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1. 发明授权

US3999941A Process for the manufacture of polycondensation products containing phosphorus, the products and their use as flameproofing agents 失效
标题翻译：用于制造含磷的缩聚产物的方法，该产品及其用作防火剂
公开(公告)号：US3999941A
公开(公告)日：1976-12-28
申请号：US577150
申请日：1975-05-13
申请人： Hermann Nachbur , Joerg Kern , Arthur Maeder
发明人： Hermann Nachbur , Joerg Kern , Arthur Maeder
IPC分类号： B27K3/15 , B27K3/50 , C08G61/12 , C08G79/06 , D06M13/285 , D06M15/431 , D06M15/667 , D06M15/673 , D06M13/28 , D06M15/62
CPC分类号： D06M15/673 , C08G61/128 , C08G79/06 , C08L97/02 , D06M13/285 , D06M15/431 , D06M15/667 , B27K2240/30 , B27K3/15 , C08L85/02 , Y10T442/2689
摘要： The subject of the invention is a process for the manufacture of polycondensation products from hydroxymethylphosphonium compounds, characterized in that at least one anhydrous tetrakis-(hydroxymethyl)-phosphonium salt or tetrakis-(hydroxymethyl)-phosphonium hydroxide is condensed with itself in an anhydrous medium, optionally using an acid catalyst and optionally in the presence of at least one inert organic solvent, at 100.degree. to 150.degree. C, preferably 120.degree. to 150.degree. C, the condensation being continued until 0.5 to 1.5 mols of water have been eliminated per 1 mol of phosphonium compound employed, free hydroxyl groups are, if appropriate, at least partially etherified with at least one alkanol with 1 to 4 carbon atoms, and that the salt of the polycondensation products are, where relevant, converted into the corresponding hydroxides.The polycondensation products are used for the flameproofing of organic fibre material, especially textiles. Appropriately, the procedure followed is that an aqueous preparation is applied to these materials which contains at least 1) a polycondensation product of the indicated type and 2) a polyfunctional compound, and that the material thus treated are dried and subjected to a heat treatment.
摘要翻译：本发明的主题是由羟甲基鏻化合物制造缩聚产物的方法，其特征在于至少一种无水四（羟甲基）鏻盐或四（羟甲基）鏻氢氧化物与自身在无水介质中缩合，任选地使用酸催化剂，任选地在至少一种惰性有机溶剂的存在下，在100-150℃，优选120-150℃下，继续进行缩合直至0.5-1.5摩尔的水已被除去如果合适的话，使用1mol鏻化合物，如果合适，游离羟基与至少一种具有1至4个碳原子的链烷醇至少部分醚化，并且缩聚产物的盐在相关时转化为相应的氢氧化物。

2. 发明授权

US4185037A Process for the manufacture of phosphorus-containing condensation products, the products and their use as flameproofing agents 失效
标题翻译：制造含磷缩合产物的方法，该产品及其用作防火剂
公开(公告)号：US4185037A
公开(公告)日：1980-01-22
申请号：US963500
申请日：1978-11-24
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： D06M15/673 , B27K3/15 , C07F9/54 , C08L61/32 , C09K21/12 , D06B3/10 , D06M15/431 , D06M15/667 , C07C87/20 , C07C87/36 , C07C87/52 , C07C91/04
CPC分类号： D06M15/667 , C07F9/5407 , C08L61/32 , C09K21/12 , D06M15/431
摘要： The subject of the invention is a process for the manufacture of polycondensation products of hydroxymethylphosphonium compounds and an amine, characterized in that (a) 1 mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with 0.02 to 0.3 mol, preferably 0.02 to 0.25 mol, of an amine at 100.degree. to 150.degree. C., optionally in the presence of an inert organic solvent, if appropriate free hydroxyl groups are at least partially etherified with at least one alkanol with 1 to 4 carbon atoms and if appropriate the salts of the polycondensation products are converted into the corresponding hydroxides.The condensation products are used for flameproofing organic fiber material, especially textiles.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和胺的缩聚产物的方法，其特征在于（a）1摩尔四（羟甲基）鏻化合物与0.02至0.3摩尔，优选0.02至 0.25mol的胺，任选在惰性有机溶剂的存在下，如果合适的游离羟基至少部分用至少一个具有1至4个碳原子的链烷醇醚化，并且如果合适的话，缩聚产物的盐转化为相应的氢氧化物。缩合产物用于隔离有机纤维材料，特别是纺织品。

3. 发明授权

US4026889A Phosphorus-containing condensation products 失效
标题翻译：含磷缩合产物
公开(公告)号：US4026889A
公开(公告)日：1977-05-31
申请号：US624630
申请日：1975-10-21
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： B27K3/15 , C07F9/54 , C08G12/36 , C08G12/40 , C08G16/02 , C08L61/32 , D06M15/667 , D06M15/673 , C07D251/72
CPC分类号： D06M15/673 , C07F9/54 , C08G12/36 , C08G12/40 , C08G16/0243 , C08L61/32 , D06M15/667 , B27K2240/30 , B27K3/15
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethylphosphonium compounds and bicyclic dienes, characterized in that (a) one mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with (b) 0.02 to 1 mol, preferably 0.1 to 0.5 mol, of a 2,4,6,8,9-pentaazo-bicyclo-[3.3.1]-nona-2,6-diene of the formula ##STR1## or its salt, wherein R represents hydrogen, hydroxyl or an optionally substituted aliphatic, cycloaliphatic, aromatic or heterocyclic radical; at 40.degree. to 120.degree. C, optionally in the presence of formaldehyde or a formaldehyde-releasing agent and optionally in the presence of an inert organic solvent, the condensation is optionally thereafter continued at temperatures of 100.degree. to 150.degree. C and, if appropriate, free hydroxyl groups are etherified at least partially with at least one alkanol with 1 to 4 carbon atoms and, if appropriate, the salts of the condensation products are converted into the corresponding hydroxides.The condensation products are used for flameproofing organic fiber material, especially textiles.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和双环二烯的水溶性缩合产物的方法，其特征在于（a）将一摩尔四（羟甲基）鏻化合物与（b）0.02缩合成 1摩尔，优选0.1至0.5摩尔的式（1）的2,4,6,8,9-五偶氮 - 双环[3.3.1] - ona -2,6-二烯或其盐其中R表示氢，羟基或任选取代的脂族，脂环族，芳族或杂环基; 在40℃至120℃下，任选在甲醛或甲醛释放剂存在下，任选在惰性有机溶剂存在下，任选地在100至150℃的温度下继续冷凝，如果合适至少部分用至少一个具有1-4个碳原子的链烷醇醚化游离羟基，如果合适的话，缩合产物的盐转化为相应的氢氧化物。

4. 发明授权

US3946092A Bromine substituted phosphates 失效
标题翻译：溴取代磷酸盐
公开(公告)号：US3946092A
公开(公告)日：1976-03-23
申请号：US483493
申请日：1974-06-27
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： C07F9/09 , C07F9/12 , C08K5/521 , C08K5/523 , D06M13/02 , D06M13/244 , D06M13/282 , D06M13/292 , D06M13/298
CPC分类号： D06M13/298 , C07F9/091 , C07F9/093 , C07F9/12 , C08K5/521 , C08K5/523 , D06M13/292
摘要： New phosphates are provided which correspond to the formula ##EQU1## wherein X is phenyl or substituted phenyl, R.sub.1 and R.sub.2 each is bromoalkylene, D.sub.1 and D.sub.2 each is hydrogen, hydroxyl or bromine or D.sub.1 and D.sub.2 alone or together are linked to a second phosphate radical. The phosphates are useful as flameproofing agents for organic fiber material, especially polyester fiber, or for plastics.
摘要翻译：提供新的磷酸酯，其对应于式D1-R1O角度D2-R2O-X，其中X是苯基或取代的苯基，R1和R2各自是溴亚烷基，D1和D2各自是氢，羟基或溴，或者单独使用D1和D2 或一起连接到第二磷酸根基团。磷酸盐可用作有机纤维材料，特别是聚酯纤维或塑料的防火剂。

5. 发明授权

US3931310A Phosphorus-containing condensation products 失效
标题翻译：含磷缩合产物
公开(公告)号：US3931310A
公开(公告)日：1976-01-06
申请号：US285268
申请日：1972-08-31
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： D06M15/673 , B27K3/15 , C07F9/54 , C08L61/32 , D06M15/431 , D06M15/667 , D06M101/12
CPC分类号： D06M15/667 , C07F9/54 , C07F9/5407 , C08L61/32 , D06M15/431 , B27K2240/30 , B27K3/15
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethyl-phosphonium compounds and dicyandiamide, characterised in that (a) 1 mol of a tetrakis-(hydroxymethyl)phosphonium compound is condensed with (b) 0.02 to 0.2 mol, preferably 0.05 to 0.15 mol, of an optionally methylolated dicyandiamide at 40.degree. to 120.degree.C, optionally in the presence of formaldehyde or a formaldehyde-donating agent, and an inert organic solvent, and optionally subsequently further condensed at temperature of 100.degree. to 150.degree.C, and if appropriate free hydroxyl groups are at least partially etherified with at least one alkanol with 1 to 4 carbon atoms and if appropriate the salts of the condensation products are converted into the corresponding hydroxides.The condensation products are used for flameproofing organic fibre material, especially textiles.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和双氰胺的水溶性缩合产物的方法，其特征在于（a）1摩尔四（羟甲基）鏻化合物与（b）0.02与 0.2mol，优选0.05-0.15mol任选的羟甲基化双氰胺在40-120℃，任选地在甲醛或甲醛供体剂和惰性有机溶剂的存在下，任选地随后在100℃的温度下进一步冷凝至少150℃，如果合适的游离羟基与至少一个具有1至4个碳原子的链烷醇至少部分醚化，如果合适，则缩合产物的盐转化为相应的氢氧化物。

6. 发明授权

US4055689A Process for flameproofing organic fiber material 失效
标题翻译：隔爆有机纤维材料的工艺
公开(公告)号：US4055689A
公开(公告)日：1977-10-25
申请号：US648541
申请日：1976-01-12
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： C07F9/09 , C07F9/12 , C08K5/521 , C08K5/523 , D06M13/292 , D06M13/298 , C09K3/28 , C09D5/18
CPC分类号： D06M13/298 , C07F9/091 , C07F9/093 , C07F9/12 , C08K5/521 , C08K5/523 , D06M13/292 , Y10S428/921 , Y10T442/2672
摘要： Process for flameproofing organic material, which comprises applying to said material a preparation containing a phosphate of the formula ##STR1## wherein X is phenyl or substituted phenyl, R.sub.1 and R.sub.2 each is bromoalkylene, then drying the material and subjecting it to heat treatment.
摘要翻译：用于隔爆有机材料的方法，其包括向所述材料施加含有式（I）的磷酸酯的制剂，其中X为苯基或取代的苯基，R 1和R 2各自为溴代亚烷基，然后干燥该材料并对其进行热处理。

7. 发明授权

US3994971A Phosphorus-containing condensation products 失效
标题翻译：含磷缩合产物
公开(公告)号：US3994971A
公开(公告)日：1976-11-30
申请号：US604411
申请日：1975-08-13
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： B27K3/15 , B27K3/50 , C07F9/54 , C08L61/32 , D06M15/431 , D06M15/667 , D06M15/673 , C07C125/08 , C07F9/22 , C09K3/28
CPC分类号： D06M15/673 , C07F9/5407 , C08L61/32 , D06M15/431 , D06M15/667 , B27K2240/30 , B27K3/15 , Y10T442/268
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethylphosphonium compounds and cyanamide, characterized in that (a) one mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with (b) 0.02 to 0.5 mol, preferably 0.1 to 0.3 mol, of cyanamide at 40.degree. to 120.degree. C, optionally in the presence of formaldehyde or a formaldehyde-donating agent and optionally in the presence of an inert organic solvent, and optionally subsequently further condensed at temperatures of 100.degree. to 150.degree. C and, if appropriate, free hydroxyl groups are at least partially etherified with at least one alkanol with 1 to 4 carbon atoms and if appropriate the salts of the condensation products are converted into the corresponding hydroxides.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和氨腈的水溶性缩合产物的方法，其特征在于（a）一摩尔四（羟甲基）鏻化合物与（b）0.02至0.5 mol，优选0.1至0.3mol氰氨腈，任选在甲醛或甲醛供体剂存在下，任选在惰性有机溶剂存在下，任选地随后在100℃的温度下进一步冷凝如果合适，游离羟基至少部分用至少一个具有1至4个碳原子的链烷醇醚化，如果合适，则缩合产物的盐转化为相应的氢氧化物。

8. 发明授权

US3932502A Process for the manufacture of phosphorus-containing condensation products, the products and their use as flameproofing agents 失效
标题翻译：制造含磷缩合产物的方法，该产品及其用作防火剂
公开(公告)号：US3932502A
公开(公告)日：1976-01-13
申请号：US285172
申请日：1972-08-31
申请人： Hermann Nachbur , Arthur Maeder
发明人： Hermann Nachbur , Arthur Maeder
IPC分类号： D06M15/673 , B27K3/15 , C07F9/54 , C08L61/32 , D06M15/431 , D06M15/667 , C07C127/24
CPC分类号： D06M15/667 , C07F9/54 , C07F9/5407 , C08L61/32 , D06M15/431 , B27K2240/30 , B27K3/15 , Y10T442/268
摘要： The subject of the invention is a process for the manufacture of water-soluble condensation products of hydroxymethylphosphonium compounds and thiourea or biuret, characterised in that (a) one mol of a tetrakis-(hydroxymethyl)-phosphonium compound is condensed with (b) 0.02 to 0.5 mol, preferably 0.1 to 0.3 mol, of optionally methylolated thiourea or biuret at 40.degree. to 120.degree.C, optionally in the presence of formaldehyde or a formaldehyde-releasing agent and optionally in the presence of an inert organic solvent, the condensation is optionally thereafter continued at temperatures of 100.degree. to 150.degree.C and, if appropriate, free hydroxyl groups are etherified at least partially with at least one alkanol with 1 to 4 carbon atoms and, if appropriate, the salts of the condensation products are converted into the corresponding hydroxides. In addition to the preferred molar ratio range of 1:0.1 to 0.3, the range of 0.2 to 0.5 is also advantageous.The condensation products are used for flameproofing organic fibre material, especially textiles.
摘要翻译：本发明的主题是制备羟甲基鏻化合物和硫脲或缩二脲的水溶性缩合产物的方法，其特征在于（a）一摩尔四（羟甲基）鏻化合物与（b）0.02 至少0.5mol，优选0.1至0.3mol的任选的羟甲基化硫脲或缩二脲在40至120℃下，任选地在甲醛或甲醛释放剂存在下，任选地在惰性有机溶剂的存在下，然后任选地在100℃至150℃的温度下继续进行，如果合适，游离羟基至少部分用至少一个具有1至4个碳原子的链烷醇醚化，并且如果合适，将缩合产物的盐转化为相应的氢氧化物。除了优选的摩尔比范围为1:0.1至0.3之外，0.2至0.5的范围也是有利的。

9. 发明授权

US4921535A Heat-sensitive recording material 失效
标题翻译：热敏记录材料
公开(公告)号：US4921535A
公开(公告)日：1990-05-01
申请号：US205877
申请日：1988-06-13
申请人： Hermann Nachbur , Rosalinde Braun
发明人： Hermann Nachbur , Rosalinde Braun
IPC分类号： B41M5/337
CPC分类号： B41M5/3375
摘要： A heat-sensitive recording material whose color reactant system comprises a color former, a developer for said color former and, in addition, a sulfamide compound of formula ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are each independently hydrogen, alkyl containing not more than 12 carbon atoms which is unsubstituted or substituted by halogen, hydroxy, cyano or lower alkoxy; C.sub.5 -C.sub.10 cycloalkyl; phenalkyl, phenyl or naphthyl, each unsubstituted or ring-substituted by halogen, cyano, lower alkyl or lower alkoxy, or --NR.sub.2 R.sub.3 is 5- or 6-membered, preferably saturated, heterocyclic radical; with the proviso that R.sub.1, R.sub.2 and R.sub.3 may not simultaneously by hydrogen.
摘要翻译：一种热敏记录材料，其着色反应物体系包含成色剂，用于所述成色剂的显色剂，另外还有式（1）的磺酰胺化合物，其中R 1，R 2和R 3各自独立地为氢，含有不超过12个未被取代或被卤素，羟基，氰基或低级烷氧基取代的碳原子; C5-C10环烷基; 苯基或萘基，各自未被取代或被卤素，氰基，低级烷基或低级烷氧基环取代，或-NR2R3是5-或6-元，优选饱和的杂环基; 条件是R1，R2和R3不能同时被氢。

10. 发明授权

US4754063A Salicylates and process for their preparation 失效
标题翻译：水杨酸盐及其制备方法
公开(公告)号：US4754063A
公开(公告)日：1988-06-28
申请号：US51782
申请日：1987-05-20
申请人： Hermann Nachbur
发明人： Hermann Nachbur
IPC分类号： B41M5/155 , B41M5/333 , C07C51/353 , C07C51/41 , C07C65/105 , C08G61/02 , C07F3/06
CPC分类号： C07C65/105 , B41M5/155 , B41M5/3335
摘要： The invention relates to metal salicylates of the formula ##STR1## wherein Me is a metal ion of valency n,n is 2, 3 or 4, andeach of the rings A and B independently of the other is unsubstituted or substituted by halogen, lower alkyl, lower alkoxy or an .alpha.-methylbenzyl radical.The metal salicylates are particularly suitable developers for the color former in pressure-sensitive or heat-sensitive recording materials.
摘要翻译：本发明涉及下式的金属水杨酸盐，其中Me是价数n，n为2,3或4的金属离子，并且环A和B各自独立地为未被取代或被卤素取代，低级烷基，低级烷氧基或α-甲基苄基。金属水杨酸盐是用于压敏或热敏记录材料中的成色剂的特别合适的显影剂。

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