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1. 发明申请

US20060014970A1 Method for the continuous production of epoxids from olefins and hydroperoxides on a suspended catalyst 审中-公开
标题翻译：在悬浮催化剂上从烯烃和氢过氧化物连续生产环氧化物的方法
公开(公告)号：US20060014970A1
公开(公告)日：2006-01-19
申请号：US10531438
申请日：2003-10-23
申请人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf , Georg Krug , Wolfgang Harder
发明人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf , Georg Krug , Wolfgang Harder
IPC分类号： C07D301/19
CPC分类号： B01J19/2465 , B01J8/20 , B01J19/2475 , B01J2219/00094 , C07D301/12
摘要： Continuous process for the epoxidation of olefins by means of hydroperoxide, in which the epoxidation is carried out in a reactor in which at least one catalyst suspended in a liquid phase is present, wherein the liquid phase is passed through a device which has openings or channels and is installed in the reactor and the epoxide-containing liquid is separated off by means of crossflow filtration so that the suspended catalyst is retained in the reaction system.
摘要翻译：用于通过氢过氧化物环氧化烯烃的连续方法，其中环氧化在其中存在至少一种悬浮在液相中的催化剂的反应器中进行，其中液相通过具有开口或通道的装置并安装在反应器中，并且通过交叉流过滤分离含环氧化物的液体，使得悬浮的催化剂保留在反应体系中。

2. 发明申请

US20070178029A1 Pipe assembly reactor comprising a helically shaped cross section 有权
标题翻译：管组装反应器，其包括螺旋形截面
公开(公告)号：US20070178029A1
公开(公告)日：2007-08-02
申请号：US10586135
申请日：2005-01-20
申请人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf
发明人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf
IPC分类号： B01J19/18
CPC分类号： B01J8/067 , B01J19/2425 , B01J19/243 , B01J19/2445 , B01J2208/00849 , B01J2219/1944 , F28D7/024 , F28F1/02 , F28F1/08
摘要： Process and apparatus for the continuous preparation of a chemical compound in at least one reactor, where at least one of the reactors is a shell-and-tube reactor which has a shell and at least one internal tube located within the shell, wherein at least one of the internal tubes has, at least in part, a noncircular cross section and a helical configuration in the region in which it is surrounded by the shell.
摘要翻译：用于在至少一个反应器中连续制备化学化合物的方法和装置，其中至少一个反应器是壳管式反应器，其具有壳和位于壳内的至少一个内管，其中至少内管中的一个至少部分地具有在其被壳包围的区域中的非圆形横截面和螺旋形构造。

3. 发明申请

US20050250955A1 Method for producing propenyl oxide using a secondary reactor comprising several feed and/or outlet points 审中-公开
标题翻译：使用包含多个进料和/或出口点的二次反应器生产丙烯基氧化物的方法
公开(公告)号：US20050250955A1
公开(公告)日：2005-11-10
申请号：US10521782
申请日：2003-07-28
申请人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf
发明人： Hans-Georg Goebbel , Peter Bassler , Joaquim Teles , Peter Rudolf
IPC分类号： C07D301/12 , C07D301/19
CPC分类号： C07D301/12
摘要： Process for preparing oxiranes by reacting an organic compound with a hydroperoxide in the presence of a solvent and a catalyst, which comprises at least the steps (i) to (iii): (i) reaction of the hydroperoxide with the organic compound to give a product mixture comprising the reacted organic compound and unreacted hydroperoxide, (ii) separation of the unreacted hydroperoxide from the mixture resulting from step (i), (iii) reaction of the hydroperoxide which has been separated off in step (ii) with the organic compound, wherein the reaction in step (iii) is carried out in a tube reactor which has at least two feed points for the reaction mixture comprising at least the organic compound, the hydroperoxide and the solvent or at least two outlets for the product mixture, or at least two feed points and at least two outlets.
摘要翻译：至少在步骤（ⅰ）至（ⅲ）中，至少包括步骤（ⅰ）至（ⅲ）：（i）使有机化合物与氢过氧化物在溶剂和催化剂存在下反应制备环氧乙烷的方法，包含反应的有机化合物和未反应的氢过氧化物的产物混合物，（ii）从步骤（i），（iii）中得到的混合物中分离出未反应的氢过氧化物，（iii）步骤（ii）中已经分离的氢过氧化物与有机化合物其中步骤（iii）中的反应在管式反应器中进行，所述管式反应器具有至少两个进料点，所述反应混合物至少包含有机化合物，氢过氧化物和溶剂，或至少两个用于产物混合物的出口，或至少两个进料点和至少两个出口。

4. 发明授权

US08211822B2 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US08211822B2
公开(公告)日：2012-07-03
申请号：US12556961
申请日：2009-09-10
申请人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
发明人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
IPC分类号： B01J21/06 , B01J21/08
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

5. 发明授权

US08119550B2 Process for epoxidation and catalyst to be used therein 有权
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US08119550B2
公开(公告)日：2012-02-21
申请号：US10526939
申请日：2003-09-16
申请人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
发明人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
IPC分类号： B01J29/06 , C07D301/19
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明还涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的用途。

6. 发明授权

US07608728B2 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US07608728B2
公开(公告)日：2009-10-27
申请号：US10555961
申请日：2004-05-10
申请人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
发明人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

7. 发明申请

US20060167286A1 Process for epoxidation and catalyst to be used therein 有权
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US20060167286A1
公开(公告)日：2006-07-27
申请号：US10526939
申请日：2003-09-16
申请人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： B01J29/04 , C07D301/19
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明还涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的用途。

8. 发明申请

US20070043226A1 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US20070043226A1
公开(公告)日：2007-02-22
申请号：US10555961
申请日：2004-05-10
申请人： Ulrich Muller , Georg Krug , Peter Rudolf , Joaquim Teles , Hans-Georg Gobbel , Peter Bassler
发明人： Ulrich Muller , Georg Krug , Peter Rudolf , Joaquim Teles , Hans-Georg Gobbel , Peter Bassler
IPC分类号： C07D301/19
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

9. 发明申请

US20050085646A1 Process for epoxidation and catalyst to be used therein 审中-公开
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US20050085646A1
公开(公告)日：2005-04-21
申请号：US10960989
申请日：2004-10-12
申请人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： B01J29/89 , B01J37/00 , B01J37/02 , B01J37/08 , B01J37/10 , C07B61/00 , C07D301/03 , C07D301/12 , C07D301/19 , C07D303/04 , C01B33/36 , C01B39/00 , C01F7/00
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention finally relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C—C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明最终涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的应用。

10. 发明申请

US20050054865A1 Catalyst for epoxidation reactions 审中-公开
公开(公告)号：US20050054865A1
公开(公告)日：2005-03-10
申请号：US10938604
申请日：2004-09-13
申请人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
发明人： Ulrich Muller , Georg Krug , Peter Bassler , Hans-Georg Gobbel , Peter Rudolf , Joaquim Teles
IPC分类号： C07D303/04 , B01J29/89 , B01J37/04 , C01B39/06 , C01B39/40 , C07B61/00 , C07D301/12 , C07D301/06 , B01J29/04 , B01J29/87
CPC分类号： C07D301/12 , B01J29/89
摘要： The present invention relates to the manufacture of solid materials or shaped bodies containing at least one zeolite and being at least partly crystalline. Furthermore, the present invention relates to the solid materials or shaped bodies as such and to the use of these materials for reactions of compounds having at least one C—C double bond with at least one hydroperoxide. Specifically, the present invention relates to a process for the manufacture of a solid material containing at least one zeolite and being at least partly crystalline, wherein the synthesis of the said solid material involves at least one partial step of contacting at least one transition metal oxide source with at least one epoxide or hydrolysate thereof prior to or during the at least partial crystallization of said solid material.

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