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1. 发明授权

US5006659A Preparation of 7-chloroquinoline-8-carboxylic acids 失效
标题翻译： 7-氯喹啉-8-羧酸的制备
公开(公告)号：US5006659A
公开(公告)日：1991-04-09
申请号：US464568
申请日：1990-01-16
申请人： Helmut Hagen , Jacques Dupuis , Heinz Eilingsfeld
发明人： Helmut Hagen , Jacques Dupuis , Heinz Eilingsfeld
IPC分类号： C07D215/48
CPC分类号： C07D215/48
摘要： 7-Chloroquinoline-8-carboxylic acids of the formula (I) ##STR1## where R is hydrogen, chlorine or methyl, are prepared by direct oxidation of the corresponding 8-methylqunoline compound with nitric acid or nitrogen oxide in the presence of sulfuric acid and a heavy metal catalyst.
摘要翻译：存在式（I）的7-氯喹啉-8-羧酸，其中R是氢，氯或甲基，是通过在硝基或氮氧化物存在下直接氧化相应的8-甲基均聚物化合物的硫酸和重金属催化剂。

2. 发明授权

US4533612A Electrophotographic recording materials containing special charge carrier-transporting compounds 失效
标题翻译：含有特殊电荷载体输送化合物的电子照相记录材料
公开(公告)号：US4533612A
公开(公告)日：1985-08-06
申请号：US675264
申请日：1984-11-27
申请人： Heinz Eilingsfeld , Karl-Heinz Etzbach , Gerhard Hoffmann , Peter Neumann
发明人： Heinz Eilingsfeld , Karl-Heinz Etzbach , Gerhard Hoffmann , Peter Neumann
IPC分类号： C07D249/20 , G03G5/06 , G03G5/14
CPC分类号： G03G5/0633 , C07D249/20
摘要： Electrophotographic recording materials which comprise an electrically conductive base, charge carrier-producing compounds (sensitizers), and charge carrier-transporting compounds, possess high photoconductivity and low conductivity in the dark, and contain, as charge carrier-transporting compounds, 2-substituted benzotriazoles of the formula ##STR1## are used for reprographic purposes and for the production of electrophotographic printing plates, in particular offset printing plates.
摘要翻译：包含导电性碱，电荷载体产生化合物（敏化剂）和电荷载流子传输化合物的电子照相记录材料在黑暗中具有高的光电导率和低电导率，并且作为电荷载流子传输化合物含有2-取代的苯并三唑式（I）的化合物用于复制目的和用于生产电子照相印版，特别是胶版印刷版。

3. 发明授权

US4483795A Substituted phenyl disazo dyes containing a 2-amino-substituted thiazole radical 失效
标题翻译：含有2-氨基取代的噻唑基的取代的苯基二偶氮染料
公开(公告)号：US4483795A
公开(公告)日：1984-11-20
申请号：US433887
申请日：1982-10-13
申请人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
发明人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
IPC分类号： C09B31/14 , C09B33/12 , D06P1/18 , D06P3/54
CPC分类号： C09B31/14
摘要： Compounds of the general formula I ##STR1## where D is the radical of a diazo component,R is hydrogen, hydroxy or unsubstituted or substituted alkyl, alkenyl, cycloalkyl, aralkyl, phenyl or heterocyclic ring,R.sup.1 and R.sup.2 independently of one another are hydrogen or unsubstituted or substituted alkyl, alkenyl, alkynyl, cycloalkyl, aralkyl or aryl, orR.sup.1 and R.sup.2 together with the nitrogen are a saturated heterocyclic 5-membered to 7-membered ring,X is hydrogen, chlorine, bromine, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, allyloxy, .beta.-cyanoethoxy, benzyloxy, phenoxy, .beta.-alkoxycarbonylethoxy, where alkoxy is of 1 to 4 carbon atoms, alkylmercapto of 1 to 4 carbon atoms, phenylmercapto or alkanoylamino of 1 to 4 carbon atoms, andY is chlorine, alkyl of 1 to 4 carbon atoms, allyloxy, alkoxy of 1 to 4 carbon atoms or .beta.-cyanoethoxy, orX and Y together are a fused benzene ring which is unsubstituted or substituted by alkyl alkoxy chlorine or bromine.The compounds are in particular suitable for dyeing cotton and union fabrics of cotton and synthetic fibers, preferably polyesters. The dyeings obtained are, in part, very fast.
摘要翻译：通式I的化合物其中D是重氮组分的基团，R是氢，羟基或未取代或取代的烷基，烯基，环烷基，芳烷基，苯基或杂环，R 1和R 2彼此独立地是氢或未取代或取代的烷基，烯基，炔基，环烷基，芳烷基或芳基，或R 1和R 2与氮一起为饱和杂环5元至7元环，X为氢，氯，溴，1至 4个碳原子的烷氧基，1至4个碳原子的烷氧基，烯丙氧基，β-氰基乙氧基，苄氧基，苯氧基，β-烷氧基羰基乙氧基，其中烷氧基为1至4个碳原子，烷基巯基为1至4个碳原子，苯基巯基或烷酰基氨基为1至 4个碳原子，Y为氯，1至4个碳原子的烷基，烯丙氧基，1至4个碳原子的烷氧基或β-氰基乙氧基，或X和Y一起是未被取代或被烷基烷氧基取代的稠合苯环或溴。该化合物特别适用于棉和合成纤维，优选聚酯的棉和联合织物的染色。所获得的染色部分地非常快。

4. 发明授权

US4372885A Bisazo dyes containing a 2-amino-substituted thiazole radical 失效
标题翻译：含有2-氨基取代的噻唑基的双偶氮染料
公开(公告)号：US4372885A
公开(公告)日：1983-02-08
申请号：US931248
申请日：1978-08-04
申请人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
发明人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
IPC分类号： C09B31/14 , D06P1/18 , D06P3/36 , D06P3/54
CPC分类号： C09B31/14
摘要： Compounds of the general formula I ##STR1## where D is the radical of a diazo component,R is hydrogen, hydroxy or unsubstituted or substituted alkyl, alkenyl, cycloalkyl, aralkyl, phenyl or heterocyclic ring,R.sup.1 and R.sup.2 independently of one another are hydrogen or unsubstituted or substituted alkyl, alkenyl, alkynyl, cycloalkyl, aralkyl or aryl, orR.sup.1 and R.sup.2 together with the nitrogen are a saturated heterocyclic 5-membered to 7-membered ring,X is hydrogen, chlorine, bromine, alkyl of 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, allyloxy, .beta.-cyanoethoxy, benzyloxy, phenoxy, .beta.-alkoxycarbonylethoxy, where alkoxy is of 1 to 4 carbon atoms, alkylmercapto of 1 to 4 carbon atoms, phenylmercapto or alkanoylamino of 1 to 4 carbon atoms, andY is chlorine, alkyl of 1 to 4 carbon atoms, allyloxy, alkoxy of 1 to 4 carbon atoms or .beta.-cyanoethoxy, orX and Y together are a fused benzene ring which is unsubstituted or substituted by alkyl, alkoxy, chlorine or bromine.The compounds are in particular suitable for dyeing cotton and union fabrics of cotton and synthetic fibers, preferably polyesters. The dyeings obtained are, in part, very fast.
摘要翻译：通式I的化合物其中D是重氮组分的基团，R是氢，羟基或未取代或取代的烷基，烯基，环烷基，芳烷基，苯基或杂环，R 1和R 2彼此独立地是氢或未取代或取代的烷基，烯基，炔基，环烷基，芳烷基或芳基，或R 1和R 2与氮一起为饱和杂环5元至7元环，X为氢，氯，溴，1至 4个碳原子的烷氧基，1至4个碳原子的烷氧基，烯丙氧基，β-氰基乙氧基，苄氧基，苯氧基，β-烷氧基羰基乙氧基，其中烷氧基为1至4个碳原子，1至4个碳原子的烷基巯基，苯基巯基或烷酰基氨基为1至 4个碳原子，Y为氯，1至4个碳原子的烷基，烯丙氧基，1至4个碳原子的烷氧基或β-氰基乙氧基，或X和Y一起是未被取代或被烷基，烷氧基取代的稠合苯环，氯或溴。该化合物特别适用于棉和合成纤维，优选聚酯的棉和联合织物的染色。所获得的染色部分地非常快。

5. 发明授权

US4278606A Preparation of 1-amino-2-phenoxy-4-hydroxyanthraquinone 失效
标题翻译： 1-氨基-2-苯氧基-4-羟基蒽醌的制备
公开(公告)号：US4278606A
公开(公告)日：1981-07-14
申请号：US128118
申请日：1980-03-07
申请人： Heinrich Hiller , Heinz Eilingsfeld , Helmut Reinicke , Fritz Traub
发明人： Heinrich Hiller , Heinz Eilingsfeld , Helmut Reinicke , Fritz Traub
IPC分类号： C07C225/36 , C09B1/54 , C07C97/26
CPC分类号： C09B1/547
摘要： In a process for the preparation of 1-amino-2-phenoxy-4-hydroxyanthraquinone by reacting 1-amino-2-halogeno-4-hydroxyanthraquinone with a phenol in an alkaline aqueous medium at an elevated temperature, the improvement that 1-amino-2-chloro-4-hydroxyanthraquinone is reacted in aqueous suspension, at a pH of from 9 to 13 and at from 120.degree. to 150.degree. C., with the phenol in the presence of(a) ammonium salts N.sup..sym. (R).sub.4 A.sup..crclbar., wherein one or more R's are linear or branched C.sub.4 -C.sub.20 -alkyl or C.sub.7 -C.sub.10 -phenylalkyl and the remaining R or R's may also be phenyl or N.sup..sym. (R).sub.3 may be pyridinium, and A.sup..crclbar. is one equivalent of an anion, of(b) ethylene oxide/propylene oxide block copolymers or of(c) oxyethylation products of alkylphenols, of alkenylamines, of alkylamines or of alkanols. A very pure product is obtained, in high yield.
摘要翻译：在碱性水性介质中，在升高的温度下，通过使1-氨基-2-卤代-4-羟基蒽醌与苯酚反应来制备1-氨基-2-苯氧基-4-羟基蒽醌的方法中，1-氨基 -2-氯-4-羟基蒽醌在水悬浮液中，在9-13℃和120-150℃下与苯酚在（a）铵盐N（+）（ R）4A（ - ），其中一个或多个R是直链或支链C 4 -C 20 - 烷基或C 7 -C 10 - 苯基烷基，其余的R或R也可以是苯基或N（+）（R）3可以是吡啶鎓， A（ - ）是（b）环氧乙烷/环氧丙烷嵌段共聚物或（c）烷基酚，链烯基胺，烷基胺或链烷醇的氧乙基化产物的阴离子的当量。获得非常纯的产物，产率高。

6. 发明授权

US4250090A 2-Amino-5-arylazoarylazothiazole compounds 失效
标题翻译： 2-氨基-5-芳基氮杂芳基唑类化合物
公开(公告)号：US4250090A
公开(公告)日：1981-02-10
申请号：US24248
申请日：1979-03-27
申请人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
发明人： Heinz Eilingsfeld , Guenter Hansen , Guenther Seybold , Georg Zeidler
IPC分类号： C09B29/36 , C09B31/14 , C09B56/00 , D06P1/39 , D06P3/06 , D06P3/32
CPC分类号： C09B31/14 , C09B29/3691 , C09B56/005
摘要： Acid azo dyes containing thiazole coupling components, of the general formula ##STR1## where D is the radical of a diazo component,R is hydrogen, acetyl, benzoyl or an aliphatic, cycloaliphatic, aromatic or heterocyclic radical,R.sup.1 and R.sup.2 independently of one another are optionally substituted alkyl, cycloalkyl, aralkyl or aryl,R.sup.1 may also be hydrogen andR.sup.1 and R.sup.2 together with the nitrogen may be a heterocyclic radical, andthe radicals D, R, R.sup.1 and/or R.sup.2 may in total contain from 1 to 4 --SO.sub.3 H groups.The deeply colored novel compounds are particularly suitable for dyeing polyamides, and the dyeings obtained have very good lightfastness and wetfastness.
摘要翻译：含有噻唑偶联组分的酸性偶氮染料，通式为其中D为重氮组分的基团，R为氢，乙酰基，苯甲酰基或脂族，脂环族，芳族或杂环基团，R1和R2独立地为一个另一个是任选取代的烷基，环烷基，芳烷基或芳基，R 1还可以是氢，R 1和R 2与氮一起可以是杂环基，基团D，R，R 1和/或R 2可以总共含有1至 4个-SO 3 H基团。深色的新型化合物特别适用于染色聚酰胺，所得染色剂具有非常好的耐光性和耐湿性。

7. 发明授权

US4042604A Isolation of dinitroanthraquinone having a high content of .alpha.,.alpha.- d 失效
标题翻译：具有高含量{60，{60-二硝基化合物的二硝基蒽醌的分离
公开(公告)号：US4042604A
公开(公告)日：1977-08-16
申请号：US686365
申请日：1976-05-14
申请人： Heinz Eilingsfeld , Dietrich Lach
发明人： Heinz Eilingsfeld , Dietrich Lach
IPC分类号： C07C205/47 , C07C67/00 , C07C201/00 , C09B1/00 , C07C79/37
CPC分类号： C07C225/34
摘要： A process for the isolation of mixtures of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone which have a high content of .alpha.,.alpha.'-dinitroanthraquinones by heating a suspension of the crude dinitroanthraquinone mixture in certain organic liquids at from 60.degree. to 200.degree. C until solution equilibrium has been set up, and separating the undissolved material from the solution. The undissolved material contains more than 90% and as a rule more than 95% by weight of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone. The pure mixture of 1,5-dinitroanthraquinone and 1,8-dinitroanthraquinone may be used for the manufacture of dyes.
摘要翻译：通过在60°至200°的某些有机液体中加热粗二硝基蒽醌混合物的悬浮液，分离具有高α，α'-二硝基蒽醌含量的1,5-二硝基蒽醌和1,8-二硝基蒽醌的混合物的方法直到溶液平衡已经建立，并将未溶解的材料与溶液分离。未溶解的材料含有超过90％且通常超过95重量％的1,5-二硝基蒽醌和1,8-二硝基蒽醌。 1,5-二硝基蒽醌和1,8-二硝基蒽醌的纯混合物可用于制备染料。

8. 发明授权

US5206375A Thiophene derivatives 失效
标题翻译：噻吩衍生物
公开(公告)号：US5206375A
公开(公告)日：1993-04-27
申请号：US865685
申请日：1992-04-08
申请人： Ernst Schefczik , Karl-Heinz Etzbach , Heinz Eilingsfeld
发明人： Ernst Schefczik , Karl-Heinz Etzbach , Heinz Eilingsfeld
IPC分类号： C07D333/38 , C07D333/44 , C07D409/04 , C07D409/06 , C09B29/00
CPC分类号： C07D409/04 , C07D333/38 , C07D333/44 , C07D409/06 , C09B29/0059
摘要： The novel compound of the general formula I ##STR1## where X is fluorine, chlorine, bromine, SO.sub.2 Y or unsubstituted or substituted hydroxyl or mercapto, Y is alkyl, alkenyl, cycloalkyl, aralkyl, aryl, chlorine or unsubstituted or substituted hydroxyl or amino, R is hydrogen, C.sub.1 -C.sub.4 -alkyl or a radical which can be introduced by electrophilic substitution or a radial of the formula --CH.dbd.T, in which T is a radical of a methyleneactive compound or of an amine, and R.sup.1 is hydrogen, acyl or unsubstituted or substituted alkyl, cycloalkyl or alkenyl, and R.sup.2 is hydrogen or unsubstituted or substituted alkyl or alkenyl, or R.sup.1 and R.sup.2 together with the nitrogen form a saturated heterocyclic structure and R.sup.1 and R.sup.2 together form a radical of the formula ##STR2## are useful as diazo and/or coupling components or generally as dye intermediates, depending on their constitution.
摘要翻译：其中X为氟，氯，溴，SO 2 Y或未取代或取代的羟基或巯基的通式I的新化合物，Y为烷基，烯基，环烷基，芳烷基，芳基，氯或未取代或取代的羟基或氨基， R是氢，C 1 -C 4烷基或可以通过亲电取代引入的基团或式-CH = T的径向，其中T是亚甲基活性化合物或胺的基团，R 1是氢，酰基或未取代或取代的烷基，环烷基或链烯基，R 2为氢或未取代或取代的烷基或烯基，或R 1和R 2与氮一起形成饱和杂环结构，并且R 1和R 2一起形成下式基团：根据其构成，可用作重氮和/或偶联组分或通常作为染料中间体。

9. 发明授权

US4490541A 5(3)-Aminopyrazolo-3,4(4,5)-dicarboximide azo dyestuff intermediates 失效
标题翻译： 5（3） - 氨基吡唑-3,4（4,5） - 二甲酰亚胺偶氮染料中间体
公开(公告)号：US4490541A
公开(公告)日：1984-12-25
申请号：US456095
申请日：1983-01-06
申请人： Heinz Eilingsfeld , Karl-Heinz Etzbach
发明人： Heinz Eilingsfeld , Karl-Heinz Etzbach
IPC分类号： C07D477/00 , C07D207/44 , C07D207/456 , C07D487/04 , C09B29/09 , C07D487/02
CPC分类号： C07D207/456 , C07D487/04
摘要： Compounds of the general formula I ##STR1## where R.sup.1 is hydrogen, unsubstituted or substituted alkyl, cycloalkyl or aryl, acyl, alkoxycarbonyl, phenoxycarbonyl, unsubstituted or substituted carbamyl, thiocarbamyl or sulfamyl, or alkylsulfonyl or arylsulfonyl, and R.sup.2 is hydrogen or a radical of a primary amine, are very useful as diazo components for the preparation of azo dyes.
摘要翻译：通式I的化合物其中R 1是氢，未取代或取代的烷基，环烷基或芳基，酰基，烷氧基羰基，苯氧基羰基，未取代或取代的氨基甲酰基，硫代氨基甲酰基或氨基磺酰基或烷基磺酰基或芳基磺酰基，R2是氢或伯胺的基团作为制备偶氮染料的重氮组分非常有用。

10. 发明授权

US4481272A Layered electrophotographic recording medium comprising heterocyclic nitrogen containing organic dye compounds 失效
标题翻译：含有杂环氮的有机染料化合物的分层电照相记录介质
公开(公告)号：US4481272A
公开(公告)日：1984-11-06
申请号：US554435
申请日：1983-11-22
申请人： Albrecht Eckell , Heinz Eilingsfeld , Albert Elzer , Franz Feichtmayr , Gerhard Hoffmann , Reinhold J. Leyrer , Peter Neumann
发明人： Albrecht Eckell , Heinz Eilingsfeld , Albert Elzer , Franz Feichtmayr , Gerhard Hoffmann , Reinhold J. Leyrer , Peter Neumann
IPC分类号： G03G5/00 , G03G5/06 , G03G5/14
CPC分类号： G03G5/0629
摘要： An electrophotographic recording medium which consists essentially of an electrically conductive base and a photosemiconductive double layer which comprises a first layer containing charge carrier-producing dyes, and a second layer containing one or more compounds which are charge carrier-transporting when exposed to light, wherein the charge carrier-producing dyes are those of the general formula I ##STR1## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are each hydrogen or a non-ionic substituent, X and Y are each the radical of a methylene-active compound, or of an aliphatic, cycloaliphatic, araliphatic, aromatic or heterocyclic amine or hydrazine, and Z is hydrogen, methyl or phenyl, and the production of this recording medium.
摘要翻译：一种电子照相记录介质，其基本上由导电基底和光电双层组成，该双层包含含有载电荷产生染料的第一层，以及含有一种或多种当暴露于光时是电荷载流子传输的化合物的第二层，其中电荷载体产生染料是通式I的那些，其中R 1，R 2，R 3和R 4各自为氢或非离子取代基，X和Y各自为亚甲基活性化合物的基团，或的脂族，脂环族，芳脂族，芳族或杂环胺或肼，Z是氢，甲基或苯基，以及该记录介质的制备。

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