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1. 发明授权

US06596445B1 O-acyloxime photoinitiators 有权
标题翻译： O-酰基肟光引发剂
公开(公告)号：US06596445B1
公开(公告)日：2003-07-22
申请号：US09338152
申请日：1999-06-23
申请人： Akira Matsumoto , Hidetaka Oka , Masaki Ohwa , Hisatoshi Kura , Jean-Luc Birbaum , Kurt Dietliker
发明人： Akira Matsumoto , Hidetaka Oka , Masaki Ohwa , Hisatoshi Kura , Jean-Luc Birbaum , Kurt Dietliker
IPC分类号： C07C25164
CPC分类号： C07C251/66 , B33Y70/00 , C07C251/68 , C07C323/47 , C07D295/135 , C07D335/18 , C08F2/50 , G03F7/0007 , G03F7/002 , G03F7/0045 , G03F7/031 , G03F7/0388
摘要： Oximeester compounds of the formulae I, II, III and IV wherein R1 is phenyl, C1-C20alkyl or C2-C20alkyl optionally interrupted by —O—, C2-C20alkanoyl or benzoyl, or R1 is C2-C12alkoxycarbonyl or phenoxycarbonyl; R1′ is C2-C12alkoxycarbonyl, or R1′ is phenoxycarbonyl, or R1′ is —CONR10R11 or CN; R2 is C2-C12alkanoyl, C4-C6alkenoyl, benzoyl, C2-C6alkoxycarbonyl or phenoxycarbonyl; R3, R4, R5, R6 and R7 are hydrogen, halogen, C1-C12alkyl, cyclopentyl, cyclohexyl, phenyl, benzyl, benzoyl, C2-C12alkanoyl, C2-C12alkoxycarbonyl, phenoxycarbonyl or a group OR8, SR9, SOR9, SO2R9 or NR10R11; R4′, R5′ and R6′ are hydrogen, halogen, C1-C12alkyl, cyclopentyl, cyclohexyl, phenyl, benzyl, benzoyl, C2-C12-alkanoyl, C2-C12alkoxycarbonyl, phenoxycarbonyl, or are a group OR8, SR9, SOR9, SO2R9, NR10R11; provided that at least one of R3, R4, R5, R6, R7, R′4, R′5 and R′6 is OR8, SR9 or NR10R11; R8, R9, R10 and R11 are for example hydrogen, C1-C12alkyl, phenyl; are suitable as initiators for the photopolymerization of radically polymerizable compounds.
摘要翻译：式I，II，III和IV其中R 1的肟酯化合物是苯基，任选被-O - ，C 2 -C 20烷酰基或苯甲酰基中断的C 1 -C 20烷基或C 2 -C 20烷基，或者R 1是C 2 -C 12烷氧基羰基或苯氧基羰基; R1'是C2-C12烷氧基羰基，或R1'是苯氧基羰基，或R1'是-CONR10R11或CN; R2是C2-C12烷酰基，C4-C6链烯酰基，苯甲酰基，C2-C6烷氧基羰基或苯氧基羰基; R3，R4，R5，R6和R7是氢，卤素，C1-C12烷基，环戊基，环己基，苯基，苄基，苯甲酰基，C2-C12烷酰基，C2-C12烷氧基羰基，苯氧基羰基或OR8，SR9，SOR9，SO2R9或NR10R11; R4'，R5'和R6'为氢，卤素，C1-C12烷基，环戊基，环己基，苯基，苄基，苯甲酰基，C2-C12-烷酰基，C2-C12烷氧基羰基，苯氧基羰基，或为OR8，SR9，SOR9，SO2R9 ，NR10R11; 条件是R3，R4，R5，R6，R7，R'4，R'5和R'6中的至少一个是OR8，SR9或NR10R

2. 发明授权

US06485885B1 Photopolymerizable thermosetting resin compositions 有权
标题翻译：光聚合性热固性树脂组合物
公开(公告)号：US06485885B1
公开(公告)日：2002-11-26
申请号：US09720441
申请日：2000-12-22
申请人： Hidetaka Oka , Masaki Ohwa , Akira Matsumoto , Hisatoshi Kura
发明人： Hidetaka Oka , Masaki Ohwa , Akira Matsumoto , Hisatoshi Kura
IPC分类号： G03F7004
CPC分类号： G03F7/031 , G03F7/038
摘要： Compositions comprising (A) an oligomer or polymer containing at least one carboxylic acid group in the molecule; (B) at least one compound of formulas (I, II, III, IV, V or VI), wherein R1 inter alia is phenyl or alkyl; R2 is for example C2-C12alkonoyl which is unsubstituted or substituted or is benzoyl; R3, R4, R5, R6 and R7 independently of one another are for instance hydrogen, C1-C12alkyl, cyclohexyl or phenyl which is unsubstituted or substituted, or are benzyl, benzoyl, C2-C12alkanoyl or phenoxycarbonyl; R8 is for example hydrogen or C1-C12alkyl or a group (B); M is for example C1-C12alkylene, cyclohexylene or phenylene; M1 inter alia is a direct bond or C1-C12alkylenoxy; and Ar is a 5- or 6-membered aromatic heterocyclic ring; (C) a photopolymerizable reactive or unreactive diluent; and (D) as a thermosetting component an epoxy compound containing at least two epoxy groups in one molecule; are highly suitable as resists which are alkaline developable.
摘要翻译：包含（A）在分子中含有至少一个羧酸基团的低聚物或聚合物的组合物; （B）至少一种式（I，II，III，IV，V或VI）化合物，其中R 1特别是苯基或烷基; R2是例如未取代或取代的C 2 -C 12烷氧基或苯甲酰基; R 3，R 4，R 5，R 6和R 7彼此独立地是例如氢，C 1 -C 12烷基，环己基或未取代或取代的苯基，或者是苄基，苯甲酰基，C 2 -C 12烷酰基或苯氧基羰基; R8是例如氢或C1-C12烷基或基团（B）; M为例如C 1 -C 12亚烷基，亚环己基或亚苯基; M1特别是直接键或C1-C12亚烷基氧基; 且Ar为5-或6-元芳族杂环; （C）可光聚合反应性或非活性稀释剂; 和（D）作为热固性组分在一个分子中含有至少两个环氧基团的环氧化合物; 非常适合作为碱性显影的抗蚀剂。

3. 发明申请

US20100136491A1 OXIME ESTER PHOTOINITIATORS 有权
标题翻译： OXIME ESTER光敏剂
公开(公告)号：US20100136491A1
公开(公告)日：2010-06-03
申请号：US12598477
申请日：2008-04-24
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F7/20 , C07D209/88 , C07D209/80 , C07D417/12 , C08F2/46 , G02B5/22
CPC分类号： G03F7/027 , C07D209/80 , C07D209/86 , C07D209/88 , C07D403/10 , C07D409/06 , C07D409/14 , G02B5/20 , G03F7/2002 , G03F7/2037 , G03F7/2039 , G03F7/30
摘要： Compounds of formula (I), (II), and (III), wherein R1, R2, R′2 and R′″2 for example are C1-C20alkyl, provided that at least one of R1, R2, R′2 and R′″2 carries a specified substituent; R3, R4, and R5 for example independently of one another are hydrogen or a defined substituent provided that at least one of R3, R4 or R5 is other than hydrogen or C1-C20alkyl; R6, R7, R8, R′7, RV, R′8, R″6, R″7, R′″6 and R′″7 for example independently of one another have one of the meanings as given for R3, R4, and R5; and R9 for example is C1-C20alkyl; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I），（II）和（III）的化合物，其中R 1，R 2，R'2和R'2例如是C 1 -C 20烷基，条件是R 1，R 2，R'2和 R“2携带指定的取代基; R 3，R 4和R 5例如彼此独立地是氢或定义的取代基，条件是R 3，R 4或R 5中的至少一个不是氢或C 1 -C 20烷基; R6，R7，R8，R'7，RV，R'8，R“6，R”7，R“”6“和”7“，例如彼此独立地具有R 3，R 4 ，和R5; 例如，R 9为C 1 -C 20烷基; 在光聚合反应中表现出出人意料的良好性能。

4. 发明申请

US20100136467A1 OXIME ESTER PHOTOINITIATORS 有权
标题翻译： OXIME ESTER光敏剂
公开(公告)号：US20100136467A1
公开(公告)日：2010-06-03
申请号：US12598481
申请日：2008-04-28
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F1/00 , C07D409/06 , C07D335/08 , C07D417/12 , C07D409/14 , G03F7/20
CPC分类号： C07D409/06 , B33Y70/00 , C07D209/86 , C07D335/16 , C07D405/12 , C07D409/14 , C07D417/12
摘要： Compounds of the formula (I) and (II) M1, M2 and M3 independently of one another are no bond, a direct bond, CO, O, S, SO, SO2or NR14; provided that at least one of M1, M2 or M3 is a direct bond, CO, O, S, SO, SO2 or NR14; M4 is a direct bond, CR″3R″4, CS, O, S, SO, or SO2; Y is S or NR18; R1 for example is hydrogen, C3-C8cycloalkyl, phenyl or napthyl, both of which are optionally substituted; R2 for example is C1-C20alkyl; R″2 has one of the meanings given for R2; R3 and R4 are for example hydrogen, halogen, C1-C20alkyl; R′3, R′4, R″3 and R″4 indepedently of one another have one of the meanings given for R3 and R4; and R5 is for example hydrogen, halogen, C1-C20alkyl; provided that in the compounds of the formula (I) at least two oxime ester groups are present and provided that at least one specified substituent R2 or R″2 is present; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I）和（II）中的M1，M2和M3彼此独立的化合物不是键，直接键，CO，O，S，SO，SO 2或NR 14; 条件是M1，M2或M3中的至少一个是直接键，CO，O，S，SO，SO 2或NR 14; M4是直接键，CR“3R”4，CS，O，S，SO或SO 2; Y为S或NR18; R 1例如是氢，C 3 -C 8环烷基，苯基或萘基，它们都是任选被取代的; R 2例如是C 1 -C 20烷基; R“2具有R2的含义之一; R3和R4是例如氢，卤素，C1-C20烷基; R'3，R'4，R“3和R”4彼此独立地具有R3和R4给出的含义之一; R5是例如氢，卤素，C1-C20烷基; 条件是在式（I）的化合物中存在至少两个肟酯基团，条件是存在至少一个特定的取代基R 2或R“2; 在光聚合反应中表现出出人意料的良好性能。

5. 发明申请

US20100086881A1 OXIME ESTER PHOTOINITIATORS 有权
标题翻译： OXIME ESTER光敏剂
公开(公告)号：US20100086881A1
公开(公告)日：2010-04-08
申请号：US12598601
申请日：2008-04-28
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F7/20 , C07D209/88 , B32B27/18 , C07D335/08 , C09K3/00 , C08F2/46 , G02B5/20
CPC分类号： C07D401/12 , B33Y70/00 , C07D417/06 , C08F2/50 , G03F7/031 , Y10T428/31855
摘要： Compounds of the formula (I), wherein A1 is formula (II); A2 is formula (III); A3 is formula (IV); A4 is formula (V); w, x, y and z independently of each other are an integer from 0-4, provided that the sum of x+y+z is an integer from 2-4, corresponding to the valency of Q; M1, M2, M3 and M4 for example are a direct bond, CO or O; Y for example is a direct bond or S; Q is a (x+y)-valent linking group; R1 is for example hydrogen, C1-C20alkyl or phenyl or naphthyl; R2 and R″2 for example are is hydrogen or C1-C20alkyl; R3, R4, R′3, R′4, R″3 and R″4 for example are hydrogen, halogen, phenyl, or C1-C20alkyl; and R24 is for example a direct bond; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I）化合物，其中A1为式（II）; A2是式（III）; A3是式（IV）; A4是公式（V）; w，x，y和z彼此独立地是0-4的整数，条件是x + y + z的和是2-4的整数，对应于Q的化合价; M1，M2，M3和M4例如是直接键，CO或O; Y例如是直接债券或S; Q是（x + y）价的连接基团; R1是例如氢，C1-C20烷基或苯基或萘基; R2和R“2例如是氢或C1-C20烷基; R 3，R 4，R'3，R'4，R“3和R”4例如是氢，卤素，苯基或C 1 -C 20烷基; 并且R 24例如是直接键; 在光聚合反应中表现出出人意料的良好性能。

6. 发明授权

US08586268B2 Oxime ester photoinitiators 有权
标题翻译：肟酯光引发剂
公开(公告)号：US08586268B2
公开(公告)日：2013-11-19
申请号：US12086567
申请日：2006-11-09
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G02B5/20 , G03F7/031
CPC分类号： G03F7/031 , B33Y70/00 , C07D209/86 , C07D409/06 , C08F2/50 , G03F7/0007 , G03F7/001
摘要： Compounds of the Formula (I) and (II) wherein M1, M2 and M3 independently of one another are no bond, a direct bond, CO, O, S, SO, SO2 or NR14; provided that at least one of M1, M2 or M3 is a direct bond, CO, O, S, SO, SO2 or NR14; M4 is a direct bond, CR″3R″4, CS, O, S, SO, or SO2; Y is S or NR18; R1 for example is hydrogen, C3-C8cycloalkyl, phenyl or naphthyl, both of which are optionally substituted; R2 for example is C1-C20alkyl; R″2 has one of the meanings given for R2; R3 and R4 are for example hydrogen, halogen, C1-C20alkyl; R′3, R′4, R″3 and R″4 independently of one another have one of the meanings given for R3 and R4; and R5 is for example hydrogen, halogen, C1-C20alkyl; provided that in the compounds of the Formula (I) at least two oxime ester groups are present; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：其中M1，M2和M3彼此独立的式（I）和（II）的化合物不是键，直接键，CO，O，S，SO，SO 2或NR 14; 条件是M1，M2或M3中的至少一个是直接键，CO，O，S，SO，SO 2或NR 14; M4是直接键，CR''3R''4，CS，O，S，SO或SO2; Y为S或NR18; R 1例如是氢，C 3 -C 8环烷基，苯基或萘基，它们都是任选取代的; R 2例如是C 1 -C 20烷基; R'2具有R2中给出的含义之一; R3和R4是例如氢，卤素，C1-C20烷基; R 3，R'4，R“3和R”4彼此独立地具有R3和R4给出的含义之一; R5是例如氢，卤素，C1-C20烷基; 条件是在式（I）的化合物中存在至少两个肟酯基团; 在光聚合反应中表现出出人意料的良好性能。

7. 发明申请

US20100188765A1 Oxime Ester Photoinitiators 有权
标题翻译：肟酯光引发剂
公开(公告)号：US20100188765A1
公开(公告)日：2010-07-29
申请号：US12086567
申请日：2006-11-09
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F7/004 , C07D209/58 , C08F2/50 , G03F7/20 , G03F7/031 , G02B5/22
CPC分类号： G03F7/031 , B33Y70/00 , C07D209/86 , C07D409/06 , C08F2/50 , G03F7/0007 , G03F7/001
摘要： Compounds of the Formula (I) and (II) wherein M1, M2 and M3 independently of one another are no bond, a direct bond, CO, O, S, SO, SO2 or NR14; provided that at least one of M1, M2 or M3 is a direct bond, CO, O, S, SO, SO2 or NR14; M4 is a direct bond, CR″3R″4, CS, O, S, SO, or SO2; Y is S or NR18; R1 for example is hydrogen, C3-C8cycloalkyl, phenyl or naphthyl, both of which are optionally substituted; R2 for example is C1-C20alkyl; R″2 has one of the meanings given for R2; R3 and R4 are for example hydrogen, halogen, C1-C20alkyl; R′3, R′4, R″3 and R″4 independently of one another have one of the meanings given for R3 and R4; and R5 is for example hydrogen, halogen, C1-C20alkyl; provided that in the compounds of the Formula (I) at least two oxime ester groups are present; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：其中M1，M2和M3彼此独立的式（I）和（II）的化合物不是键，直接键，CO，O，S，SO，SO 2或NR 14; 条件是M1，M2或M3中的至少一个是直接键，CO，O，S，SO，SO 2或NR 14; M4是直接键，CR“3R”4，CS，O，S，SO或SO 2; Y为S或NR18; R 1例如是氢，C 3 -C 8环烷基，苯基或萘基，它们都是任选取代的; R 2例如是C 1 -C 20烷基; R“2具有R2的含义之一; R3和R4是例如氢，卤素，C1-C20烷基; R'3，R'4，R“3和R”4彼此独立地具有R3和R4给出的含义之一; R5是例如氢，卤素，C1-C20烷基; 条件是在式（I）的化合物中存在至少两个肟酯基团; 在光聚合反应中表现出出人意料的良好性能。

8. 发明申请

US20090087759A1 Oxime Ester Photoinitiators 有权
标题翻译：肟酯光引发剂
公开(公告)号：US20090087759A1
公开(公告)日：2009-04-02
申请号：US12085383
申请日：2006-11-08
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F1/02 , C07D209/88 , C08F2/46 , G03F7/20
CPC分类号： C07D209/86 , C07D209/88 , C07D403/10 , C07D409/06 , C07D409/10 , G03F7/031
摘要： Compounds of the formula (I), (II), and wherein R1, R2, R′2 and R′″2 for example are C1-C20alkyl; R3, R4, and R5 for example independently of one another are hydrogen or a defined substituent provided that at least one of R3, R4 or R5 is other than hydrogen or C1-C20alkyl; R6, R7, R8, R′6, R′7, R′8, R″6, R″7, R′″6 and R′″7 for example independently of one another have one of the meanings as given for R3, R4, and R5; and R9 for example is C1-C20alkyl; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I），（II）和其中R 1，R 2，R'2和R“2的化合物例如是C 1 -C 20烷基; R 3，R 4和R 5例如彼此独立地是氢或定义的取代基，条件是R 3，R 4或R 5中的至少一个不是氢或C 1 -C 20烷基; R6，R7，R8，R'6，R'7，R'8，R'6，R'7，R“'6和R”'7例如彼此独立地具有一个含义如R3，R4和R5所示; 例如，R 9为C 1 -C 20烷基; 在光聚合反应中表现出出人意料的良好性能。

9. 发明授权

US08911921B2 Oxime ester photoinitiators 有权
标题翻译：肟酯光引发剂
公开(公告)号：US08911921B2
公开(公告)日：2014-12-16
申请号：US12598477
申请日：2008-04-24
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G03F7/031 , G02B5/20
CPC分类号： G03F7/027 , C07D209/80 , C07D209/86 , C07D209/88 , C07D403/10 , C07D409/06 , C07D409/14 , G02B5/20 , G03F7/2002 , G03F7/2037 , G03F7/2039 , G03F7/30
摘要： Compounds of formula (I), (II), and (III), wherein R1, R2, R′2 and R′″2 for example are C1-C20alkyl, provided that at least one of R1, R2, R′2 and R′″2 carries a specified substituent; R3, R4, and R5 for example independently of one another are hydrogen or a defined substituent provided that at least one of R3, R4 or R5 is other than hydrogen or C1-C20alkyl; R6, R7, R8, R′7, RV, R′8, R″6, R″7, R′″6 and R′″7 for example independently of one another have one of the meanings as given for R3, R4, and R5; and R9 for example is C1-C20alkyl; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I），（II）和（III）的化合物，其中R 1，R 2，R'2和R'2例如是C 1 -C 20烷基，条件是R 1，R 2，R'2和 R“2携带指定的取代基; R 3，R 4和R 5例如彼此独立地是氢或定义的取代基，条件是R 3，R 4或R 5中的至少一个不是氢或C 1 -C 20烷基; R6，R7，R8，R'7，RV，R'8，R“6，R”7，R“”6“和”7“，例如彼此独立地具有R 3，R 4 ，和R5; 例如，R 9为C 1 -C 20烷基; 在光聚合反应中表现出出人意料的良好性能。

10. 发明授权

US08524425B2 Oxime ester photoinitiators 有权
标题翻译：肟酯光引发剂
公开(公告)号：US08524425B2
公开(公告)日：2013-09-03
申请号：US12598481
申请日：2008-04-28
申请人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
发明人： Akira Matsumoto , Junichi Tanabe , Hisatoshi Kura , Masaki Ohwa
IPC分类号： G02B5/20 , G03F7/031
CPC分类号： C07D409/06 , B33Y70/00 , C07D209/86 , C07D335/16 , C07D405/12 , C07D409/14 , C07D417/12
摘要： Compounds of the formula (I) and (II) M1, M2 and M3 independently of one another are no bond, a direct bond, CO, O, S, SO, SO2 or NR14; provided that at least one of M1, M2 or M3 is a direct bond, CO, O, S, SO, SO2 or NR14; M4 is a direct bond, CR″3R″4, CS, O, S, SO, or SO2; Y is S or NR18; R1 for example is hydrogen, C3-C8cycloalkyl, phenyl or napthyl, both of which are optionally substituted; R2 for example is C1-C20alkyl; R″2 has one of the meanings given for R2; R3 and R4 are for example hydrogen, halogen, C1-C20alkyl; R′3, R′4, R″3 and R″4 independently of one another have one of the meanings given for R3 and R4; and R5 is for example hydrogen, halogen, C1-C20alkyl; provided that in the compounds of the formula (I) at least two oxime ester groups are present and provided that at least one specified substituent R2 or R″2 is present; exhibit an unexpectedly good performance in photopolymerization reactions.
摘要翻译：式（I）和（II）M1，M2和M3彼此独立的化合物不是键，直接键，CO，O，S，SO，SO 2或NR 14; 条件是M1，M2或M3中的至少一个是直接键，CO，O，S，SO，SO 2或NR 14; M4是直接键，CR''3R''4，CS，O，S，SO或SO2; Y为S或NR18; R 1例如是氢，C 3 -C 8环烷基，苯基或萘基，它们都是任选被取代的; R 2例如是C 1 -C 20烷基; R'2具有R2中给出的含义之一; R3和R4是例如氢，卤素，C1-C20烷基; R 3，R'4，R“3和R”4彼此独立地具有R3和R4给出的含义之一; R5是例如氢，卤素，C1-C20烷基; 条件是在式（I）的化合物中存在至少两个肟酯基团，条件是存在至少一个特定的取代基R 2或R“2; 在光聚合反应中表现出出人意料的良好性能。

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