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1. 发明授权

US4533382A Device and method for making and collecting fine metallic powder 失效
标题翻译：制造和收集细金属粉末的装置和方法
公开(公告)号：US4533382A
公开(公告)日：1985-08-06
申请号：US608112
申请日：1984-05-08
申请人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
IPC分类号： B22F9/12 , B22F9/00
CPC分类号： B22F9/12
摘要： Fine powder of a metal is made by vaporizing the metal in a vaporization chamber, mixing the metallic vapor with an inert carrier gas, and then adiabatically expanding the mixture through a nozzle, which preferably is a convergent-divergent nozzle. A jet flow from the nozzle is very rapidly cooled by this adiabatic expansion, which quickly condenses the metal vapor in the jet flow into very fine particles. Optionally the jet flow is directed against a metal powder collecting means, which may be a collection plate, but preferably is a bath of oil which entrains the particles and keeps them from agglomerating together by partially neutralizing their surface activity. Thus fine metal powder with particle diameters of the order of a few hundreds of angstroms can be economically produced.
摘要翻译：通过在蒸发室中蒸发金属，将金属蒸气与惰性载气混合，然后通过优选为收敛扩散喷嘴的喷嘴绝热地使混合物膨胀而制成金属细粉末。来自喷嘴的射流通过这种绝热膨胀非常快速地冷却，这使得喷射流中的金属蒸气迅速冷凝成非常细的颗粒。任选地，喷射流被引向金属粉末收集装置，金属粉末收集装置可以是收集板，但是优选地是一种油的浴，其夹带颗粒并通过部分中和它们的表面活性使它们不凝聚在一起。因此，可以经济地制造粒径为几百埃的细金属粉末。

2. 发明授权

US4594101A Fine composite powder material and method and apparatus for making the same 失效
标题翻译：精细复合粉末材料及其制造方法和装置
公开(公告)号：US4594101A
公开(公告)日：1986-06-10
申请号：US608167
申请日：1984-05-08
申请人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
IPC分类号： B22F1/00 , B01J12/02 , B01J19/26 , B22F9/02 , B22F9/12 , B22F9/28 , C22C1/10 , C22C32/00 , B22F9/00
CPC分类号： C22C32/0068 , B01J12/02 , B01J19/26 , B22F9/12 , C22C1/1031 , B01J2219/00119 , B01J2219/00132 , B01J2219/00159 , B01J2219/00162 , B01J2219/00191
摘要： A composite fine powder material is made of first particles with average particle diameter less than or equal to about ten microns, each having a composite structure and being made up of a plurality of fine second particles of a ceramic made by reacting together a first metal and a gas, embedded in a matrix of a second metal. This composite fine powder material is made by vaporizing the first metal, mixing the vapor with the gas, expanding the mixture through a first nozzle mechanism for providing adiabatic expansion cooling under reaction between the first metal and the gas to provide the fine second particles of ceramic, producing vapor of the second metal and mixing it in with the fine second particles at the downstream of the first nozzle mechanism, directing the resulting mixture through a second expansion nozzle mechanism to form the first particles of composite structure, and then collecting these first particles.
摘要翻译：复合细粉末材料由平均粒径小于或等于约10微米的第一颗粒制成，每个颗粒具有复合结构，并且由多个细小的第二颗粒构成，陶瓷通过使第一金属和一种嵌入第二金属的基体中的气体。这种复合细粉末材料是通过蒸发第一金属，将蒸气与气体混合，将混合物膨胀通过第一喷嘴机构膨胀，以在第一金属和气体之间的反应下提供绝热膨胀冷却，以提供细小的第二陶瓷颗粒产生第二金属的蒸汽并在第一喷嘴机构的下游将其与细小的第二颗粒混合，将所得混合物引导通过第二膨胀喷嘴机构以形成复合结构的第一颗粒，然后收集这些第一颗粒。

3. 发明授权

US4533413A Reinforced material incorporating fine composite powder and method and apparatus for making the same 失效
标题翻译：包含精细复合粉末的增强材料及其制造方法和装置
公开(公告)号：US4533413A
公开(公告)日：1985-08-06
申请号：US608113
申请日：1984-05-08
申请人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
IPC分类号： B22F1/00 , B01J12/02 , B01J19/26 , B22F1/02 , B22F9/02 , B22F9/12 , C01B21/068 , C01B21/072 , C22C1/05 , C22C1/10 , C22C29/00 , C22C29/06 , C22C29/08 , C22C29/12 , C22C29/14 , C22C29/16 , C22C32/00 , C22C23/02
CPC分类号： C22C1/1031 , B01J12/02 , B01J19/26 , B22F9/12 , C22C32/0036 , C22C32/0068 , B01J2219/00065 , B01J2219/00119 , B01J2219/00132 , B01J2219/00159 , B01J2219/00164 , Y10T428/12007 , Y10T428/12486
摘要： A composite material made of a matrix of a first metal and reinforcing first particles with average particle diameter less than or equal to about ten microns dispersed in the first metal matrix, with the reinforcing first particles each having a composite structure, being made up of a plurality of fine second particles of a ceramic made by reacting together a second metal and a gas and being combined with one another by a matrix of a third metal. This composite material is made by vaporizing the second metal, mixing the vapor with the gas, expanding the mixture through a nozzle means for providing adiabatic expansion cooling under reaction between the second metal and the gas to provide the fine second particles of ceramic, producing vapor of the third metal and mixing it in with the fine second particles at the downstream of the first nozzle means, directing the resulting mixture through a second expansion nozzle means to form the first particles of composite structure, and directing an output flow from the second nozzle means into a bath of the first metal to amalgamate the first particles with the matrix of first metal.
摘要翻译：由第一金属的基质和平均粒径小于或等于约十微米的增强的第一颗粒分散在第一金属基体中的复合材料制成，其中增强的第一颗粒各自具有复合结构，该复合材料由通过将第二金属和气体反应在一起并通过第三金属的基体彼此组合而形成的陶瓷的多个细小的第二颗粒。该复合材料通过蒸发第二金属，将蒸气与气体混合，将混合物膨胀通过喷嘴装置，在第二金属和气体之间的反应下提供绝热膨胀冷却，从而提供微细的第二陶瓷颗粒，产生蒸气的第三金属并在第一喷嘴装置的下游与细小的第二颗粒混合，将所得混合物引导通过第二膨胀喷嘴装置，以形成第一复合结构颗粒，并引导来自第二喷嘴的输出流意味着进入第一金属的浴，以与第一金属的基质合并第一颗粒。

4. 发明授权

US4533383A Device and method for making and collecting fine alloy powder 失效
标题翻译：制造和收集细合金粉末的装置和方法
公开(公告)号：US4533383A
公开(公告)日：1985-08-06
申请号：US608168
申请日：1983-05-08
申请人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Sato , Toshio Natsume , Hidenori Katagiri
IPC分类号： B01J12/02 , B01J19/26 , B22F9/12 , C22C1/00 , B22F9/00
CPC分类号： B01J19/26 , B01J12/02 , B22F9/12 , B01J2219/00065 , B01J2219/00074 , B01J2219/00119 , B01J2219/00132 , B01J2219/00159 , B01J2219/00164
摘要： Fine powder of an alloy of two or more metals is made by vaporizing each of these metals in its own vaporization chamber, mixing each of the metallic vapors with an inert carrier gas, and then adiabatically expanding each of the mixture gases through its own nozzle, which preferably is a convergent-divergent nozzle. Jet flows from the nozzles are collided together, after having been very rapidly cooled by this adiabatic expansion, and thereby the metal vapors in the jet flows are quickly condensed into very fine alloy particles. Optionally the combined flows from the jets are directed against an alloy powder collecting means, which may be a collection plate, but preferably is a bath of oil which entrains the alloy particles and keeps them from agglomerating together by partially neutralizing their surface activity. Thus fine alloy powder with particle diameters of the order of a few hundreds of angstroms can be economically produced.
摘要翻译：通过在其自身的蒸发室中蒸发这些金属中的每一种来制造两种或更多种金属的合金的细粉末，将每种金属蒸气与惰性载气混合，然后通过其自己的喷嘴绝热地膨胀混合气体，其优选是收敛扩散喷嘴。在通过这种绝热膨胀非常快速地冷却之后，从喷嘴喷射的喷嘴相互碰撞，从而喷射流中的金属蒸气迅速冷凝成非常细小的合金颗粒。任选地，来自射流的组合流被引导到合金粉末收集装置，该合金粉末收集装置可以是收集板，但是优选地是通过部分中和它们的表面活性而使合金颗粒夹带并防止它们聚集在一起的油浴。因此，可以经济地制造粒径在数百埃左右的精细合金粉末。

5. 发明授权

US4508682A Method for making composite material including matrix metal and metal cored ceramic surfaced fine powder material 失效
标题翻译：复合材料的制备方法，包括基体金属和金属芯陶瓷表面的细粉末材料
公开(公告)号：US4508682A
公开(公告)日：1985-04-02
申请号：US481466
申请日：1983-04-01
申请人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
IPC分类号： B22F1/02 , B22F9/12 , C22C1/10 , C22C29/06 , C22C29/12 , C22C29/14 , C22C29/16 , C22C32/00 , B22F9/00 , C22C23/00
CPC分类号： C22C1/1031 , B22F1/02 , B22F9/12 , C22C2001/1047
摘要： A composite material including matrix metal and ceramic surface - metallic core fine powder material is disclosed, composed of fine particles each having a metallic core and a ceramic surface layer, in which the average value of the ratio of the thickness of the surface layer of a powder particle to the radius of the particle is substantially greater than 0.05, dispersed within a matrix of matrix metal. A method and an apparatus for making this material from matrix metal, core metal, and a gas which combines with the core metal to form the ceramic outer layers of the particles are also described, in which a gaseous mixture of vapor of the core metal and the gas is passed through a convergent-divergent nozzle and is thereby rapidly cooled by adiabatic expansion so that the core metal as it solidifies forms metal cores for fine particles while the gas reacts with the outer layers of these particles to form ceramic surface layers, the jet from the nozzle then impacting against the surface of a pool of the molten matrix metal.
摘要翻译：公开了一种包含基体金属和陶瓷表面 - 金属芯细粉末材料的复合材料，其由具有金属芯和陶瓷表面层的细颗粒组成，其中，表面层的厚度的比值的平均值粉末颗粒到颗粒的半径基本上大于0.05，分散在基体金属的基体内。还描述了一种用于从基体金属，芯金属和与芯金属组合以形成颗粒的陶瓷外层的气体制造该材料的方法和装置，其中，芯金属的蒸气和气体通过会聚发散喷嘴，由此通过绝热膨胀快速冷却，使得当芯体固化时形成的金属芯形成细颗粒的金属芯，同时气体与这些颗粒的外层反应形成陶瓷表面层，然后从喷嘴喷射然后冲击熔融基质金属池的表面。

6. 发明授权

US4626561A Method of making two phase material of high molecular weight polymer and fine particles dispersed therein 失效
标题翻译：制备高分子量聚合物和细颗粒分散在其中的两相材料的方法
公开(公告)号：US4626561A
公开(公告)日：1986-12-02
申请号：US611547
申请日：1984-05-17
申请人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
IPC分类号： C08K3/00 , C08J3/20 , C08K3/02 , C08K3/08 , C08L23/00 , C08L67/00 , C08L101/00
CPC分类号： C08K3/08
摘要： A composite material having a high molecular weight polymer material as the matrix material and extremely fine particles of diameters of the order of tens to hundreds of angstroms dispersed in the matrix material is obtained by rapidly adiabatically cooling vapor of a metallic material through a nozzle, and squirting a jet of said fine particles into a molten mass of the high molecular weight polymer material. Optionally, inert gas may be squirted through the nozzle along with the vapor of the metallic material. Further, optionally a gas which forms a compound with the metallic material may be squirted through the nozzle with vapor of the metallic material, so that the particles become particles of a compound of the metallic material and the gas.
摘要翻译：通过快速绝热冷却金属材料的蒸气，通过喷嘴获得具有高分子量聚合物材料作为基体材料的复合材料和分散在基质材料中的数十至数百埃的直径的极细颗粒，并且将所述细颗粒的射流喷射到高分子量聚合物材料的熔融物质中。任选地，惰性气体可以与金属材料的蒸汽一起通过喷嘴喷射。此外，任选地，与金属材料形成化合物的气体可以通过金属材料的蒸气通过喷嘴喷射，使得颗粒成为金属材料和气体的化合物的颗粒。

7. 发明授权

US4526610A Metal cored ceramic surfaced fine powder material and apparatus and method for making it 失效
标题翻译：金属芯陶瓷表面处理细粉料及其制作方法
公开(公告)号：US4526610A
公开(公告)日：1985-07-02
申请号：US481464
申请日：1983-04-01
申请人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri
IPC分类号： B01J15/00 , B01J19/26 , B22F1/02 , B22F9/02 , B22F9/12 , C22C29/06 , C22C29/12 , C22C29/14 , C22C29/16
CPC分类号： B22F1/02 , B01J15/00 , B01J19/26 , B22F9/12 , B01J2219/00099 , B01J2219/00119 , B01J2219/00159 , B01J2219/00162 , B01J2219/00164 , B01J2219/00166 , Y10T428/2991 , Y10T428/2993
摘要： A ceramic surface-metallic core particle composite fine powder material is disclosed, composed of fine particles each having a metallic core and a ceramic surface layer, in which the average value of the ratio of the thickness of the surface layer of a powder particle to the radius of the particle is substantially greater than 0.05. A method and an apparatus for making this material from core metal and a gas which combines with the core metal to form the ceramic outer layer are also described, in which a gaseous mixture of vapor of the core metal and the gas is passed through a convergent-divergent nozzle and is thereby rapidly cooled by adiabatic expansion so that the core metal as it solidifies forms metal cores for fine particles while the gas reacts with the outer layers of these particles to form ceramic surface layers.
摘要翻译：公开了一种陶瓷表面金属芯颗粒复合细粉末材料，其由具有金属芯和陶瓷表面层的细颗粒组成，其中粉末颗粒的表面层的厚度与颗粒的半径基本上大于0.05。还描述了一种用于从芯金属制造该材料的方法和装置，以及与芯金属组合形成陶瓷外层的气体，其中核心金属和气体的气体的气体混合物通过会聚从而通过绝热膨胀快速冷却，使得固化的芯金属形成细颗粒的金属芯，同时气体与这些颗粒的外层反应形成陶瓷表面层。

8. 发明授权

US4626410A Method of making composite material of matrix metal and fine metallic particles dispersed therein 失效
标题翻译：制备基质金属和分散在其中的金属微粒的复合材料的方法
公开(公告)号：US4626410A
公开(公告)日：1986-12-02
申请号：US620176
申请日：1984-06-13
申请人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri , Yoshiro Hayashi , Masahiro Taguchi
发明人： Hirohisa Miura , Hiroshi Satou , Toshio Natsume , Hidenori Katagiri , Yoshiro Hayashi , Masahiro Taguchi
IPC分类号： B22D19/14 , B22D27/00 , B22F9/12 , C22C1/00 , C22C1/02 , C22C1/10 , C22C9/00 , B22F9/00 , C22C23/00
CPC分类号： B22F9/12 , B22D27/00 , C22C1/02 , C22C9/00
摘要： A composite material having a first metallic material as the matrix material and extremely fine particles of diameters of the order of tens to hundreds of angstroms of a second metal dispersed in this metallic matrix material is obtained by rapidly adiabatically cooling vapor of the second metallic material through a nozzle, and squirting a jet of fine particles produced thereby into a molten mass of the first material. Optionally, inert gas may be squirted through the nozzle along with the vapor of the second metallic material.
摘要翻译：具有第一金属材料作为基体材料的复合材料和分散在该金属基体材料中的第二金属分散在数十至数百埃数量级的极细颗粒是通过快速绝热冷却第二金属材料的蒸汽而通过喷嘴，并将由此产生的细粒子喷射喷射到第一材料的熔融物质中。任选地，惰性气体可以与第二金属材料的蒸气一起喷射通过喷嘴。

9. 发明授权

US4576725A Magnetic fluid incorporating fine magnetic powder and method for making the same 失效
标题翻译：含有细磁粉的磁性流体及其制造方法
公开(公告)号：US4576725A
公开(公告)日：1986-03-18
申请号：US620094
申请日：1984-06-13
申请人： Hirohisa Miura , Hiroshi Satou , Hidenori Katagiri , Toshio Natsume , Hidekazu Azuma
发明人： Hirohisa Miura , Hiroshi Satou , Hidenori Katagiri , Toshio Natsume , Hidekazu Azuma
IPC分类号： B22F1/00 , B22F9/12 , H01F1/06 , H01F1/28 , H01F1/34 , H01F1/44 , B22F9/00
CPC分类号： B22F1/0022 , B22F9/12 , B82Y30/00 , H01F1/066 , H01F1/28 , H01F1/442 , B22F2998/00
摘要： A magnetic fluid having a base liquid and magnetic particles with so small average particle diameter as to be of some hundreds of angstroms dispersed in the base liquid. Such a magnetic fluid is produced by ejecting a molten magnetic metal adiabatically from an expansion nozzle against a bath of a base liquid.
摘要翻译：具有基础液体的磁性流体和具有如此小的平均粒径的分散在基础液体中的几百埃的磁性颗粒。这样的磁性流体是通过从膨胀喷嘴绝热地熔融的金属金属喷射抵靠基础液体的浴而产生的。

10. 发明授权

US4695319A Metal distillation method utilizing double vaporization 失效
标题翻译：利用双蒸发的金属蒸馏法
公开(公告)号：US4695319A
公开(公告)日：1987-09-22
申请号：US759309
申请日：1985-07-26
申请人： Hirohisa Miura , Hiroshi Satoh , Toshio Natsume , Hidenori Katagiri
发明人： Hirohisa Miura , Hiroshi Satoh , Toshio Natsume , Hidenori Katagiri
IPC分类号： C22B9/02 , C22B13/06 , C22B19/04 , C22B19/32 , C22B21/06 , C22B26/22
CPC分类号： C22B19/04 , C22B13/06 , C22B19/32 , C22B21/06 , C22B26/22 , C22B9/02 , Y02P10/234
摘要： A method for separating a certain metal from a raw material including a mixture of the metal and an element which has a lower vapor pressure than the metal. The raw material including the mixture of the metal and the element is heated so as to cause a first vapor including the metal to be evolved. This first vapor is passed through a throttling means in which it undergoes adiabatic expansion and is rapidly cooled so that at least part of it is reduced to a liquid containing the metal. This liquid is reheated so as to cause a second vapor including the metal to be evolved. And the second vapor is cooled to collect the metal. An apparatus is also disclosed for performing this method.
摘要翻译：一种从原料分离某种金属的方法，包括金属和蒸汽压低于金属的元素的混合物。包括金属和元素的混合物的原料被加热以使包含金属的第一蒸气放出。该第一蒸气通过节流装置，其中它经历绝热膨胀并被快速冷却，使得其至少一部分被还原成含有金属的液体。将该液体再加热，以使包含金属的第二蒸气放出。并且将第二蒸气冷却以收集金属。还公开了一种用于执行该方法的装置。

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