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1. 发明授权

US4049742A Recovery of 1,3-butadiene from a C.sub.4 -hydrocarbon mixture 失效
标题翻译：从C {HD 4 {B-烃混合物中回收1,3-丁二烯
公开(公告)号：US4049742A
公开(公告)日：1977-09-20
申请号：US669710
申请日：1976-03-23
申请人： Hans-Martin Weitz , Ulrich Wagner , Klaus Volkamer , Eckart Schubert , Friedhelm Bandermann
发明人： Hans-Martin Weitz , Ulrich Wagner , Klaus Volkamer , Eckart Schubert , Friedhelm Bandermann
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C7/163 , C07C7/167 , C07C11/167 , C07C67/00
CPC分类号： C07C7/005 , C07C7/163
摘要： 1,3-Butadiene is recovered with the aid of a selective solvent from a C.sub.4 -hydocarbon mixture containing 1,3-butadiene, hydrocarbons which are more soluble in said selective solvent than 1,3-butadiene, including acetylenes and possibly 1,2-butadiene and C.sub.5 -hydrocarbons, and hydrocarbons which are less soluble in said selective solvent than 1,3-butadiene. The C.sub.4 -hydrocarbon mixture is separated by the use of one or more extractive distilling zones into a distillate containing the less soluble hydrocarbons, a stream consisting of 1,3-butadiene and a stream containing the more soluble hydrocarbons including the higher acetylenes and 1,3-butadiene, the latter stream being subjected to catalytic hydrogenation.
摘要翻译：借助于来自含有1,3-丁二烯的C4-碳氢化合物混合物的选择性溶剂回收1,3-丁二烯，在所述选择性溶剂中比1,3-丁二烯更可溶的烃，包括乙炔和可能的1,2- 丁二烯和C 5烃，以及比1,3-丁二烯更不溶于所述选择性溶剂的烃。通过使用一个或多个萃取蒸馏区将C4烃混合物分离成含有较不溶性烃的馏出物，由1,3-丁二烯组成的物流和含有较可溶性烃的物流，包括较高乙炔和1， 3-丁二烯，后一个流进行催化氢化。

2. 发明授权

US4310388A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 hydrocarbon 失效
标题翻译：从C4-或C5烃分离共轭二烯烃
公开(公告)号：US4310388A
公开(公告)日：1982-01-12
申请号：US126898
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
发明人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 50 to 99 percent by weight of a selective solvent boiling at from 140.degree. C. to 260.degree. C. and(b) from 1 to 50 percent by weight of an organic solvent boiling at from 45.degree. C. to 125.degree. C.
摘要翻译：一种通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）50 至99重量％的在140℃至260℃沸腾的选择性溶剂和（b）1至50重量％的沸点为45℃至125℃的有机溶剂。

3. 发明授权

US4277315A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C4或C5烃混合物中分离共轭二烯烃
公开(公告)号：US4277315A
公开(公告)日：1981-07-07
申请号：US126897
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
发明人： Klaus Volkamer , Klaus Broellos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Juergen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 1 to 99 percent by weight of an N-alkyl-substituted lower aliphatic acid amide or of an N-alkyl-substituted alicyclic acid amide having 5 ring members and(b) from 1 to 99 percent by weight of an lower aliphatic carboxylic acid ester or carbonic acid ester boiling at from 30.degree. C. to 200.degree. C.
摘要翻译：通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）1 至99重量％的N-烷基取代的低级脂肪酸酰胺或具有5个环成员的N-烷基取代的脂环酸酰胺和（b）1至99重量％的低级脂族羧酸酯或碳酸酯在30〜200℃下沸腾。

4. 发明授权

US4278504A Isolation of a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C4或C5烃混合物中分离共轭二烯烃
公开(公告)号：US4278504A
公开(公告)日：1981-07-14
申请号：US126903
申请日：1980-03-03
申请人： Klaus Volkamer , Klaus Brollos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Jurgen Schneider
发明人： Klaus Volkamer , Klaus Brollos , Alfred Lindner , Ulrich Wagner , Hans-Martin Weitz , Klaus-Jurgen Schneider
IPC分类号： C07C1/00 , C07C7/08 , C07C11/12 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08
摘要： A process for isolating a conjugated diolefin from a C.sub.4 - or C.sub.5 -hydrocarbon mixture containing the diolefin, by single-stage or multi-stage extractive distillation using a selective solvent, wherein the selective solvent is a solvent mixture which comprises(a) from 1 to 99 percent by weight of an N-alkyl-substituted lower aliphatic acid amide or of an N-alkyl-substituted alicyclic acid amide having 5 ring members and(b) from 1 to 99 percent by weight of an aliphatic or alicyclic ether boiling at from 30.degree. C. to 200.degree. C.
摘要翻译：通过使用选择性溶剂的单级或多级萃取蒸馏从含有二烯烃的C4-或C5-烃混合物中分离共轭二烯烃的方法，其中所述选择性溶剂是溶剂混合物，其包含（a）1 至99重量％的N-烷基取代的低级脂肪酸酰胺或具有5个环成员的N-烷基取代的脂环族酰胺酰胺，和（b）1至99重量％的沸腾的脂族或脂环族醚从30℃至200℃

5. 发明授权

US4162198A Separation of a mixture of C.sub.4 -hydrocarbons by extractive distillation 失效
标题翻译：通过萃取蒸馏分离C {HD 4 {B-烃的混合物
公开(公告)号：US4162198A
公开(公告)日：1979-07-24
申请号：US906469
申请日：1978-05-17
申请人： Dieter Stockburger , Klaus Volkamer , Detlef Bender , Klaus-Juergen Schneider , Harald Schwentker , Ulrich Wagner , Hans-Martin Weitz
发明人： Dieter Stockburger , Klaus Volkamer , Detlef Bender , Klaus-Juergen Schneider , Harald Schwentker , Ulrich Wagner , Hans-Martin Weitz
IPC分类号： B01D3/40 , C07C1/00 , C07C7/08 , C07C9/00 , C07C11/00 , C07C11/167 , C07C67/00 , B01D3/06
CPC分类号： C07C7/08 , B01D3/40 , Y10S203/20
摘要： A process for separating, by means of a selective solvent, a mixture of C.sub.4 -hydrocarbons which contains some hydrocarbons which are more soluble in the selective solvent and some which are less soluble therein, in which process the hydrocarbon mixture is separated, in an extractive distillation zone, into a top product which contains the less soluble hydrocarbons and an extract which contains the more soluble hydrocarbons and the selective solvent, the extract, taken off as the bottom product, is subjected to a flash evaporation and the resulting vapor component of the extract is recycled to the extractive distillation zone while the liquid phase remaining after the flash evaporation is fed to a solvent recovery zone, in which the liquid phase obtained from the flash evaporation is separated into a product containing the hydrocarbons and, as the bottom product, the selective solvent which has been freed from the hydrocarbons, the resulting selective solvent is recycled to the extractive distillation zone and the product which is obtained from the solvent recovery zone and contains the hydrocarbons is partially or completely recycled to the extractive distillation zone, after increasing the pressure in a compression zone, in which process the extract taken off the extractive distillation zone is brought, prior to the flash evaporation to a higher pressure than the pressure in the extractive distillation zone and thereafter the extract which is under this higher pressure is heated, in a heat exchange zone, by indirect heat exchange with the selective solvent obtained as the bottom product from the solvent recovery zone, and the heated extract is subsequently let down, in the flash evaporation, to a pressure which is at least equal to the pressure in the extractive distillation zone and is higher than the pressure in the solvent recovery zone.
摘要翻译：通过选择性溶剂分离出含有一些较易溶于选择性溶剂的烃和一些较不溶于其中的烃类的混合物的混合物的方法，在该方法中，烃混合物在萃取过程中分离蒸馏区，成为含有较少溶解性烃的顶部产物和含有较多可溶性烃和选择性溶剂的提取物，作为底部产物取出的萃取物进行闪蒸，并将得到的蒸气成分萃取液再循环到萃取蒸馏区，闪蒸蒸发后剩余的液相被送入溶剂回收区，其中将从闪蒸蒸发获得的液相分离成含有烃的产物，作为底部产物，已经从烃中除去的选择性溶剂，所得到的选择性溶剂被再循环到萃取物中蒸馏区和从溶剂回收区获得并且含有烃的产物在增加压缩区中的压力之后部分或完全再循环到萃取蒸馏区，在该过程中，提取物从萃取蒸馏区被带走在闪蒸蒸发到比萃取蒸馏区中的压力高的压力之前，然后将在该较高压力下的提取物在热交换区域中与作为底部产物获得的选择性溶剂进行间接热交换然后将被加热的提取物在闪蒸中降至至少等于萃取蒸馏区压力的压力，并高于溶剂回收区的压力。

6. 发明授权

US4287379A Process for obtaining isobutene from C.sub.4 -hydrocarbon mixtures containing isobutene 失效
标题翻译：从含有异丁烯的C 4烃混合物中获得异丁烯的方法
公开(公告)号：US4287379A
公开(公告)日：1981-09-01
申请号：US137750
申请日：1980-04-07
申请人： Erwin Brunner , Eckart Schubert , Alfred Lindner , Franz Merger , Klaus Volkamer , Max Strohmeyer , Gerhard Sandrock
发明人： Erwin Brunner , Eckart Schubert , Alfred Lindner , Franz Merger , Klaus Volkamer , Max Strohmeyer , Gerhard Sandrock
IPC分类号： B01J31/00 , C07B61/00 , C07C1/00 , C07C7/148 , C07C11/09 , C07C41/42 , C07C67/00 , C07C7/00
CPC分类号： C07C41/42 , C07C11/09 , C07C41/06 , C07C7/14891
摘要： A process for obtaining isobutene from a C.sub.4 -hydrocarbon mixture containing isobutene, by reacting the mixture with a primary alcohol in the presence of an acid condensing agent and decomposing the resulting tertiary ether in the presence of an acid catalyst at an elevated temperature, wherein a primary C.sub.3 - or C.sub.4 -alcohol is used.
摘要翻译：通过在酸缩合剂存在下使该混合物与伯醇反应并在酸催化剂存在下在升高的温度下分解得到的叔乙醚，从含有异丁烯的C 4烃混合物中获得异丁烯的方法，其中a 使用初级C3-或C4-醇。

7. 发明授权

US4414004A Removal of condensable aliphatic hydrocarbons and acidic gases from natural gas 失效
标题翻译：从天然气中去除可冷凝的脂族烃和酸性气体
公开(公告)号：US4414004A
公开(公告)日：1983-11-08
申请号：US356721
申请日：1982-03-10
申请人： Eckhart Wagner , Ulrich Wagner , Klaus Volkamer , Wolfgang Vodrazka
发明人： Eckhart Wagner , Ulrich Wagner , Klaus Volkamer , Wolfgang Vodrazka
IPC分类号： B01D53/14 , C07C7/11 , C10G5/04
CPC分类号： C10G5/04 , B01D53/1456 , B01D53/1487 , B01D53/1493 , C07C7/11 , C10G2300/1025
摘要： A process for removing condensable aliphatic hydrocarbons and acidic gases such as H.sub.2 S, CO.sub.2 and COS from natural gas containing these, wherein the natural gas is initially treated with polyethylene glycol dialkyl ethers, as the solvent, in a first absorption stage to effect absorption of the condensable aliphatic hydrocarbons; the natural gas drawn off from the first absorption stage is then treated with polyethylene glycol dialkyl ethers, as the solvent, under superatmospheric pressure in a second absorption stage, the acidic gases being completely or partly absorbed; the solvent charged with the condensable aliphatic hydrocarbons which is obtained from the first absorption stage is treated with water in an extraction stage, to form a hydrocarbon phase containing the condensable aliphatic hydrocarbons and an aqueous dialkyl ether phase, and the hydrocarbon phase is separated from the aqueous dialkyl ether phase. The solvent charged with acid gases which is obtained from the second absorption stage is regenerated by expansion and/or stripping in a regeneration stage and the regenerated solvent is recycled to the absorption.
摘要翻译：从含有这些的天然气中除去可冷凝的脂族烃和酸性气体如H 2 S，CO 2和COS的方法，其中在第一吸收阶段天然气首先用聚乙二醇二烷基醚作为溶剂处理，以实现吸收可缩合的脂族烃; 然后在第二吸收阶段的超大气压下，用作为溶剂的聚乙二醇二烷基醚处理从第一吸收阶段排出的天然气，酸性气体被完全或部分吸收; 在萃取阶段用水处理从第一吸收阶段得到的可冷凝脂肪族烃的溶剂，形成含有可冷凝脂族烃和二烷基醚水相的烃相，将烃相与二烷基醚相水相。通过在再生阶段中的膨胀和/或汽提再生从第二吸收阶段获得的装有酸性气体的溶剂，并将再生的溶剂再循环至吸收。

8. 发明授权

US4336233A Removal of CO.sub.2 and/or H.sub.2 S and/or COS from gases containing these constituents 失效
标题翻译：从含有这些成分的气体中去除二氧化碳和/或硫化氢和/或COS
公开(公告)号：US4336233A
公开(公告)日：1982-06-22
申请号：US177615
申请日：1980-08-13
申请人： Max Appl , Ulrich Wagner , Hans J. Henrici , Klaus Kuessner , Klaus Volkamer , Ernst Fuerst
发明人： Max Appl , Ulrich Wagner , Hans J. Henrici , Klaus Kuessner , Klaus Volkamer , Ernst Fuerst
IPC分类号： B01D53/14 , B01D53/40 , B01D53/48 , B01D53/77 , C10K1/14 , B01D53/34
CPC分类号： C10K1/143 , B01D53/1493 , C10K1/14 , Y02C10/06 , Y02P20/152
摘要： An aqueous solution containing from 0.81 to 1.3 moles of piperazine per liter is used as a washing agent for removing impurities such as H.sub.2 S, CO.sub.2 and COS from gases. Piperazine can also be used, in amounts of up to 0.8 mole per liter, together with physical or chemical solvents, to accelerate the absorption of H.sub.2 S, CO.sub.2 and COS. The washing process is used for natural gases, coke-oven gases, gases from the gasification of coal and synthesis gases, of any origin.
摘要翻译：使用含有0.81〜1.3摩尔哌嗪/升的水溶液作为从气体中除去H 2 S，CO 2，COS等杂质的洗涤剂。哌嗪也可以以每升高达0.8摩尔的量与物理或化学溶剂一起使用，以加速H2S，CO2和COS的吸收。洗涤过程用于天然气，焦炉气体，来自任何来源的煤和合成气体的气化。

9. 发明授权

US4647344A Recovery of isoprene from a C.sub.5 -hydrocarbon mixture 失效
标题翻译：从C5烃混合物中回收异戊二烯
公开(公告)号：US4647344A
公开(公告)日：1987-03-03
申请号：US662602
申请日：1984-10-19
申请人： Alfred Lindner , Ulrich Wagner , Klaus Volkamer , Walter Rebafka
发明人： Alfred Lindner , Ulrich Wagner , Klaus Volkamer , Walter Rebafka
IPC分类号： C07B61/00 , C07C1/00 , C07C7/08 , C07C7/10 , C07C7/163 , C07C11/18 , C07C67/00 , B01D3/40
CPC分类号： C07C7/08 , C07C7/10 , Y10S203/20
摘要： Isoprene is recovered from a C.sub.5 -hydrocarbon mixture containing isoprene, penta-1,3-diene and cyclopentadiene by separating the said mixture by liquid-liquid extraction or extractive distillation with the aid of a selective solvent, in combination with a distillation upstream or downstream from the liquid-liquid extraction or extractive distillation, by a method in which a stream containing penta-1,3-diene and cyclopentadiene is separated off in the upstream or downstream distillation and is catalytically hydrogenated, and the hydrogenated stream is fed to the upper part of the liquid-liquid extraction or extractive distillation.
摘要翻译：通过使用选择性溶剂的液 - 液萃取或萃取蒸馏分离所述混合物，与上游或下游的蒸馏相结合，从含有异戊二烯，五-1,3-二烯和环戊二烯的C5-烃混合物回收异戊二烯从液 - 液萃取或萃取蒸馏中，通过在上游或下游蒸馏中分离出含有五-1,3-二烯和环戊二烯的物流并进行催化氢化的方法，并将氢化流进料至上层液体萃取或萃取蒸馏的一部分。

10. 发明授权

US4277314A Isolation of 1,3-butadiene from a C4-hydrocarbon mixture 失效
标题翻译：从C4烃混合物中分离出1,3-丁二烯
公开(公告)号：US4277314A
公开(公告)日：1981-07-07
申请号：US40283
申请日：1979-05-18
申请人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
发明人： Alfred Lindner , Klaus Volkamer , Ulrich Wagner
IPC分类号： C07C7/08 , C07C1/00 , C07C7/00 , C07C7/05 , C07C11/167 , C07C67/00 , B01D3/40
CPC分类号： C07C7/005 , C07C7/05
摘要： A process for isolating 1,3-butadiene by means of a selective solvent from a C.sub.4 -hydrocarbon mixture which contains 1,3-butadiene, propyne, hydrocarbons which are more soluble than 1,3-butadiene in the selective solvent and hydrocarbons which are less soluble than 1,3-butadiene in the selective solvent, wherein the C.sub.4 -hydrocarbon mixture is separated, using one or more extractive distillation zones, into a distillate containing the less soluble hydrocarbons, a stream of 1,3-butadiene and a stream containing the more soluble hydrocarbons, and the propyne is separated off either by distillation of the C.sub.4 -hydrocarbon mixture in a distillation zone upstream of the extractive distillation zone or zones or by distillation of the stream of 1,3-butadiene, obtained from the extractive distillation zone or zones, in a downstream distillation zone, giving a stream of hydrocarbons containing propyne and 1,3-butadiene, which stream is fed to an additional distillation zone, while at the same time a second stream of liquid or gaseous hydrocarbons is fed to the additional distillation zone, and the bottom product from the additional distillation zone is recycled to the extractive distillation.
摘要翻译：通过选择性溶剂从含有1,3-丁二烯，丙炔，在选择性溶剂中比1,3-丁二烯更可溶的烃的C 4烃混合物分离1,3-丁二烯的方法和烃，其为在选择性溶剂中比1,3-丁二烯更难溶解，其中使用一个或多个萃取蒸馏区将C4-烃混合物分离成含有较不溶性烃的馏出物，1,3-丁二烯流和流含有较多的可溶性烃，丙炔通过在萃取蒸馏区或蒸馏区上游的蒸馏区中蒸馏出C4烃混合物，或通过蒸馏萃取物获得的1,3-丁二烯来分离。蒸馏区或区域，在下游蒸馏区中，产生含有丙炔和1,3-丁二烯的烃流，该料流被供给到另外的蒸馏区，同时a 液体或气态烃的第二流进料到另外的蒸馏区，并且来自附加蒸馏区的底部产物被再循环至萃取蒸馏。

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