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1. 发明授权

US08461394B2 Process for preparing C5 aldehyde mixtures with a high n-pentanal content 有权
标题翻译：制备具有高正戊醛含量的C5醛混合物的方法
公开(公告)号：US08461394B2
公开(公告)日：2013-06-11
申请号：US12995800
申请日：2009-04-28
申请人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
发明人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
IPC分类号： C07C45/50
CPC分类号： B01J31/0237 , B01J31/185 , B01J2231/321 , B01J2531/822 , C07C45/50 , Y02P20/582 , C07C47/02
摘要： A process for preparing a C5 aldehyde mixture from a hydrocarbon mixture comprising at least one linear butene by terminal hydroformylation under isomerizing conditions, using a catalyst system comprising rhodium, a bisphosphite ligand, and an amine.
摘要翻译：一种通过使用包含铑，二亚磷酸酯配位体和胺的催化剂体系在异构化条件下通过末端加氢甲酰基化从包含至少一个直链丁烯的烃混合物制备C5醛混合物的方法。

2. 发明申请

US20110130595A1 PROCESS FOR PREPARING C5 ALDEHYDE MIXTURES WITH A HIGH N-PENTANAL CONTENT 有权
标题翻译：制备具有高N-PENTANAL CONTENT的C5醛类混合物的方法
公开(公告)号：US20110130595A1
公开(公告)日：2011-06-02
申请号：US12995800
申请日：2009-04-28
申请人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
发明人： Hans-Gerd Lueken , Dirk Fridag , Udo Lenz , Hermann-Josef Schulte-Althoff , Klaus-Diether Wiese , Alfred Kaizik , Patrick Muhlack , Wilfried Bueschken , Frank Hoeper
IPC分类号： C07C45/00
CPC分类号： B01J31/0237 , B01J31/185 , B01J2231/321 , B01J2531/822 , C07C45/50 , Y02P20/582 , C07C47/02
摘要： A process for preparing a C5 aldehyde mixture from a hydrocarbon mixture comprising at least one linear butene by terminal hydroformylation under isomerizing conditions, using a catalyst system comprising rhodium, a bisphosphite ligand, and an amine.
摘要翻译：一种通过使用包含铑，二亚磷酸酯配位体和胺的催化剂体系在异构化条件下通过末端加氢甲酰基化从包含至少一个直链丁烯的烃混合物制备C5醛混合物的方法。

3. 发明授权

US09428433B2 Control of the viscosity of reaction solutions in hydroformylation processes 有权
标题翻译：控制加氢甲酰化过程中反应溶液的粘度
公开(公告)号：US09428433B2
公开(公告)日：2016-08-30
申请号：US14653717
申请日：2013-12-09
申请人： Dirk Fridag , Udo Lenz , Hans-Gerd Lueken , Robert Franke , Markus Rudek , Klaus-Diether Wiese , Soenke Broecker , Markus Priske , Christoph Patalong
发明人： Dirk Fridag , Udo Lenz , Hans-Gerd Lueken , Robert Franke , Markus Rudek , Klaus-Diether Wiese , Soenke Broecker , Markus Priske , Christoph Patalong
IPC分类号： C07C45/50 , B01J19/00 , B01J19/24
CPC分类号： C07C45/50 , B01J19/24 , B01J2219/00162 , B01J2219/00245 , B01J2219/24 , C07C47/02
摘要： The present invention relates to a method and a device for controlling the viscosity of reaction solutions in the hydroformylation of olefin-containing mixtures.
摘要翻译：本发明涉及用于控制含烯烃混合物的加氢甲酰基化反应溶液粘度的方法和装置。

4. 发明授权

US08846994B2 Method for producing low-odor n-butane 有权
标题翻译：生产低气味正丁烷的方法
公开(公告)号：US08846994B2
公开(公告)日：2014-09-30
申请号：US13381735
申请日：2010-05-21
申请人： Hans-Gerd Lueken , Alfred Kaizik , Markus Winterberg , Wilfried Bueschken , Dirk Fridag
发明人： Hans-Gerd Lueken , Alfred Kaizik , Markus Winterberg , Wilfried Bueschken , Dirk Fridag
IPC分类号： C07C5/00 , C07C9/10 , C07C7/163 , C07C7/10
CPC分类号： C07C9/10 , C07C7/10 , C07C7/163
摘要： The invention relates to a method for producing low-odor n-butane by catalytic hydrogenation of a feed mixture. The aim of the invention is to provide such a method, wherein the feed material, in addition to n-butane, n-butene and up to 1 mass % formic acid and/or up to 1 mass % pentanals and/or up to 0.5 mass % pentanols, also comprises carbon monoxide. The aim is achieved by treating the feed mixture in the temperature range of 15 to 120° C. with an aqueous solution of an alkali metal or alkaline earth metal hydroxide in the concentration range of 0.5 to 30 mass % and subsequently subjecting the feed mixture to the catalytic hydrogenation.
摘要翻译：本发明涉及通过进料混合物的催化氢化生产低气味正丁烷的方法。本发明的目的是提供这样的方法，其中除了正丁烷，正丁烯和至多1质量％的甲酸和/或至多1质量％的戊醛和/或至多0.5的进料之外，质量％戊醇还含有一氧化碳。目的是通过在0.5〜30质量％的浓度范围内用碱金属或碱土金属氢氧化物的水溶液处理15〜120℃的温度范围内的进料混合物，然后将进料混合物催化氢化。

5. 发明授权

US08581008B2 Process for preparing α,β-unsaturated C10-aldehydes 有权
标题翻译：制备α，β-不饱和C10醛的方法
公开(公告)号：US08581008B2
公开(公告)日：2013-11-12
申请号：US13256116
申请日：2010-02-23
申请人： Alfred Kaizik , Dirk Fridag , Hans-Gerd Lueken , Wilfried Bueschken
发明人： Alfred Kaizik , Dirk Fridag , Hans-Gerd Lueken , Wilfried Bueschken
IPC分类号： C07C45/45
CPC分类号： C07C45/74 , Y02P20/582 , C07C47/21
摘要： The invention relates to a method for continuously producing α,β-unsaturated C10-aldehydes from aliphatic C5-aldehydes, comprising the following steps: aldol-condensing aliphatic C5-aldehydes into α,β-unsaturated C10-aldehydes in the presence of an aqueous base in a tube reactor; phase separating the output of the tube reactor into an aqueous catalyst phase and an organic product phase; separating the organic product phase into α,β-unsaturated C10-aldehydes, aliphatic C5-aldehydes, and auxiliary products; discharging a part of the aqueous catalyst phase to remove the reaction water and supplementing said part with liquor solution and subsequently returning said part to the tube reactor. The task of the invention is to improve a method of said kind in a way such that it requires lower energy input. This is achieved in that the aliphatic C5-aldehydes and/or the α,β-unsaturated C10-aldehydes are dispersed in the aqueous base as drops, wherein the average Sauter diameter of the drops is between 0.2 mm and 2 mm.
摘要翻译：本发明涉及一种从脂肪族C5醛连续生产α，β-不饱和C10醛的方法，包括以下步骤：将脂族C 5 - 醛缩合成α，β-不饱和C10醛在水溶液基于管式反应器; 将管式反应器的输出相分离成水性催化剂相和有机产物相; 将有机产物相分离成α，β-不饱和C10醛，脂族C5醛和辅助产物; 排出一部分水性催化剂相以除去反应水并用液体溶液补充所述部分，随后将所述部分返回到管式反应器。本发明的任务是改进所述种类的方法，使其需要较低的能量输入。这是因为脂族C 5 - 醛和/或α，β-不饱和C 10 - 醛以水滴的形式分散在水性碱中，其中液滴的平均Sauter直径在0.2mm与2mm之间。

6. 发明授权

US08563782B2 Producing α,β-unsaturated aldehydes by means of a reaction mixing pump 有权
标题翻译：通过反应混合泵生产α，β-不饱和醛
公开(公告)号：US08563782B2
公开(公告)日：2013-10-22
申请号：US13498690
申请日：2010-08-03
申请人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
发明人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
IPC分类号： C07C45/72
CPC分类号： C07C45/74 , Y02P20/582 , C07C47/21
摘要： The invention relates to a method for producing α,β-unsaturated aldehydes, wherein a catalytic aldol condensation of charged aldehydes is carried out in the presence of an aqueous base within a continuous-flow reactor. The aim of the invention is to provide a method for aldolizing aldehydes that can be carried out in a particularly economical manner. The aim is achieved by using a reaction mixing pump as the reactor.
摘要翻译：本发明涉及一种生产α，β-不饱和醛的方法，其中带电醛的催化醛醇缩合在连续流反应器内的碱性水溶液存在下进行。本发明的目的是提供一种可以以特别经济的方式进行醛脱醛化的方法。目的是通过使用反应混合泵作为反应器来实现。

7. 发明申请

US20120190895A1 PRODUCING ALPHA,BETA-UNSATURATED ALDEHYDES BY MEANS OF A REACTION MIXING PUMP 有权
标题翻译：通过反应混合泵生产ALPHA，BETA不饱和醛
公开(公告)号：US20120190895A1
公开(公告)日：2012-07-26
申请号：US13498690
申请日：2010-08-03
申请人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
发明人： Alfred Kaizik , Hans-Gerd Lueken , Dirk Fridag , Wilfried Bueschken , Dirk Mackowiak , Frank Brocksien
IPC分类号： C07C45/72
CPC分类号： C07C45/74 , Y02P20/582 , C07C47/21
摘要： The invention relates to a method for producing α,β-unsaturated aldehydes, wherein a catalytic aldol condensation of charged aldehydes is carried out in the presence of an aqueous base within a continuous-flow reactor. The aim of the invention is to provide a method for aldolizing aldehydes that can be carried out in a particularly economical manner. The aim is achieved by using a reaction mixing pump as the reactor.
摘要翻译：本发明涉及一种生产α，β-不饱和醛的方法，其中在连续流动反应器内的碱性水溶液存在下进行带电醛的催化醛醇缩合。本发明的目的是提供一种可以以特别经济的方式进行醛脱醛化的方法。目的是通过使用反应混合泵作为反应器来实现。

8. 发明申请

US20120123169A1 PROCESS FOR PREPARING ALPHA,BETA-UNSATURATED C10-ALDEHYDES 有权
标题翻译：制备ALPHA，不饱和C10-醛缩合物的方法
公开(公告)号：US20120123169A1
公开(公告)日：2012-05-17
申请号：US13256116
申请日：2010-02-23
申请人： Alfred Kaizik , Dirk Fridag , Hans-Gerd Lueken , Wilfried Bueschken
发明人： Alfred Kaizik , Dirk Fridag , Hans-Gerd Lueken , Wilfried Bueschken
IPC分类号： C07C45/45
CPC分类号： C07C45/74 , Y02P20/582 , C07C47/21
摘要： The invention relates to a method for continuously producing α,β-unsaturated C10-aldehydes from aliphatic C5-aldehydes, comprising the following steps: aldol-condensing aliphatic C5-aldehydes into α,β-unsaturated C10-aldehydes in the presence of an aqueous base in a tube reactor; phase separating the output of the tube reactor into an aqueous catalyst phase and an organic product phase; separating the organic product phase into α,β-unsaturated C10-aldehydes, aliphatic C5-aldehydes, and auxiliary products; discharging a part of the aqueous catalyst phase to remove the reaction water and supplementing said part with liquor solution and subsequently returning said part to the tube reactor. The task of the invention is to improve a method of said kind in a way such that it requires lower energy input. This is achieved in that the aliphatic C5-aldehydes and/or the α,β-unsaturated C10-aldehydes are dispersed in the aqueous base as drops, wherein the average Sauter diameter of the drops is between 0.2 mm and 2 mm.
摘要翻译：本发明涉及从脂肪族C5醛连续生产α，β-不饱和C10醛的方法，包括以下步骤：将脂族C 5 - 醛缩合成α，β-不饱和C10醛，在管式反应器中的水性碱; 将管式反应器的输出相分离成水性催化剂相和有机产物相; 将有机产物相分离成α，β-不饱和C10醛，脂肪族C5醛和辅助产物; 排出一部分水性催化剂相以除去反应水并用液体溶液补充所述部分，随后将所述部分返回到管式反应器。本发明的任务是改进所述种类的方法，使其需要较低的能量输入。这是通过脂肪族C5醛和/或α，β-不饱和C10醛以水滴的形式分散在水性基质中，其中液滴的平均Sauter直径在0.2mm和2mm之间。

9. 发明授权

US07495134B2 Carbonylation method by adding secondary sterically hindered amines 有权
标题翻译：通过添加第二空间位阻胺的羰基化方法
公开(公告)号：US07495134B2
公开(公告)日：2009-02-24
申请号：US12065091
申请日：2006-06-02
申请人： Dieter Hess , Dagmara Ortmann , Oliver Moeller , Klaus-Diether Wiese , Dirk Fridag , Wilfried Bueschken
发明人： Dieter Hess , Dagmara Ortmann , Oliver Moeller , Klaus-Diether Wiese , Dirk Fridag , Wilfried Bueschken
IPC分类号： C07C45/50 , B01J31/00
CPC分类号： C07C45/50 , B01J31/0237 , B01J31/0247 , B01J31/24 , B01J2231/321 , C07F9/65744 , C07C47/02
摘要： The invention relates to a process for reaction of a carbonylatable compound using a metal complex catalyst comprising a metal of transition group VIII and an organophosphorus ligand and in the presence of a stabilizer based on a sterically hindered secondary amine.
摘要翻译：本发明涉及使用包含过渡族VIII金属和有机磷配体的金属络合物催化剂和基于空间位阻仲胺的稳定剂存在下使羰基化化合物反应的方法。

10. 发明授权

US07193116B2 Method for producing aldehydes by means of hydroformylation of olefinically unsaturated compounds, said hydroformylation being catalyzed by unmodified metal complexes in the presence of cyclic carbonic acid esters 有权
标题翻译：通过烯属不饱和化合物的加氢甲酰化制备醛的方法，所述加氢甲酰化在环状碳酸酯存在下由未改性的金属络合物催化
公开(公告)号：US07193116B2
公开(公告)日：2007-03-20
申请号：US10519557
申请日：2003-08-07
申请人： Oliver Moeller , Klaus-Diether Wiese , Dieter Hess , Cornelia Borgmann , Alfred Kaizik , Dirk Fridag
发明人： Oliver Moeller , Klaus-Diether Wiese , Dieter Hess , Cornelia Borgmann , Alfred Kaizik , Dirk Fridag
IPC分类号： C07C45/50
CPC分类号： C07C45/50 , C07D319/06 , Y02P20/584 , C07C47/02
摘要： The present invention relates to a process for preparing aldehydes by hydroformylation catalyzed by metals of groups 8 to 10 of the Periodic Table of the Elements in the presence of cyclic carbonic esters.
摘要翻译：本发明涉及通过在环状碳酸酯存在下元素周期表第8至10族的金属催化的羰基化来制备醛的方法。

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