ml / g，含有均匀分布的离子交换基团，离子交换容量为0.5mg 基于干燥的当量/ g或更多的多孔材料。离子吸附模块可以非常容易地用离子交换材料填充，并且即使层被放置在向上的流中，填充层也不会移动。离子吸附模块和使用离子交换材料的水处理方法是非常有用的。

9. 发明授权

US07201832B2 Electrodeionization deionized water producing apparatus 失效
标题翻译：电离去离子水生产设备
公开(公告)号：US07201832B2
公开(公告)日：2007-04-10
申请号：US10422772
申请日：2003-04-25
申请人： Koji Yamanaka , Hiroshi Inoue , Naoyuki Tajima
发明人： Koji Yamanaka , Hiroshi Inoue , Naoyuki Tajima
IPC分类号： B01D61/48
CPC分类号： C02F1/4695 , B01D61/44 , B01J47/028 , B01J47/08 , C02F1/42 , C02F1/4604 , C02F1/4696 , C02F2001/46133 , C02F2103/04 , C02F2201/4611 , C02F2201/46115 , C02F2201/46125
摘要： In the electrodeionization deionized water producing apparatus, water is passed through a deionizing chamber(s) packed with an organic porous ion exchange material having a three-dimensional network structure to remove ionic impurities in the water, thereby producing deionized water. At the same time, a DC electric field is applied to the deionizing chamber(s) to discharge ionic impurities adsorbed on the organic porous ion exchange material outside the system, wherein the DC electric field is applied so that the ions to be discharged may electrophoretically move in the direction reverse to the flow of water through the organic porous ion exchange material.
摘要翻译：在电去离子去离子水生成装置中，使水通过填充有具有三维网状结构的有机多孔离子交换材料的去离子室，以去除水中的离子杂质，从而产生去离子水。同时，将DC电场施加到去离子室以排出吸附在系统外部的有机多孔离子交换材料上的离子杂质，其中施加DC电场使得待排出的离子可以电泳沿着与有机多孔离子交换材料的水流相反的方向移动。

10. 发明申请

US20060254969A1 Column for ion chromatograph, suppressor and ion chromatograph 审中-公开
标题翻译：离子色谱柱，抑制离子色谱柱
公开(公告)号：US20060254969A1
公开(公告)日：2006-11-16
申请号：US10543819
申请日：2004-01-28
申请人： Koji Yamanaka , Hiroshi Inoue , Akiko Yoshida , Masashi Fujita
发明人： Koji Yamanaka , Hiroshi Inoue , Akiko Yoshida , Masashi Fujita
IPC分类号： B01D15/08
CPC分类号： B01J20/28083 , B01D15/361 , B01J20/28054 , B01J20/28085 , B01J20/28088 , B01J39/26 , B01J41/20 , G01N30/96 , G01N2030/525 , G01N2030/965
摘要： A separation column for ion chromatograph, which is packed with an organic porous ion exchanger having a three-dimensionally network structure which has a continuous pore structure comprising macropores connected with each other and, being present in the wall between them, a mesopore having a radius of 0.01 to 50 μm, has a total pore volume of 1 to 50 ml/g, exhibits a value obtained by dividing the half width of the main peak of the pore distribution curve thereof by the radius of the peak top of the main peak of 0.5 or less, and has ion exchange groups introduced so that the exchanger has an ion-exchange capacity of 0.1 to 5000 μg equivalent/g-dry organic porous ion exchanger. The separation column exhibits high performance capability especially for the separation and concentration of low molecular weight ions, and thus can be used for passing a sample solution through it with a reduced pressure while retaining a high capability for ion resolution.
摘要翻译：一种用于离子色谱的分离柱，其中填充有具有三维网状结构的有机多孔离子交换器，该有机多孔离子交换器具有连续的孔结构，其包含彼此连接的大孔，并且存在于它们之间的壁中，具有半径为0.01〜50μm，总孔体积为1〜50ml / g，通过将其孔分布曲线的主峰的半值宽度除以主峰顶峰的半径得到的值 0.5以下，并且具有导入的离子交换基团，使得交换器的离子交换容量为0.1〜5000mug当量/ g干燥有机多孔离子交换剂。分离柱表现出高性能特性，特别是分离和浓缩低分子量离子，因此可用于使样品溶液以较低的压力通过，同时保持高的离子分辨能力。

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