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1. 发明授权

US5672723A Process for preparation of 1-acyl-2-substituted hydrazines 失效
标题翻译： 1-酰基-2-取代肼的制备方法
公开(公告)号：US5672723A
公开(公告)日：1997-09-30
申请号：US604679
申请日：1996-02-21
申请人： Hiroki Hotta , Hiroyasu Sugizaki , Tetsuya Toya , Mikio Yanagi
发明人： Hiroki Hotta , Hiroyasu Sugizaki , Tetsuya Toya , Mikio Yanagi
IPC分类号： C07C241/04 , C07C243/38 , C07D311/58 , C07D311/04 , C07C241/02
CPC分类号： C07D311/58 , C07C241/04 , Y02P20/582
摘要： The present invention can provide a process for the preparation of an 1-acyl-2-substituted hydrazine compound from a mixture containing the 1-acyl-2-substituted hydrazine and an 1-acyl-1-substituted hydrazine by selective hydrolysis or alcoholysis of the 1-acyl-yl-1-substituted hydrazine in the presence of an acid catalyst, and by separation of the resulting carboxylic acid and derivative thereof. The 1-acyl-2-alkyl hydrazine obtained has a high purity.
摘要翻译：本发明可以提供从含有1-酰基-2-取代的肼和1-酰基-1-取代的肼的混合物中通过选择性水解或醇解来制备1-酰基-2-取代的肼化合物的方法 1-酰基 - 取代的肼在酸催化剂的存在下，分离得到的羧酸及其衍生物。所得的1-酰基-2-烷基肼具有高纯度。

2. 发明授权

US5530021A Hydrazine derivative and pesticidal composition comprising said derivative as an effective ingredient 失效
标题翻译：肼衍生物和包含所述衍生物作为有效成分的农药组合物
公开(公告)号：US5530021A
公开(公告)日：1996-06-25
申请号：US308643
申请日：1994-09-19
申请人： Mikio Yanagi , Hiroyasu Sugizaki , Tetsuya Toya , Yasuhito Kato , Hidetoshi Shirakura , Tetsuo Watanabe , Yoshimi Yajima , Seiichirou Kodama , Akio Masui , Toshiaki Yanai , Yoshihisa Tsukamoto , Yoshihiro Sawada , Shinji Yokoi
发明人： Mikio Yanagi , Hiroyasu Sugizaki , Tetsuya Toya , Yasuhito Kato , Hidetoshi Shirakura , Tetsuo Watanabe , Yoshimi Yajima , Seiichirou Kodama , Akio Masui , Toshiaki Yanai , Yoshihisa Tsukamoto , Yoshihiro Sawada , Shinji Yokoi
IPC分类号： A01N43/16 , A01N43/18 , A01N43/24 , A01N43/32 , A01N43/42 , A01N43/46 , A01N43/60 , A01N43/62 , A01N43/72 , A01N43/84 , A01P7/04 , C07D223/16 , C07D241/42 , C07D241/44 , C07D243/12 , C07D265/36 , C07D267/14 , C07D279/16 , C07D281/10 , C07D311/12 , C07D311/22 , C07D311/58 , C07D311/68 , C07D313/08 , C07D319/16 , C07D319/18 , C07D319/20 , C07D321/10 , C07D327/06 , C07D335/06 , C07D337/08 , C07D339/00 , C07D339/08 , C07D493/10 , C07F7/18
CPC分类号： C07D493/10 , A01N43/16 , A01N43/24 , A01N43/32 , A01N43/84 , C07D265/36 , C07D311/22 , C07D311/58 , C07D311/68 , C07D319/18 , C07D319/20 , C07D321/10 , C07D327/06 , C07F7/1844
摘要： A novel hydrazine derivative and a pesticidal composition containing the hydrazine derivative as the effecting ingredient. The hydrazine derivative show high pesticidal activity against harmful pests which are resistant to known pesticides such as organophosphorus pesticides, pyrethroids, etc., especially against Lepidoptera harmful pests such as Plutella xylostella, Spodoptera litura, Cnaphalocrocis medinalis, Adoxophyes orana, etc., and is effective for controlling harmful pests in paddy field, upland field, orchard, forest or places to be kept environmentally hygienic.
摘要翻译：一种新颖的肼衍生物和含有肼衍生物作为有效成分的农药组合物。肼衍生物对杀虫剂具有很强的杀虫活性，对有机磷杀虫剂，拟除虫菊酯等已知的农药具有抗性，特别是针对鳞翅目有害害虫如小菜蛾（Plutella xylostella），斜纹夜蛾（Spodoptera litura），Cnaphalocrocis medinalis，Adoxophyes orana等，有效控制水田，旱田，果园，森林或环境卫生的有害害虫。

3. 发明授权

US5378726A New hydrazine derivative and pesticidal composition comprising said derivative as an effective ingredient 失效
标题翻译：包含所述衍生物作为有效成分的新肼衍生物和杀虫组合物
公开(公告)号：US5378726A
公开(公告)日：1995-01-03
申请号：US152877
申请日：1993-11-15
申请人： Mikio Yanagi , Hiroyasu Sugizaki , Tetsuya Toya , Yasuhito Kato , Hidetoshi Shirakura , Tetsuo Watanabe , Yoshimi Yajima , Seiichirou Kodama , Akio Masui , Toshiaki Yanai , Yoshihisa Tsukamoto , Yoshihiro Sawada , Shinji Yokoi
发明人： Mikio Yanagi , Hiroyasu Sugizaki , Tetsuya Toya , Yasuhito Kato , Hidetoshi Shirakura , Tetsuo Watanabe , Yoshimi Yajima , Seiichirou Kodama , Akio Masui , Toshiaki Yanai , Yoshihisa Tsukamoto , Yoshihiro Sawada , Shinji Yokoi
IPC分类号： A01N43/16 , A01N43/18 , A01N43/24 , A01N43/32 , A01N43/42 , A01N43/46 , A01N43/60 , A01N43/62 , A01N43/72 , A01N43/84 , A01P7/04 , C07D223/16 , C07D241/42 , C07D241/44 , C07D243/12 , C07D265/36 , C07D267/14 , C07D279/16 , C07D281/10 , C07D311/12 , C07D311/22 , C07D311/58 , C07D311/68 , C07D313/08 , C07D319/16 , C07D319/18 , C07D319/20 , C07D321/10 , C07D327/06 , C07D335/06 , C07D337/08 , C07D339/00 , C07D339/08 , C07D493/10 , C07F7/18
CPC分类号： C07D493/10 , A01N43/16 , A01N43/24 , A01N43/32 , A01N43/84 , C07D265/36 , C07D311/22 , C07D311/58 , C07D311/68 , C07D319/18 , C07D319/20 , C07D321/10 , C07D327/06 , C07F7/1844
摘要： A novel hydrazine derivative and a pesticidal composition containing the hydrazine derivative as the effecting ingredient. The hydrazine derivative show high pesticidal activity against harmful pests which are resistant to known pesticides such as organophosphorus pesticides, pyrethroids, etc., especially against Lepidopters harmful pests such as Plutella xylostella, Spodoptera litura, Cnaphalocrocis medinalis, Adoxophyes orana, etc., and is effective for controlling harmful pests in paddy field, upland field, orchard, forest or places to be kept environmentally hygienic.
摘要翻译：一种新颖的肼衍生物和含有肼衍生物作为有效成分的农药组合物。肼衍生物对杀虫剂具有较高的杀虫活性，对有机磷杀虫剂，拟除虫菊酯等已知的农药具有抗性，特别是针对小菜蛾，斜纹夜蛾，白僵菌，Adoxophyes orana等对鳞翅目害虫有害害虫的杀虫活性，有效控制水田，旱田，果园，森林或环境卫生的有害害虫。

4. 发明申请

US20090270459A1 Flea control agent containing N-Substituted indole derivative 审中-公开
标题翻译：含有N-取代吲哚衍生物的跳蚤控制剂
公开(公告)号：US20090270459A1
公开(公告)日：2009-10-29
申请号：US12456823
申请日：2009-06-22
申请人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
发明人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
IPC分类号： A01N43/38 , A01N43/40 , A01P7/04
CPC分类号： A01N43/38 , A01N43/40
摘要： Conventional control agents against fleas parasitic on animals do not have sufficient selective toxicity and are hence not safe for the animals to which the control agents are applied. The control agents are not always satisfactory also in control effect and quick-acting properties. Intensive studies were made on the insecticidal activity of N-substituted indole compounds against fleas and on the safety thereof for mammals including pets. As a result, it was found that an N-substituted indole derivative, e.g., 1-(3-chloro-5-trifluoromethylpyridin 2-yl)-3-(dichlorofluoromethylthio)indole, 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(dichlorofluoromethylthio)-indole, or 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(trifluoromethylthio)indole, has high insecticidal activity and quick-acting properties and is lowly toxic to mammals including pets.
摘要翻译：防止寄生在动物上的跳蚤的传统控制剂不具有足够的选择性毒性，因此对于施用控制剂的动物是不安全的。在控制效果和速效特性方面，控制剂并不总是令人满意。对N-取代吲哚化合物对跳蚤的杀虫活性及其对哺乳动物（包括宠物）的安全性进行了深入研究。结果发现，N-取代的吲哚衍生物，例如1-（3-氯-5-三氟甲基吡啶-2-基）-3-（二氯氟甲硫基）吲哚，1-（2,6-二氯-4- 三氟甲基苯基）-3-（二氯氟甲硫基） - 吲哚或1-（2,6-二氯-4-三氟甲基苯基）-3-（三氟甲硫基）吲哚具有很高的杀虫活性和速效性，对包括宠物在内的哺乳动物具有低毒性。

5. 发明申请

US20100056601A1 Control agent containing N-Substituted indole derivative for acarian parasitic on animal 审中-公开
标题翻译：含有N-取代吲哚衍生物的控制剂用于动物的寄生虫
公开(公告)号：US20100056601A1
公开(公告)日：2010-03-04
申请号：US12590367
申请日：2009-11-06
申请人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
发明人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
IPC分类号： A61K31/404
CPC分类号： A01N47/02 , A01N43/38 , A01N43/40
摘要： Conventional control agents against acarians parasitic on animals do not have sufficient selective toxicity and are hence not safe for the animals to which the control agents are applied. The control agents are not always satisfactory also in control effect and quick-acting properties. Intensive studies were made on the insecticidal activity of N-substituted indole compounds against acarians and on the safety thereof for mammals including pets. As a result, it was found that an N-substituted indole derivative, e.g., 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(trifluoromethylthio)indole, or 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(dichlorofluoromethylthio)indole, has high insecticidal activity and quick-acting properties and is lowly toxic to mammals including pets.
摘要翻译：对动物寄生寄生虫的传统控制剂不具有足够的选择性毒性，因此对施用对照剂的动物来说是不安全的。在控制效果和速效特性方面，控制剂并不总是令人满意。对N-取代吲哚化合物对猕猴桃的杀虫活性及其对哺乳动物（包括宠物）的安全性进行了深入研究。结果发现，N-取代的吲哚衍生物，例如1-（2,6-二氯-4-三氟甲基苯基）-3-（三氟甲硫基）吲哚或1-（2,6-二氯-4- 三氟甲基苯基）-3-（二氯氟甲硫基）吲哚，具有高杀虫活性和速效性，对包括宠物在内的哺乳动物具有低毒性。

6. 发明申请

US20070197578A1 Control agent containing n-substituted indole derivative for acarian parasitic on animal 审中-公开
标题翻译：含有对取代吲哚衍生物的控制剂用于动物的寄生虫
公开(公告)号：US20070197578A1
公开(公告)日：2007-08-23
申请号：US10593920
申请日：2004-04-22
申请人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
发明人： Satoshi Tanabe , Hiroki Hotta , Tetsuya Toya , Katsuhiko Hosoda
IPC分类号： A61K31/44
CPC分类号： A01N47/02 , A01N43/38 , A01N43/40
摘要： Conventional control agents against acarians parasitic on animals do not have sufficient selective toxicity and are hence not safe for the animals to which the control agents are applied. The control agents are not always satisfactory also in control effect and quick-acting properties. Intensive studies were made on the insecticidal activity of N-substituted indole compounds against acarians and on the safety thereof for mammals including pets. As a result, it was found that an N-substituted indole derivative, e.g., 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(trifuloromethylthio)indole, or 1-(2,6-dichloro-4-trifluoromethylphenyl)-3-(dichlo-rofluoromethylthio)indole, has high insecticidal activity and quick-acting properties and is lowly toxic to mammals including pets.
摘要翻译：对动物寄生寄生虫的传统控制剂不具有足够的选择性毒性，因此对施用对照剂的动物来说是不安全的。在控制效果和速效特性方面，控制剂并不总是令人满意。对N-取代吲哚化合物对猕猴桃的杀虫活性及其对哺乳动物（包括宠物）的安全性进行了深入研究。结果发现，N-取代的吲哚衍生物，例如1-（2,6-二氯-4-三氟甲基苯基）-3-（三氟甲硫基）吲哚或1-（2,6-二氯-4- 三氟甲基苯基）-3-（二氯 - 氟甲硫基）吲哚，具有很高的杀虫活性和速效性，对包括宠物在内的哺乳动物具有低毒性。

7. 发明授权

US06271418B1 Process for preparing (hetero) aromatic substituted benzene derivatives 失效
公开(公告)号：US06271418B1
公开(公告)日：2001-08-07
申请号：US09512151
申请日：2000-02-22
申请人： Tetsuya Toya , Hidetoshi Shirakura , Junichi Kon
发明人： Tetsuya Toya , Hidetoshi Shirakura , Junichi Kon
IPC分类号： C07C21100
CPC分类号： C07D213/55 , C07C67/307 , C07C67/317 , C07C2601/16 , C07C69/753 , C07C69/76
摘要： Three processes are described for preparing (hetero)aromatic substituted benzene derivatives which comprise aromatization of cyclohexenone derivatives via (chloro)cyclohexadiene derivatives.

8. 发明授权

US06340772B1 Process for preparing (hetero) aromatic substituted benzene derivatives 有权
公开(公告)号：US06340772B1
公开(公告)日：2002-01-22
申请号：US09841313
申请日：2001-04-24
申请人： Tetsuya Toya , Hidetoshi Shirakura , Junichi Kon
发明人： Tetsuya Toya , Hidetoshi Shirakura , Junichi Kon
IPC分类号： C07C21100
摘要： Three processes are described for preparing (hetero)aromatic substituted benzene derivatives which comprise aromatization of cyclohexenone derivatives via (chloro)cyclohexadiene derivatives.

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