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1. 发明授权

US5725607A Method for reducing the toxicity of spent liquors and novel cationic dyes 失效
公开(公告)号：US5725607A
公开(公告)日：1998-03-10
申请号：US670045
申请日：1996-06-25
申请人： Henry Giera , Felix Reichel , Horst Berneth , Thomas Bocker , Karin Hassenruck , Karl Lange , Karlheinrich Meisel
发明人： Henry Giera , Felix Reichel , Horst Berneth , Thomas Bocker , Karin Hassenruck , Karl Lange , Karlheinrich Meisel
IPC分类号： C07D249/06 , C07D213/38 , C07D231/56 , C07D249/14 , C07D277/20 , C07D277/50 , C07D409/04 , C09B23/14 , C09B23/16 , C09B26/04 , C09B44/10 , C09B44/20 , C09B55/00 , C09B57/00 , D06P1/00 , D06P1/41
CPC分类号： C09B23/143 , C09B23/145 , C09B23/164 , C09B26/04 , C09B44/10 , D06P1/41 , Y10S8/917 , Y10S8/919 , Y10S8/922 , Y10S8/924 , Y10S8/927
摘要： There has been found 1) a method for reducing the toxicity of spent liquors from dyeing with cationic dyes or mixtures thereof, characterized by the step of dyeing with cationic dyes having a computed electrostatic shielding energy (idealized hydration energy) of .gtoreq.50 kcal/mol, 2) cationic, generally low toxicity dyes, their preparation and use for dyeing.

2. 发明授权

US5869731A Method for reducing the toxicity of spent liquors and novel cationic dyes 失效
标题翻译：降低废液和新型阳离子染料毒性的方法
公开(公告)号：US5869731A
公开(公告)日：1999-02-09
申请号：US937289
申请日：1997-09-25
申请人： Henry Giera , Felix Reichel , Horst Berneth
发明人： Henry Giera , Felix Reichel , Horst Berneth
IPC分类号： C07D249/06 , C07D213/38 , C07D231/56 , C07D249/14 , C07D277/20 , C07D277/50 , C07D409/04 , C09B23/14 , C09B23/16 , C09B26/04 , C09B44/10 , C09B44/20 , C09B55/00 , C09B57/00 , D06P1/00 , D06P1/41 , C09D11/00 , D06P3/32 , D21H21/28
CPC分类号： C09B23/143 , C09B23/145 , C09B23/164 , C09B26/04 , C09B44/10 , D06P1/41 , Y10S8/917 , Y10S8/919 , Y10S8/922 , Y10S8/924 , Y10S8/927
摘要： There has been found1) a method for reducing the toxicity of spent liquors from dyeing with cationic dyes or mixtures thereof, characterized by the step of dyeing with cationic dyes having a computed electrostatic shielding energy (idealized hydration energy) of .gtoreq.50 kcal/mol,2) cationic, generally low toxicity dyes, their preparation and use for dyeing.
摘要翻译：已经发现1）一种用于降低用阳离子染料或其混合物染色的废液的毒性的方法，其特征在于用阳离子染料染色的步骤，所述阳离子染料具有计算的静电屏蔽能量（理想化水合能量）> 50kcal / mol，2）阳离子，一般低毒性染料，其制备和用途用于染色。

3. 发明授权

US5866353A Electro chemical biosensor containing diazacyanine mediator for co-enzyme regeneration 失效
标题翻译：含有二氮芥酸介质的电化学生物传感器用于辅酶再生
公开(公告)号：US5866353A
公开(公告)日：1999-02-02
申请号：US762098
申请日：1996-12-09
申请人： Horst Berneth , Thomas Bocker , Henry Giera , Alison J. Murray , Hans-Ulrich Siegmund
发明人： Horst Berneth , Thomas Bocker , Henry Giera , Alison J. Murray , Hans-Ulrich Siegmund
IPC分类号： G01N27/327 , C12Q1/00 , C12Q1/32 , C09B44/10 , C12M1/00 , G01N27/26
CPC分类号： C12Q1/004 , Y10S435/817
摘要： A variety of diazacyanine mediators that are soluble in aqueous media and which do not inhibit enzymatic activity are provided for use on the surface of a working electrode of a electrochemical biosensor for electrochemical co-enzyme regeneration. The co-enzyme, dihydronicotinamide adenine dinucleotide (NADH) or dihydronicotinamide adenine dinucleotide phosphate (NADPH), is oxidized to NAD.sup.+ OR NADP.sup.+ which is reduced by an oxidoreductase such as a dehydrogenase acting on a substrate. By applying the mediator together with NADH or NADPH to the surface of the working electrode, the voltage necessary to achieve oxidation is substantially reduced. Biosensor electrodes such as graphite electrodes may be produced-by screen printing techniques.
摘要翻译：提供了可溶于水性介质并且不抑制酶活性的各种二氮芥酸介质用于电化学生物传感器用于电化学辅酶再生的工作电极的表面。辅酶，二氢烟酰胺腺嘌呤二核苷酸（NADH）或二氢烟酰胺腺嘌呤二核苷酸磷酸（NADPH）被氧化成NAD + OR NADP +，其由氧化还原酶例如作用于底物的脱氢酶而还原。通过将介体与NADH或NADPH一起施加到工作电极的表面，实现氧化所需的电压显着降低。生物传感器电极如石墨电极可以通过丝网印刷技术制造。

4. 发明授权

US5749925A Dyeing or printing process with new and known cationic 4,5-dihydro-iH-1,2,3-triazolium compounds as dyestuffs and new cationic 4,5-dihydro-1H-1,2,3-triazolium compounds 失效
标题翻译：新的和已知的阳离子4,5-二氢-h-1,2,3-三唑鎓化合物作为染料和新的阳离子4,5-二氢-1H-1,2,3-三唑鎓化合物的染色或印刷方法
公开(公告)号：US5749925A
公开(公告)日：1998-05-12
申请号：US670913
申请日：1996-06-26
申请人： Thomas Bocker , Horst Berneth , Henry Giera
发明人： Thomas Bocker , Horst Berneth , Henry Giera
IPC分类号： C07D249/06 , C07D417/04 , C09B26/06 , C09B57/00 , D06P3/24 , D06P3/32 , D06P3/52 , D06P3/70 , D06P1/42 , D06P3/76
CPC分类号： C07D417/04 , C07D249/06 , C09B26/06 , C09B57/00 , Y10S8/917 , Y10S8/918 , Y10S8/919 , Y10S8/927
摘要： 4,5-Dihydro-1H-1,2,3-triazolium compounds of the formula (I) ##STR1## in which R.sup.1 and R.sup.2 independently of one another denote C.sub.6 -C.sub.14 -aryl or a heterocyclic radical having up to 3 rings and up to 4 heteroatoms from the series consisting of O, S and N, R.sup.3 and R.sup.4 independently of one another denote hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.2 -C.sub.12 -alkenyl, C.sub.4 -C.sub.8 -cycloalkyl, C.sub.7 -C.sub.17 -aralkyl, C.sub.6 -C.sub.14 -aryl or nitrile or R.sup.3 and R.sup.4 together denote a 2- to 5-membered C bridge, which can optionally be interrupted by up to two oxygen and/or nitrogen atoms, and X.sup.- denotes an anion, wherein all the alkyl, alkenyl, cycloalkyl, aralkyl and aryl radicals and fused and heterocyclic radicals present can optionally be substituted by nonionic substituents, carboxyl groups, ammonium groups and/or pyridinium groups, are used as dyestuffs. New 4,5-dihydro-1H-1,2,3-triazolium compounds correspond to the formula (I), with the provisos that if R.sup.3 and R.sup.4 in each case denote hydrogen then in the case where R.sup.1 =4-methylphenyl R.sup.2 does not represent 4-nitrophenyl, 4-methoxyphenyl or phenyl and R.sup.1 and R.sup.2 do not both simultaneously represent 4-methylphenyl, 4-nitrophenyl, 4-methoxyphenyl or phenyl.
摘要翻译： R 1和R 2彼此独立地表示的式（I）的化合物（I）的4,5-二氢-1H-1,2,3-三唑鎓表示C 6 -C 14 - 芳基或具有至多 3个环和至多4个由O，S和N组成的系列的杂原子，R 3和R 4彼此独立地表示氢，C 1 -C 12 - 烷基，C 2 -C 12 - 链烯基，C 4 -C 8环烷基，C 7 -C 17 - 芳烷基，C 6 -C 14 - 芳基或腈，或者R 3和R 4一起表示2-至5-元C桥，其可以任选地被多达两个氧和/或氮原子间隔，X-表示阴离子，其中所有存在的烷基，烯基，环烷基，芳烷基和芳基以及稠合和杂环基团可任选被非离子取代基，羧基，铵基和/或吡啶鎓基取代，用作染料。新的4,5-二氢-1H-1,2,3-三唑鎓化合物对应于式（I），条件是如果R 3和R 4在每种情况下表示氢，则在R1 = 4-甲基苯基R2的情况下不代表4-硝基苯基，4-甲氧基苯基或苯基，R1和R2不同时表示4-甲基苯基，4-硝基苯基，4-甲氧基苯基或苯基。

5. 发明授权

US4968797A Chromogenic 4,4-diaryldihydroquinazolones 失效
标题翻译：显色的4,4-二芳基二氢喹唑啉酮
公开(公告)号：US4968797A
公开(公告)日：1990-11-06
申请号：US115137
申请日：1987-10-30
申请人： Horst Berneth , Alfred Brack , Karlheinrich Meisel
发明人： Horst Berneth , Alfred Brack , Karlheinrich Meisel
IPC分类号： B41M5/323 , B41M5/136 , C07C275/46 , C07C275/50 , C07C275/54 , C07C311/61 , C07D239/82 , C07D401/06 , C07D401/12 , C07D403/04 , C07D403/06 , C07D403/10 , C07D413/06 , C09B11/00 , C09B11/04
CPC分类号： C07D401/06 , B41M5/136 , C07C275/46 , C07C275/50 , C07C275/54 , C07C311/61 , C07D239/82 , C07D401/12 , C07D403/06 , C07D403/10 , C07D413/06 , C09B11/04
摘要： 4,4-diaryldihydroquinazolones of the formula ##STR1## wherein X.sup.1, X.sup.2 and X.sup.3, independently of one another, denote hydrogen, halogen, alkyl, aryl, alkanoylamino, aroylamino, heteryl, NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3, at least one of the radicalsX.sup.1, X.sup.2 or X.sup.3 standing for NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3,R.sup.1 denotes hydrogen, alkyl, cycloalkyl, aralkyl, aryl or the members of a bridge to the o-carbon of ring C,R.sup.2 denotes a radical of an acid,Y.sup.1, Y.sup.2 and Y.sup.3, independently of one another, denote hydrogen, alkyl, cycloalkyl, aralkyl aryl or heteryl or the remaining members of a 5- or 6-membered ring which reaches to one of the o-position benzene C atoms and may contain further hetero atoms orY.sup.1 +Y.sup.2 denote the remaining members of a 5- or 6-membered ring which may contain further hetero atoms andthe rings A, B and C and the radicals mentioned can in turn carry nonionic substituents customary in dye-stuff chemistry, find utility in pressure-copyable thermoreactive and electrochromic recording materials.

6. 发明授权

US4754034A Chromogenic 4,4-diaryldihydroquinazolones 失效
标题翻译：显色的4,4-二芳基二氢喹唑啉酮
公开(公告)号：US4754034A
公开(公告)日：1988-06-28
申请号：US789686
申请日：1985-10-21
申请人： Horst Berneth , Alfred Brack , Karlheinrich Meisel
发明人： Horst Berneth , Alfred Brack , Karlheinrich Meisel
IPC分类号： B41M5/323 , B41M5/136 , C07C275/46 , C07C275/50 , C07C275/54 , C07C311/61 , C07D239/82 , C07D401/06 , C07D401/12 , C07D403/04 , C07D403/06 , C07D403/10 , C07D413/06 , C09B11/00 , C09B11/04 , C07D239/80
CPC分类号： C07D401/06 , B41M5/136 , C07C275/46 , C07C275/50 , C07C275/54 , C07C311/61 , C07D239/82 , C07D401/12 , C07D403/06 , C07D403/10 , C07D413/06 , C09B11/04
摘要： 4,4-diaryldihydroquinazolones of the formula ##STR1## wherein X.sup.1, X.sup.2 and X.sup.3, independently of one another, denote hydrogen, halogen, alkyl, aryl, alkanoylamino, aroylamino, heteryl, NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3, at least one of the radicals X.sup.1, X.sup.2 or X.sup.3 standing for NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3,R.sup.1 denotes hydrogen, alkyl, cycloalkyl, aralkyl, aryl or the members of a bridge to the o-carbon of ring C,R.sup.2 denotes a radical of an acid,Y.sup.1, Y.sup.2 and Y.sup.3, independently of one another, denote hydrogen, alkyl, cycloalkyl, aralkyl aryl or heteryl or the remaining members of a 5- or 6-membered ring which reaches to one of the o-position benzene C atoms and may contain further hetero atoms orY.sup.1 +Y.sup.2 denote the remaining members of a 5- or 6-membered ring which may contain further hetero atoms andthe rings A, B and C and the radicals mentioned can in turn carry nonionic substituents customary in dye-stuff chemistry, find utility in pressure-copyable thermoreactive and electrochromic recording materials.
摘要翻译：式（I）的4-二芳基二氢喹唑啉酮其中X 1，X 2和X 3彼此独立地表示氢，卤素，烷基，芳基，烷酰基氨基，芳酰氨基，异酰基，NY1Y2，OY3或SY3，至少一个的基团X 1，X 2或X 3代表NY1Y2，OY3或SY3，R1表示氢，烷基，环烷基，芳烷基，芳基或与环C的邻碳的桥的成员，R2表示酸的基团， Y 1，Y 2和Y 3彼此独立地表示氢，烷基，环烷基，芳烷基芳基或杂芳基或5-位或6-元环的其余成员，其到达位置苯C原子之一并且可以含有另外的杂原子或Y1 + Y2表示可含有更多杂原子的5或6元环的剩余成员，并且环A，B和C以及所提及的基团可以依次携带染料化学中常规的非离子取代基，可用于压力可复制的热反应和电致变色记录材料。

7. 发明授权

US4727140A Chromogenic 4,4-diaryl-2-oxobenzo-3,1-oxazines 失效
标题翻译：显色的4,4-二芳基-2-氧代苯并-3,1-恶嗪
公开(公告)号：US4727140A
公开(公告)日：1988-02-23
申请号：US789802
申请日：1985-10-21
申请人： Karlheinrich Meisel , Horst Berneth
发明人： Karlheinrich Meisel , Horst Berneth
IPC分类号： B41M5/323 , B41M5/136 , C07D265/18 , C07D413/04 , C09B11/04 , C09B19/00
CPC分类号： C07D265/18 , B41M5/136 , C07D413/04 , C09B11/04
摘要： 4,4-Diaryl-2-oxobenzo-3,1-oxazines of the general formula ##STR1## wherein X.sup.1, X.sup.2 and X.sup.3, independently of one another, denote hydrogen, halogen, alkyl, aryl, alkanoylamino, aroylamino, heteryl, NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3,at least one of the radicals X.sup.1, X.sup.2 or X.sup.3 standing for NY.sup.1 Y.sup.2, OY.sup.3 or SY.sup.3,R.sup.1 denotes hydrogen, alkyl, cycloalkyl, aralkyl, aryl or the members of a bridge to the o-carbon of ring B,Y.sup.1, Y.sup.2 and Y.sup.3, independently of one another, denote hydrogen, alkyl, cycloalkyl, aralkyl or aryl or the remaining members of a 5- or 6-membered ring which reaches to one of the o-position benzene C atoms and may contain further heteroatoms or Y.sup.1 +Y.sup.2 denote the remaining members of a 5- or 6-membered ring which may contain further heteroatoms andthe rings A, B and C and the radicals mentioned can in turn carry nonionic substituents customary in dyestuff chemistry, find utility in pressure-copyable and thermoreactive recording materials.
摘要翻译：通式为其中X 1，X 2和X 3彼此独立地表示氢，卤素，烷基，芳基，烷酰基氨基，芳酰基氨基，芳酰基氨基，杂芳基，NY1Y2，OY3或SY3，代表NY1Y2，OY3或SY3的基团X1，X2或X3中的至少一个，R1表示氢，烷基，环烷基，芳烷基，芳基或与O- 环B，Y 1，Y 2和Y 3彼此独立地表示氢，烷基，环烷基，芳烷基或芳基或5-位或6-元环的其余成员，其至少一个位于邻位苯C原子之一和可以含有另外的杂原子，或Y1 + Y2表示可含有其它杂原子的5或6元环的剩余成员，并且环A，B和C和所提及的基团可以依次携带染料化学中常规的非离子取代基，发现在压力复制和热反应记录材料中的应用。

8. 发明申请

US20070042295A1 Optical data carrier comprising a polymeric network in the information layer 审中-公开
标题翻译：光学数据载体包括信息层中的聚合物网络
公开(公告)号：US20070042295A1
公开(公告)日：2007-02-22
申请号：US10549100
申请日：2004-03-12
申请人： Horst Berneth , Friedrich-Karl Bruder , Rainer Hagen , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Rafael Oser , Josef-Walter Stawitz
发明人： Horst Berneth , Friedrich-Karl Bruder , Rainer Hagen , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Rafael Oser , Josef-Walter Stawitz
IPC分类号： G11B7/24
CPC分类号： G11B7/245
摘要： Optical data carriers having at least one information layer which comprises a polymeric network comprising covalently bound light-absorbent compounds.
摘要翻译：具有至少一个信息层的光学数据载体包括聚合物网络，其包含共价结合的吸光性化合物。

9. 发明授权

US6008350A Process for the production of cyanine dyes 失效
标题翻译：花青染料的生产工艺
公开(公告)号：US6008350A
公开(公告)日：1999-12-28
申请号：US612870
申请日：1996-03-13
申请人： Peter Roschger , Stephan Michaelis , Karin Hassenruck , Horst Berneth , Paul Callant
发明人： Peter Roschger , Stephan Michaelis , Karin Hassenruck , Horst Berneth , Paul Callant
IPC分类号： B41M5/385 , B41M5/24 , B41M5/30 , B41M5/32 , B41M5/337 , B41M5/388 , B41M5/39 , B41M5/40 , B41M5/42 , B41M5/46 , C07D209/14 , C07D209/90 , C07D309/34 , C07D335/02 , C07D335/04 , C07D401/14 , C07D403/14 , C07D405/14 , C07D409/14 , C07D413/06 , C09B23/00 , C09B23/01 , G03C1/12 , G03C1/498 , C09B23/12 , C07D403/08
CPC分类号： B41M5/3375 , B41M5/32 , B41M5/42 , B41M5/465 , C09B23/0008 , C09B23/0066 , G03C1/127 , G03C1/49827 , G03C1/49854 , G03C1/4989 , B41M5/24 , G03C5/164 , Y10S430/145 , Y10S430/146
摘要： The present invention relates to a process for the production of cyanine dyes with their methine chain showing group (M) and the charge compensation occuring by linked end groups through transformation of cationic cyanine dyes comprising group (D) with CH-acid compounds of the following formula (I) B.sub.1 --CH.sub.2 --B.sub.2 in an inert solvent, the substituents having the significance given in the description. ##STR1##
摘要翻译： PCT No.PCT / EP94 / 02975第 371日期：1996年3月13日 102（e）1996年3月13日PCT 1994年9月6日PCT PCT。出版物WO95 / 07950 日期：1995年3月23日本发明涉及通过将包含（D）基团的阳离子花青染料与CH-基团的转化，生成具有显示组（M）的次甲基链的花青染料和连接端基产生的电荷补偿的方法，在惰性溶剂中下式（I）B1-CH2-B2的酸化合物，该取代基在描述中给出了重要性。

10. 发明申请

US20060292326A1 Optical data store comprising a cobalt phthalocyanine with an axial substituent and axial ligand in an information photoinscribtible layer 审中-公开
标题翻译：光学数据存储器，其包含在信息光可分层中具有轴向取代基的钴酞菁和轴向配体
公开(公告)号：US20060292326A1
公开(公告)日：2006-12-28
申请号：US10534849
申请日：2003-11-04
申请人： Horst Berneth , Friedrich Bruder , Wilfried Haese , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Josef-Walter Stawitz , Rafael Oser , Rainer Hagen
发明人： Horst Berneth , Friedrich Bruder , Wilfried Haese , Karin Hassenruck , Serguei Kostromine , Christa Kruger , Timo Meyer-Friedrichsen , Josef-Walter Stawitz , Rafael Oser , Rainer Hagen
IPC分类号： B32B3/02
CPC分类号： G11B7/248 , C09B47/08 , C09B67/0035
摘要： Optical data carriers whose information layer comprises at least one light-absorbent compound which is a Co(III) phthalocyanine in which the Co metal centre bears an axial substituent R1 and an axial coordinated ligand R2, where R1 is CN, SCN, halogen, in particular Cl, Br or F, alkoxy, aryloxy, arylthio or alkylthio and R2 is no ligand or substituted or unsubstituted amine, water, an alcohol, H2S, a thioalcohol or an isonitrile.
摘要翻译：光学数据载体，其信息层包含至少一种吸光性化合物，其为Co（III）酞菁，其中Co金属中心具有轴向取代基R 1和轴向配位配位体R 0， 2，其中R 1是CN，SCN，卤素，特别是Cl，Br或F，烷氧基，芳氧基，芳硫基或烷硫基，R 2不是配体或取代或未取代的胺，水，醇，H 2 S，硫代醇或异腈。

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