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1. 发明申请

US20060041122A1 Method for purifying caprolactam 有权
标题翻译：己内酰胺纯化方法
公开(公告)号：US20060041122A1
公开(公告)日：2006-02-23
申请号：US10534802
申请日：2003-11-11
申请人： Rolf-Hartmuth Fischer , Hermann Luyken , Andreas Ansmann , Peter Babler , Christoph Benisch , Stefan Maixner , Johann-Peter Melder
发明人： Rolf-Hartmuth Fischer , Hermann Luyken , Andreas Ansmann , Peter Babler , Christoph Benisch , Stefan Maixner , Johann-Peter Melder
IPC分类号： C07D201/16
CPC分类号： C07D201/16 , C07D201/08
摘要： A process for removing high boilers from crude caprolactam which comprises high boilers, caprolactam and in some cases low boilers, and which has been obtained by a) reacting 6-aminocapronitrile with water to give a reaction mixture b) removing ammonia and unconverted water from the reaction mixture to obtain crude caprolactam, which comprises c) feeding the crude caprolactam to a distillation apparatus to obtain a first substream via the top as a product and a second substream via the bottom, by setting the pressure in the distillation in such a way that the bottom temperature does not go below 170° C., and adjusting the second substream in such a way that the caprolactam content of the second substream is not less than 10% by weight, based on the entire second substream.
摘要翻译：一种从粗己内酰胺中除去高锅炉的方法，其包括高锅炉，己内酰胺，在某些情况下是低锅炉，并且通过以下方法获得：a）使6-氨基己腈与水反应得到反应混合物; b）除去氨和未转化的水反应混合物以获得粗己内酰胺，其包括c）将粗己内酰胺加入到蒸馏装置中，通过顶部获得第一子流作为产物，通过底部通过设置第二子流，通过将蒸馏中的压力设定为使得底部温度不低于170℃，并且调节第二子流，使得第二子流的己内酰胺含量基于整个第二子流不小于10重量％。

2. 发明申请

US20060090994A1 Method for purifying caprolactam 失效
标题翻译：己内酰胺纯化方法
公开(公告)号：US20060090994A1
公开(公告)日：2006-05-04
申请号：US10534822
申请日：2003-11-11
申请人： Hermann Luyken , Andreas Ansmann , Christoph Benisch , Peter Babler , Rolf-Hartmuth Fischer , Stefan Maixner , Johann-Peter Melder
发明人： Hermann Luyken , Andreas Ansmann , Christoph Benisch , Peter Babler , Rolf-Hartmuth Fischer , Stefan Maixner , Johann-Peter Melder
IPC分类号： B01D3/34 , C07C51/44
CPC分类号： C07D201/16
摘要： A process for purifying crude caprolactam which has been obtained by 1) converting a mixture (I) comprising 6-aminocapronitrile and water to a mixture (II) comprising caprolactam, ammonia, water, high boilers and low boilers in the presence of a catalyst, then 2) removing ammonia from mixture (II) to obtain a mixture (III) comprising caprolactam, water, high boilers and low boilers, then 3) completely or partly removing water from mixture (III) to obtain crude caprolactam (IV) comprising caprolactam, high boilers and low boilers, which comprises a) feeding the crude caprolactam and an inorganic acid which has a boiling point above the boiling point of caprolactam under the distillation conditions of the following steps b) to h) to a first distillation apparatus C1, b) distilling the crude caprolactam and the inorganic acid in the first distillation apparatus C1, and removing a first substream in the bottom region and a second substream in the top region of the distillation apparatus C1, c) feeding the second substream from step b) to a second distillation apparatus C2, d) distilling the second substream from step b) in the second distillation apparatus C2, and removing a first substream in the bottom region and a second substream in the top region of the distillation apparatus C2, e) feeding the first substream from step d) to a third distillation apparatus C3, f) distilling the first substream from d) in the third distillation apparatus C3, and removing a first substream in the bottom region and purified caprolactam in the top region of distillation apparatus C3, and g) feeding the first substream from step f) to the first distillation apparatus C1.
摘要翻译：一种纯化己内酰胺的方法，其通过以下步骤获得：1）在催化剂存在下，将包含6-氨基己腈和水的混合物（I）转化为包含己内酰胺，氨，水，高锅炉和低沸点的混合物（II）然后2）从混合物（II）中除去氨以获得包含己内酰胺，水，高锅炉和低锅炉的混合物（III），然后3）从混合物（III）中完全或部分除去水，得到包含己内酰胺的粗己内酰胺（IV），高沸点锅炉和低锅炉，其包括：a）在第一蒸馏装置C1的下述步骤b）至h）的蒸馏条件下，将粗己内酰胺和沸点高于己内酰胺沸点的无机酸， b）在第一蒸馏装置C1中蒸馏粗己内酰胺和无机酸，并且除去蒸馏装置C1的顶部区域中的第一子流和顶部区域中的第二子流 c）将来自步骤b）的第二子流进料到第二蒸馏装置C2，d）在第二蒸馏装置C2中蒸馏步骤b）中的第二子流，并且除去第二蒸馏装置C2中的第一子流， e）蒸馏装置C2的顶部区域，e）将来自步骤d）的第一子流进料到第三蒸馏装置C3，f）将第一子流从d）蒸馏到第三蒸馏装置C3中，并且除去底部区域中的第一子流和在蒸馏装置C3的顶部区域中纯化的己内酰胺，并且g）将来自步骤f）的第一子流进料到第一蒸馏装置C1。

3. 发明申请

US20060110309A1 Hydrocyanic acid consisting of formamide 有权
标题翻译：氢氰酸由甲酰胺组成
公开(公告)号：US20060110309A1
公开(公告)日：2006-05-25
申请号：US10537820
申请日：2003-12-03
申请人： Peter Babler , Wolfgang Siegel , Gunther Achhammer , Anton Negele , Helmuth Menig , Wilhelm Ruppel , Peter Zehmer , Hermann Luyken , Wolker Vogt
发明人： Peter Babler , Wolfgang Siegel , Gunther Achhammer , Anton Negele , Helmuth Menig , Wilhelm Ruppel , Peter Zehmer , Hermann Luyken , Wolker Vogt
IPC分类号： B01D53/14 , C01C3/02
CPC分类号： C01C3/0204 , B01J12/007 , B01J15/005 , B01J19/02 , B01J19/2415 , B01J23/866 , B01J2219/00135 , B01J2219/0236
摘要： The present invention relates to a process for preparing hydrocyanic acid (HCN) by catalytic dehydration of gaseous formamide in a reactor which has an internal reactor surface made of a steel comprising iron and chromium and nickel, and also to a reactor for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide, which reactor has an internal reactor surface made of a steel comprising iron and chromium and nickel, and also to the use of the reactor of the present invention in a process for preparing hydrocyanic acid by catalytic dehydration of gaseous formamide.
摘要翻译：本发明涉及一种通过在反应器中催化脱水气态甲酰胺制备氢氰酸（HCN）的方法，该反应器具有由含铁和铬和镍的钢制成的内部反应器表面，并且还涉及通过以下步骤制备氢氰酸的反应器气态甲酰胺的催化脱水，该反应器具有由包含铁和铬和镍的钢制成的内部反应器表面，以及本发明的反应器在通过气态甲酰胺的催化脱水制备氢氰酸的方法中的用途。

4. 发明申请

US20060014629A1 Catalyst for epoxidation reactions 审中-公开
标题翻译：催化剂用于环氧化反应
公开(公告)号：US20060014629A1
公开(公告)日：2006-01-19
申请号：US10526353
申请日：2003-09-15
申请人： Ulrich Mueller , Georg Krug , Peter Babler , Hans- Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Mueller , Georg Krug , Peter Babler , Hans- Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： B01J29/06
CPC分类号： C07D301/12 , B01J29/89
摘要： The present invention relates to the manufacture of solid materials or shaped bodies containing at least one zeolite and being at least partly crystalline. Furthermore, the present invention relates to the solid materials or shaped bodies as such and to the use of these materials for reactions of compounds having at least one C—C double bond with at least one hydroperoxide. Specifically, the present invention relates to a process for the manufacture of a solid material containing at least one zeolite and being at least partly crystalline, wherein the synthesis of the said solid material involves at least one partial step of contacting at least one transition metal oxide source with at least one epoxide or hydrolysate thereof prior to or during the at least partial crystallization of said solid material.
摘要翻译：本发明涉及包含至少一种沸石并且至少部分结晶的固体材料或成形体的制造。此外，本发明还涉及固体材料或成形体，以及这些材料用于具有至少一个C-C双键的化合物与至少一种氢过氧化物的反应的用途。具体地说，本发明涉及制造含有至少一种沸石并且至少部分结晶的固体材料的方法，其中所述固体材料的合成涉及至少一个部分步骤，使至少一种过渡金属氧化物来源，其在所述固体材料的至少部分结晶之前或期间具有至少一种环氧化物或水解产物。

5. 发明申请

US20060025637A1 Method for the continuous production of proplyene glycol 失效
标题翻译：连续生产丙二醇的方法
公开(公告)号：US20060025637A1
公开(公告)日：2006-02-02
申请号：US10521467
申请日：2003-07-22
申请人： Peter Babler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
发明人： Peter Babler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
IPC分类号： C07C31/02
CPC分类号： B01D3/141 , B01D3/143 , C07C29/106 , C07D301/12 , C07C31/205
摘要： Process for the continuous preparation of propylene glycols, which comprises the steps (i) to (ii): (i) reacting propylene with hydrogen peroxide to form propylene oxide and give propylene glycols as by-products, (ii) reacting the propylene oxide obtained in step (i) with water to give propylene glycols, (iii) separating off the propylene glycols obtained in steps (i) and (ii).
摘要翻译：用于连续制备丙二醇的方法，其包括步骤（i）至（ii）：（i）使丙烯与过氧化氢反应以形成环氧丙烷并产生作为副产物的丙二醇，（ii）使获得的环氧丙烷在步骤（i）中用水进行丙二醇，（iii）分离步骤（i）和（ii）中获得的丙二醇。

6. 发明申请

US20060058539A1 Returning an olefin which is not reacted during the oxidation of olefins 有权
标题翻译：回收在烯烃氧化过程中不反应的烯烃
公开(公告)号：US20060058539A1
公开(公告)日：2006-03-16
申请号：US10532096
申请日：2003-10-23
申请人： Peter Babler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
发明人： Peter Babler , Hans-Georg Gobbel , Joaquim Teles , Peter Rudolf
IPC分类号： C07D301/19
CPC分类号： C07D301/12
摘要： The invention relates to a method for continuously returning an olefin which has not been reacted with hydroperoxide in order to form oxiranes during the epoxidation of olefins. Said olefin is contained in the flow of waste gas which is produced during epoxidation. Said method is characterised by the following steps: (i) compressing and cooling the flow of waste gas, (ii) separating the olefin from the flow of waste gas obtained in step (i) by distillation,(iii) epoxidating the olefin separated in (ii) with hydroperoxide.
摘要翻译：本发明涉及在烯烃环氧化期间连续返回未与氢过氧化物反应的烯烃以形成环氧乙烷的方法。所述烯烃包含在环氧化过程中产生的废气流中。所述方法的特征在于以下步骤：（i）压缩和冷却废气流，（ii）通过蒸馏从步骤（i）获得的废气流中分离烯烃，（iii）将分离的烯烃环氧化（ii）加氢过氧化物。

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