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1. 发明授权

US06734277B2 Method of enhancing pit replication in optical disks 失效
标题翻译：增加光盘中凹坑复制的方法
公开(公告)号：US06734277B2
公开(公告)日：2004-05-11
申请号：US10141678
申请日：2002-05-09
申请人： Hans-Peter Brack , John Morgan Whitney , Jan-Pleun Lens , Christopher David Goewey , Irene Dris
发明人： Hans-Peter Brack , John Morgan Whitney , Jan-Pleun Lens , Christopher David Goewey , Irene Dris
IPC分类号： C08G6400
CPC分类号： C08G64/14 , G11B7/2534
摘要： Polycarbonate compositions incorporating long chain alkylphenol endgroups, for example cardanol, show enhanced pit replication characteristics when molded into optical disks. The enhancement in molding performance is especially pronounced at the shortest mold cycle times tested. Thus, a blend of 75 parts by weight bisphenol A polycarbonate 92 percent encapped with phenol, and 25 parts by weight bisphenol A polycarbonate about 100 percent endcapped with cardanol showed enhanced pit replication performance in optical disk molding trials relative to the same bisphenol A polycarbonate alone and analogous blends utilizing short chain alkylphenols.
摘要翻译：结合长链烷基酚端基（例如腰果酚）的聚碳酸酯组合物在模制成光盘时显示增强的凹坑复制特性。在最短的模具循环时间测试中，成型性能的提高尤其明显。因此，相对于单独的相同的双酚A聚碳酸酯，75重量份的双酚A聚碳酸酯92重量％与苯酚封端的共混物和25重量份约100重量％的与腰果醇封端的双酚A聚碳酸酯的共混物在光盘成型试验中显示增强的凹坑复制性能和使用短链烷基酚的类似共混物。

2. 发明授权

US06710156B2 Method for end-capping polycarbonate resins and composition for use in same 有权
标题翻译：封端聚碳酸酯树脂的方法及其组合物
公开(公告)号：US06710156B2
公开(公告)日：2004-03-23
申请号：US10268395
申请日：2002-10-10
申请人： John Morgan Whitney , Hans-Peter Brack , Theodorus Lambertus Hoeks , Irene Dris , Dennis Karlik
发明人： John Morgan Whitney , Hans-Peter Brack , Theodorus Lambertus Hoeks , Irene Dris , Dennis Karlik
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C08G64/14 , C08G64/42
摘要： A method for end-capping polycarbonate resins, comprising the step of processing a mixture comprising a polycarbonate having free hydroxyl-end groups and an end-capping reagent in a melt transesterification reaction to produce a polycarbonate resin, wherein the end-capping reagent comprises a mixture of: (a) at least one species of a symmetrical activated aromatic carbonate, and (b) at least one species of an optionally-substituted phenol, whereby said end-capping reagent reacts with at least some of the free hydroxyl end-groups of the polycarbonate to produce an end-capped polycarbonate resin.
摘要翻译：一种封端聚碳酸酯树脂的方法，包括在熔融酯交换反应中处理包含游离羟基端基的聚碳酸酯和封端剂的混合物以制备聚碳酸酯树脂的步骤，其中封端剂包括混合物：（a）至少一种对称活性芳族碳酸酯，和（b）至少一种任选取代的苯酚，其中所述封端剂与至少一些游离羟基端基反应的聚碳酸酯以制备端封聚碳酸酯树脂。

3. 发明授权

US07759456B2 Branched polycarbonate resins and processes to prepare the same 失效
标题翻译：分支聚碳酸酯树脂及其制备方法
公开(公告)号：US07759456B2
公开(公告)日：2010-07-20
申请号：US11623847
申请日：2007-01-17
申请人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
发明人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
IPC分类号： C09J3/00 , C08G64/40 , C08G64/06 , C08G64/14
CPC分类号： C08G64/06 , C08G64/307
摘要： A method of increasing the branching and polydispersity of a polycarbonate includes the steps of: (a) including in the polycarbonate at least one species of an alkyl substituted monomer, and (b) treating the polycarbonate at an elevated temperature and for a sufficient time to increase the branching and polydispersity relative to an otherwise equivalent polycarbonate without alkyl substituents.
摘要翻译：增加聚碳酸酯的支化和多分散性的方法包括以下步骤：（a）在聚碳酸酯中包含至少一种烷基取代的单体，和（b）在高温下处理聚碳酸酯足够的时间，相对于没有烷基取代基的其他等效聚碳酸酯，增加支化和多分散性。

4. 发明申请

US20120071606A1 POLYCARBONATE GRAFT COPOLYMERS 有权
标题翻译：聚碳酸酯共聚物
公开(公告)号：US20120071606A1
公开(公告)日：2012-03-22
申请号：US12885249
申请日：2010-09-17
申请人： Rubin Huang , Andre van Zyl , Jan Pleun Lens , Theodorus Lambertus Hoeks , Hans-Peter Brack , Jan Henk Kamps
发明人： Rubin Huang , Andre van Zyl , Jan Pleun Lens , Theodorus Lambertus Hoeks , Hans-Peter Brack , Jan Henk Kamps
IPC分类号： C08L51/00 , C08F4/00 , C08F257/00
CPC分类号： C08G64/18 , C08F283/02 , C08F285/00 , C08L51/08 , C08L69/00 , C08L33/12 , C08F220/18 , C08F226/10
摘要： Methods of forming polycarbonate graft copolymers are provided. In particular, a polycarbonate polymer or copolymer containing allyl groups provides the backbone for the graft copolymer, and pendant chains are attached to the copolymer through the allyl groups. The graft copolymers exhibit a combination of high transparency, good graft levels, good scratch resistance, and/or good anti-fog properties.
摘要翻译：提供了形成聚碳酸酯接枝共聚物的方法。特别地，含有烯丙基的聚碳酸酯聚合物或共聚物提供接枝共聚物的主链，并且侧链通过烯丙基连接到共聚物上。接枝共聚物表现出高透明度，良好的接枝水平，良好的耐刮擦性和/或良好的防雾性能的组合。

5. 发明授权

US07834125B2 Polycarbonates, compositions made therefrom, methods of manufacture thereof, and articles therefrom 有权
标题翻译：聚碳酸酯，由其制成的组合物，其制造方法及其制品
公开(公告)号：US07834125B2
公开(公告)日：2010-11-16
申请号：US12338229
申请日：2008-12-18
申请人： Hans-Peter Brack , Dennis Karlik , Jan-Pleun Lens , Dennis James Patrick Maria Willemse , Josef Gerardus Berndsen
发明人： Hans-Peter Brack , Dennis Karlik , Jan-Pleun Lens , Dennis James Patrick Maria Willemse , Josef Gerardus Berndsen
IPC分类号： C08G63/00 , C08G63/02
CPC分类号： C08G64/307 , C08G64/06
摘要： A melt polymerized polycarbonate comprising repeat units in the polycarbonate derived from the melt polymerization of monomers (II) and/or (III), monomer (IV), and optionally monomer (VIII), wherein monomers (II) and (III) are diaryl dihydroxy compounds, monomer (IV) is a sterically hindered dihydroxy compound, and monomer (VIII) is a non-sterically hindered dihydroxy diaryl compound; wherein the mole ratio of repeat units in the polycarbonate derived from monomers [(II)+(III)]:(IV):(VIII) is 15-70:1-85:0-50, the sum of the mole percent of repeat units in the polycarbonate derived from monomers [(II)+(III)]+(IV) is greater than or equal to 50 mole %, and the sum of the mole percent of units in the polycarbonate derived from monomers [(II)+(III)]+(IV)+(VIII) is 100 mole %; and wherein the polycarbonate has an L* value that is at least 1 L* unit value higher than the same polycarbonate in which monomer (IV) is replaced by bisphenol A.
摘要翻译：衍生自单体（II）和/或（III），单体（IV）和任选的单体（VIII）的熔体聚合的聚碳酸酯中的重复单元的熔融聚合的聚碳酸酯，其中单体（II）和（III）是二芳基二羟基化合物，单体（Ⅳ）为空间位阻二羟基化合物，单体（Ⅷ）为非位阻二羟基二芳基化合物; 其中衍生自单体[（II）+（III）]：（IV）：（VIII）的聚碳酸酯中的重复单元的摩尔比为15-70：1-85：0-50，衍生自单体[（II）+（III）] +（IV）的聚碳酸酯中的重复单元大于或等于50摩尔％，衍生自单体[（II））的聚碳酸酯中单元的摩尔百分比之和 +（III）] +（IV）+（VIII）为100摩尔％并且其中所述聚碳酸酯具有比单体（IV）被双酚A代替的相同聚碳酸酯高至少1L *单位值的L *值。

6. 发明授权

US08426532B2 Polycarbonate graft copolymers 有权
标题翻译：聚碳酸酯接枝共聚物
公开(公告)号：US08426532B2
公开(公告)日：2013-04-23
申请号：US12885249
申请日：2010-09-17
申请人： Rubin Huang , Andre van Zyl , Jan Pleun Lens , Theodorus Lambertus Hoeks , Hans-Peter Brack , Jan Henk Kamps
发明人： Rubin Huang , Andre van Zyl , Jan Pleun Lens , Theodorus Lambertus Hoeks , Hans-Peter Brack , Jan Henk Kamps
IPC分类号： C08L69/00 , C08G64/18 , C08F290/14 , C08F283/02
CPC分类号： C08G64/18 , C08F283/02 , C08F285/00 , C08L51/08 , C08L69/00 , C08L33/12 , C08F220/18 , C08F226/10
摘要： Methods of forming polycarbonate graft copolymers are provided. In particular, a polycarbonate polymer or copolymer containing allyl groups provides the backbone for the graft copolymer, and pendant chains are attached to the copolymer through the allyl groups. The graft copolymers exhibit a combination of high transparency, good graft levels, good scratch resistance, and/or good anti-fog properties.
摘要翻译：提供了形成聚碳酸酯接枝共聚物的方法。特别地，含有烯丙基的聚碳酸酯聚合物或共聚物提供接枝共聚物的主链，并且侧链通过烯丙基连接到共聚物上。接枝共聚物表现出高透明度，良好的接枝水平，良好的耐刮擦性和/或良好的防雾性能的组合。

7. 发明申请

US20080004426A1 Branched Polycarbonate Resins and Processes to Prepare the Same 失效
标题翻译：支化聚碳酸酯树脂及其制备方法
公开(公告)号：US20080004426A1
公开(公告)日：2008-01-03
申请号：US11623847
申请日：2007-01-17
申请人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
发明人： Hans-Peter Brack , Bernd Jansen , Jan Henk Kamps , Edward Kung , Jan Pleun Lens , Hans Looij , Han Vermeulen
IPC分类号： C08J3/00 , C08F6/00 , C08G64/00 , C08L69/00
CPC分类号： C08G64/06 , C08G64/307
摘要： A method of increasing the branching and polydispersity of a polycarbonate includes the steps of: (a) including in the polycarbonate at least one species of an alkyl substituted monomer, and (b) treating the polycarbonate at an elevated temperature and for a sufficient time to increase the branching and polydispersity relative to an otherwise equivalent polycarbonate without alkyl substituents.
摘要翻译：增加聚碳酸酯的支化和多分散性的方法包括以下步骤：（a）在聚碳酸酯中包含至少一种烷基取代的单体，和（b）在高温下处理聚碳酸酯足够的时间，相对于没有烷基取代基的其他等效聚碳酸酯，增加支化和多分散性。

8. 发明授权

US07105626B2 Method for incorporating alkyl ester endgroups to improve the release properties of melt polycarbonate 有权
标题翻译：用于加入烷基酯端基以改善熔融聚碳酸酯的脱模性能的方法
公开(公告)号：US07105626B2
公开(公告)日：2006-09-12
申请号：US10938337
申请日：2004-09-10
申请人： Hans-Peter Brack , Dennis Karlik , Jan Pleun Lens
发明人： Hans-Peter Brack , Dennis Karlik , Jan Pleun Lens
IPC分类号： C08G64/00
CPC分类号： C08G64/42 , C08G2650/04
摘要： Alkyl ester end-capped polycarbonates have improved release properties and may be produced by a method comprising the step of combining a polycarbonate having free terminal OH groups with an end-capping reagent comprising a symmetrical activated carbonate and an alkyl ester, whereby the end-capping reagent reacts with at least some of the free hydroxyl end groups of the polycarbonate to produce an end-capped polycarbonate comprising optionally substituted aliphatic ester end groups.
摘要翻译：烷基酯封端的聚碳酸酯具有改进的脱模性能，并且可以通过包括以下步骤的方法制备：将具有游离的末端OH基团的聚碳酸酯与包含对称活性碳酸酯和烷基酯的封端剂组合的步骤，由此封端试剂与聚碳酸酯的至少一些游离羟基端基反应以制备包含任选取代的脂族酯端基的封端聚碳酸酯。

9. 发明授权

US06486294B1 Production of poly(carbonate-co-ester) copolymers 有权
标题翻译：聚（碳酸酯 - 共 - 酯）共聚物的生产
公开(公告)号：US06486294B1
公开(公告)日：2002-11-26
申请号：US09683807
申请日：2002-02-19
申请人： Hans-Peter Brack , Jan Pleun Lens
发明人： Hans-Peter Brack , Jan Pleun Lens
IPC分类号： C08G6400
CPC分类号： C08G63/64
摘要： A poly(carbonate-co-ester) block copolymer is synthesized using synthetic strategies that can be incorporated into conventional melt facilities that are commonly used in the production of polycarbonate polymers. The polycarbonate block of the poly(carbonate-co-ester) copolymer is derived from a polycarbonate reaction mixture comprising an aromatic dihydroxy compound and a carbonic acid diester, such as bisphenol A and diphenyl carbonate, respectively. The second block of the copolymer is derived from a polyester prepolymer, the polyester prepolymer comprising a diol, diacid or diester, and at least one monomer that is selected to advantageously incorporate desired properties into the poly(carbonate-co-ester) copolymer. The polyester prepolymer is introduced to the polycarbonate reaction mixture to form the poly(carbonate-co-ester) copolymer. Properties of the copolymer can be altered by varying numerous conditions of the reaction.
摘要翻译：使用可以结合到通常用于生产聚碳酸酯聚合物的常规熔融设备中的合成策略来合成聚（碳酸酯 - 共 - 酯）嵌段共聚物。聚（碳酸酯 - 共 - 酯）共聚物的聚碳酸酯嵌段衍生自包含芳族二羟基化合物和碳酸二酯的聚碳酸酯反应混合物，例如双酚A和碳酸二苯酯。共聚物的第二嵌段衍生自聚酯预聚物，聚酯预聚物包含二醇，二酸或二酯，以及至少一种选择以有利地将所需性质并入聚（碳酸酯 - 共酯）共聚物中的单体。将聚酯预聚物引入聚碳酸酯反应混合物中以形成聚（碳酸酯 - 共 - 酯）共聚物。通过改变多种反应条件可以改变共聚物的性质。

10. 发明授权

US06747119B2 Method and system for preparing a polycarbonate, copolymerization reagent and polycarbonate 失效
标题翻译：制备聚碳酸酯，共聚试剂和聚碳酸酯的方法和系统
公开(公告)号：US06747119B2
公开(公告)日：2004-06-08
申请号：US10107149
申请日：2002-03-28
申请人： Hans-Peter Brack , Dennis Karlik , Theodorus Lambertus Hoeks , John Morgan Whitney
发明人： Hans-Peter Brack , Dennis Karlik , Theodorus Lambertus Hoeks , John Morgan Whitney
IPC分类号： C08G6400
CPC分类号： C08G63/64 , C08G64/307
摘要： A method for preparing a polycarbonate comprises preparing a free hydroxyl-containing polycarbonate and reacting the hydroxyl-containing polycarbonate with a mixture of (B) a symmetrical optionally activated aromatic carbonic acid diester and (C) an optionally substituted aromatic hihydroxy compound, diol or diacid. A copolymerization reagent comprises a mixture of (B) a symmetrical optionally activated aromatic carbonic acid diester and (C) an optionally substituted aromatic hihydroxy compound, diol or diacid. A copolymer comprises [polycarbonate]x moieties; (B) [symmetrical optionally activated aromatic carbonic acid diester]y moieties and (C) [optionally substituted aromatic hihydroxy compound, diol or diacid]z moieties, wherein x, y and z are mole percents of the copolymer.
摘要翻译：制备聚碳酸酯的方法包括制备游离含羟基的聚碳酸酯并使含羟基的聚碳酸酯与（B）对称的任选活化的芳族碳酸二酯和（C）任选取代的芳族羟基化合物，二醇或二酸的混合物。共聚试剂包括（B）对称的任选活化的芳族碳酸二酯和（C）任选取代的芳族羟基化合物，二醇或二酸的混合物。共聚物包含[聚碳酸酯] x部分; （B）[对称任选活化的芳族碳酸二酯] y部分和（C）[任选取代的芳族羟基化合物，二醇或二酸] z部分，其中x，y和z是共聚物的摩尔百分比。

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