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1. 发明授权

US07345205B2 Method for the production of tetrahydrogeranylacetone 有权
标题翻译：四氢笨花丙酮生产方法
公开(公告)号：US07345205B2
公开(公告)日：2008-03-18
申请号：US10519684
申请日：2003-07-14
申请人： Hans-Georg Goebbel , Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Thilo Hahn , Klaus Breuer , Werner Aquila
发明人： Hans-Georg Goebbel , Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Thilo Hahn , Klaus Breuer , Werner Aquila
IPC分类号： C07C45/62
CPC分类号： C07C45/62 , C07C49/04
摘要： A process is described for preparing tetrahydrogeranylacetone in which pseudoionone, geranylacetone and/or dihydrogeranylacetone in a liquid phase, in which particles of a catalyst which is capable of preferentially hydrogenating carbon-carbon double bonds over carbon-oxygen double bonds are suspended, is conducted through a device which inhibits the transport of the catalyst particles in the presence of a hydrogen-containing gas.
摘要翻译：描述了一种制备四氢ger anyl anyl A A is ger ger ger through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through 在含氢气体的存在下抑制催化剂颗粒的输送的装置。

2. 发明申请

US20060211898A1 Method for the production of tetrahydrogeranylacetone 有权
标题翻译：四氢笨花丙酮生产方法
公开(公告)号：US20060211898A1
公开(公告)日：2006-09-21
申请号：US10519684
申请日：2003-07-14
申请人： Hans-Georg Goebbel , Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Thilo Hahn , Klaus Breuer , Werner Aquila
发明人： Hans-Georg Goebbel , Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Thilo Hahn , Klaus Breuer , Werner Aquila
IPC分类号： C07C11/00
CPC分类号： C07C45/62 , C07C49/04
摘要： A process is described for preparing tetrahydrogeranylacetone in which pseudoionone, geranylacetone and/or dihydrogeranylacetone in a liquid phase, in which particles of a catalyst which is capable of preferentially hydrogenating carbon-carbon double bonds over carbon-oxygen double bonds are suspended, is conducted through a device which inhibits the transport of the catalyst particles in the presence of a hydrogen-containing gas.
摘要翻译：描述了一种制备四氢ger anyl anyl A A is ger ger ger through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through through 在含氢气体的存在下抑制催化剂颗粒的输送的装置。

3. 发明授权

US07090748B2 Dividing-wall column with feed in whole or in part in the vaporous state and/or side stream take off in whole or in part in the vaporous state 有权
公开(公告)号：US07090748B2
公开(公告)日：2006-08-15
申请号：US10319715
申请日：2002-12-16
申请人： Gerd Kaibel , Christian Miller , Katrin Klass , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
发明人： Gerd Kaibel , Christian Miller , Katrin Klass , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
IPC分类号： B01D3/00
CPC分类号： B01D3/141 , B01D3/14 , Y10S203/11 , Y10S203/20
摘要： A dividing-wall column having a dividing wall which is essentially disposed along the long direction of the column is proposed, which divides the column interior into a feed part, a take off part, an upper shared column part and a lower shared column part, with feed in whole or in part in the vaporous state of a mixture to be separated between the upper region of the feed part and the lower region of the feed part and/or side stream take off in whole or in part in the vaporous state between the upper region of the take off part and the lower region of the take off part, where if feed is in whole or in part in the vaporous state the cross-sectional area of the upper region of the feed part is increased by plane-parallel displacement of the dividing wall toward the upper region of the take off part, and/or if the side stream take off is in whole or in part in the vaporous state, the cross-sectional area of the lower region of the take off part is increased by displacement of the dividing wall toward the lower region of the feed part, in such a manner that the F factor is substantially the same in all column regions.

4. 发明申请

US20060157336A1 Dividing-wall column with feed in whole or in part in the vaporous state and/or side stream take off in whole or in part in the vaporous state 有权
公开(公告)号：US20060157336A1
公开(公告)日：2006-07-20
申请号：US11384370
申请日：2006-03-21
申请人： Gerd Kaibel , Christian Miller , Katrin Klass , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
发明人： Gerd Kaibel , Christian Miller , Katrin Klass , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
IPC分类号： B01D3/00
CPC分类号： B01D3/141 , B01D3/14 , Y10S203/11 , Y10S203/20
摘要： A dividing-wall column having a dividing wall which is essentially disposed along the long direction of the column is proposed, which divides the column interior into a feed part, a take off part, an upper shared column part and a lower shared column part, with feed in whole or in part in the vaporous state of a mixture to be separated between the upper region of the feed part and the lower region of the feed part and/or side stream take off in whole or in part in the vaporous state between the upper region of the take off part and the lower region of the take off part, where if feed is in whole or in part in the vaporous state the cross-sectional area of the upper region of the feed part is increased by plane-parallel displacement of the dividing wall toward the upper region of the take off part, and/or if the side stream take off is in whole or in part in the vaporous state, the cross-sectional area of the lower region of the take off part is increased by displacement of the dividing wall toward the lower region of the feed part, in such a manner that the F factor is substantially the same in all column regions.

5. 发明授权

US07264696B2 Dividing-wall column with feed in whole or in part in the vaporous state and/or side stream take off in whole or in part in the vaporous state 有权
标题翻译：全部或部分进料在蒸发态和/或侧流中的分隔壁塔全部或部分脱气
公开(公告)号：US07264696B2
公开(公告)日：2007-09-04
申请号：US11384370
申请日：2006-03-21
申请人： Gerd Kaibel , Christian Miller , Katrin Klaβ , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
发明人： Gerd Kaibel , Christian Miller , Katrin Klaβ , Alois Kindler , Werner Aquila , Walter Dobler , Klaus Breuer , Achim Pommer , Thomas Dirnsteiner
IPC分类号： B01D3/42
CPC分类号： B01D3/141 , B01D3/14 , Y10S203/11 , Y10S203/20
摘要： A dividing-wall column having a dividing wall which is essentially disposed along the long direction of the column is proposed, which divides the column interior into a feed part, a take off part, an upper shared column part and a lower shared column part, with feed in whole or in part in the vaporous state of a mixture to be separated between the upper region of the feed part and the lower region of the feed part and/or side stream take off in whole or in part in the vaporous state between the upper region of the take off part and the lower region of the take off part, where if feed is in whole or in part in the vaporous state the cross-sectional area of the upper region of the feed part is increased by plane-parallel displacement of the dividing wall toward the upper region of the take off part, and/or if the side stream take off is in whole or in part in the vaporous state, the cross-sectional area of the lower region of the take off part is increased by displacement of the dividing wall toward the lower region of the feed part, in such a manner that the F factor is substantially the same in all column regions.
摘要翻译：提出了具有分隔壁的分隔壁，该分隔壁基本上沿着塔的长方向设置，其将塔内部分为进料部分，脱落部分，上共享塔部分和下共享塔部分，在进料部分的上部区域和进料部分的下部区域和/或侧馏分之间在蒸气状态下的全部或部分蒸气状态下的进料全部或部分地在蒸气状态之间分离，取出部分的上部区域和脱落部分的下部区域，如果进料全部或部分处于气态，则进料部分的上部区域的横截面面积被平面平行地增加分流壁向脱气部的上部区域的位移，和/或侧流的脱落全部或部分处于蒸发状态，脱落部的下部区域的截面积为由分界位移增加壁朝向馈送部分的下部区域，使得F因子在所有列区域中基本相同。

6. 发明授权

US07476297B2 Device and method for carrying out heterogeneously-catalysed reactive distillations in particular for the production of pseudoionone 失效
标题翻译：用于进行非均相催化反应蒸馏的装置和方法，特别是用于生产假性离子
公开(公告)号：US07476297B2
公开(公告)日：2009-01-13
申请号：US10497520
申请日：2002-12-05
申请人： Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Marcus Sigl , Helmut Jansen , Björn Kaibel
发明人： Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Marcus Sigl , Helmut Jansen , Björn Kaibel
IPC分类号： B01D3/32 , B01J8/02 , B01J19/32
CPC分类号： C07C45/74 , B01D3/009 , B01J8/003 , B01J8/0292 , B01J8/12 , B01J19/249 , B01J19/32 , B01J21/04 , B01J23/10 , B01J35/026 , B01J2219/2453 , B01J2219/2459 , B01J2219/2471 , B01J2219/2481 , B01J2219/2497 , B01J2219/3221 , B01J2219/32217 , B01J2219/32227 , B01J2219/32237 , B01J2219/32258 , B01J2219/32262 , B01J2219/32408 , B01J2219/32466 , B01J2219/326 , C07C45/72 , Y02P20/127 , Y10S203/06 , C07C49/203
摘要： A column is described for carrying out reactive distillations in the presence of a heterogeneous particulate catalyst having an ordered packing or random packings which form intermediate spaces in the column interior, the quotient of the hydraulic diameter for the gas flow through the ordered packing or the random packings and the equivalent diameter of the catalyst particles being in the range from 2 to 20, preferably in the range from 5 to 10, in such a manner that the catalyst particles are introduced into the intermediate spaces, distributed and discharged loose under the action of gravity.
摘要翻译：描述了一种柱，用于在具有在柱内部形成中间空间的有序填料或无规填料的非均相颗粒催化剂存在下进行反应性蒸馏，通过有序填料的气流的液压直径或随机的填料和催化剂颗粒的当量直径在2至20范围内，优选在5至10范围内，使得催化剂颗粒被引入中间空间，在重力。

7. 发明申请

US20050016830A1 Device and method for carrying out heterogeneously-catalysed reactive distillations in particular for the production of pseudoionone 失效
标题翻译：用于进行非均相催化反应蒸馏的装置和方法，特别是用于生产假性离子
公开(公告)号：US20050016830A1
公开(公告)日：2005-01-27
申请号：US10497520
申请日：2002-12-05
申请人： Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Marcus Sigl , Helmut Jansen , Bjorn Kaibel
发明人： Gerd Kaibel , Christian Miller , Walter Dobler , Thomas Dirnsteiner , Marcus Sigl , Helmut Jansen , Bjorn Kaibel
IPC分类号： B01D3/26 , B01D3/00 , B01J8/00 , B01J8/02 , B01J8/04 , B01J8/12 , B01J19/24 , B01J19/32 , B01J21/04 , B01J23/10 , B01J35/02 , C07B61/00 , C07C45/72 , C07C45/74 , C07C49/203 , B01D3/34
CPC分类号： C07C45/74 , B01D3/009 , B01J8/003 , B01J8/0292 , B01J8/12 , B01J19/249 , B01J19/32 , B01J21/04 , B01J23/10 , B01J35/026 , B01J2219/2453 , B01J2219/2459 , B01J2219/2471 , B01J2219/2481 , B01J2219/2497 , B01J2219/3221 , B01J2219/32217 , B01J2219/32227 , B01J2219/32237 , B01J2219/32258 , B01J2219/32262 , B01J2219/32408 , B01J2219/32466 , B01J2219/326 , C07C45/72 , Y02P20/127 , Y10S203/06 , C07C49/203
摘要： A column is described for carrying out reactive distillations in the presence of a heterogeneous particulate catalyst having an ordered packing or random packings which form intermediate spaces in the column interior, the quotient of the hydraulic diameter for the gas flow through the ordered packing or the random packings and the equivalent diameter of the catalyst particles being in the range from 2 to 20, preferably in the range from 5 to 10, in such a manner that the catalyst particles are introduced into the intermediate spaces, distributed and discharged loose under the action of gravity.
摘要翻译：描述了一种柱，用于在具有在柱内部形成中间空间的有序填料或无规填料的非均相颗粒催化剂存在下进行反应性蒸馏，通过有序填料的气流的液压直径或随机的填料和催化剂颗粒的当量直径在2至20范围内，优选在5至10范围内，使得催化剂颗粒被引入中间空间，在重力。

8. 发明授权

US4720327A Distillative separation of liquid mixtures of substances 失效
标题翻译：物质液体混合物的蒸馏分离
公开(公告)号：US4720327A
公开(公告)日：1988-01-19
申请号：US420485
申请日：1982-09-20
申请人： Werner Aquila , Axel Nissen , Gerd Kaibel , Michael Horner , Walter Rebafka
发明人： Werner Aquila , Axel Nissen , Gerd Kaibel , Michael Horner , Walter Rebafka
IPC分类号： A61K8/33 , A61Q13/00 , B01D3/34 , C07B31/00 , C07B63/00 , C07C27/00 , C07C29/141 , C07C29/80 , C07C31/04 , C07C33/025 , C07C45/00 , C07C45/82 , C07C47/21 , C07C67/00 , C11B9/00 , C11B9/02 , B01D3/38
CPC分类号： C07C45/82 , B01D3/34 , C11B9/027 , Y10S203/24 , Y10S203/90
摘要： Distillative separation of liquid mixtures of one or more water-insoluble substances which have boiling points higher than that of water and one or more substances which have boiling points lower than that of water or which form azeotropes having boiling points lower than that of water, wherein the mixture to be distilled is mixed with a quantity of water such that the boiling point of the water under the pressure applied limits the bottom temperature of the mixture of substances to be separated.
摘要翻译：沸点高于水的一种或多种水不溶性物质的液体混合物的蒸馏分离和一种或多种沸点低于水的沸点或者沸点低于水的沸点的物质，其中将要蒸馏的混合物与一定量的水混合，使得在施加压力下的水的沸点限制待分离物质的混合物的底部温度。

9. 发明授权

US06211114B1 Catalyst and process for preparing 2-buten-1-ol compounds 失效
公开(公告)号：US06211114B1
公开(公告)日：2001-04-03
申请号：US08957322
申请日：1997-11-06
申请人： Franz Josef Bröcker , Werner Aquila , Klemens Flick , Gerd Kaibel , Ernst Langguth
发明人： Franz Josef Bröcker , Werner Aquila , Klemens Flick , Gerd Kaibel , Ernst Langguth
IPC分类号： B01J27057
CPC分类号： B01J27/0573 , B01J23/44 , B01J27/0576 , B01J35/10 , C07C29/56 , C07C33/025
摘要： The fixed-bed catalyst comprises palladium and selenium or tellurium or a mixture of selenium and tellurium on a silicon dioxide support and has a BET surface area of from 80 to 380 m2/g and a pore volume of from 0.6 to 0.95 cm3/g in the pore diameter range from 3 nm to 300 &mgr;m, with from 80 to 95% of the pore volume being in the pore diameter range from 10 to 100 nm. It is prepared by impregnating a silicon dioxide support with a solution of a palladium compound and a selenium compound or tellurium compound or a mixture of a selenium compound and a tellurium compound, drying it and reducing it in the presence of hydrogen. The catalyst is used, in particular, for isomerizing 3-buten-1-ol compounds.

10. 发明授权

US06175044B1 Preparation of citral 有权
标题翻译：柠檬醛的制备
公开(公告)号：US06175044B1
公开(公告)日：2001-01-16
申请号：US09404548
申请日：1999-09-24
申请人： Jörg Therre , Gerd Kaibel , Werner Aquila , G{umlaut over (u)}nter Wegner , Hartwig Fuchs
发明人： Jörg Therre , Gerd Kaibel , Werner Aquila , G{umlaut over (u)}nter Wegner , Hartwig Fuchs
IPC分类号： C07C4551
CPC分类号： C07C45/515 , C07C45/513 , C07C45/67 , C07C47/21
摘要： 3,7-Dimethyl-2,6-octadien-1-al of formula I is prepared continuously by: thermally cleaving, in the presence or absence of an acid catalyst, 3-methyl-2-buten-1-al diprenyl acetal of formula II: thereby eliminating 3-methyl-2-buten-1-ol of formula III and yielding cis/trans-prenyl 3-methylbutadienyl ether of formula IV: thermally rearranging the resultant butadienyl ether of formula IV thereby yielding 2,4,4-trimethyl-3-formyl-1,5-hexadiene of formula V: subsequently rearranging intermediate (V) thereby yielding citral product of formula I, which comprises: as the reaction proceeds, continuously distilling the reaction mixture thereby continuously removing prenol, which is formed by degradation of acetal II, and the intermediates of formula IV and V and any citral product which is formed during the reaction; and thermally rearranging said intermediates of formula IV and V at a temperature of 100-200° C. in the absence or presence of said prenol to form citral product.
摘要翻译：通过以下方式连续制备式I的3,7-二甲基-2,6-辛二烯-1-醇：在存在或不存在酸催化剂的情况下，热裂解3-甲基-2-丁烯-1-al阮内烯式II：由此除去式III的3-甲基-2-丁烯-1-醇，得到式IV的顺/反 - 异戊烯基3-甲基丁二烯基醚：热重新排列所得的式IV的丁二烯基醚，由此得到2,4,4 式V的 - 三甲基-3-甲酰基-1,5-己二烯：随后重新排列中间体（V），从而产生式I的柠檬醛产物，其包括：随着反应的进行，连续蒸馏反应混合物，从而连续除去前醇，由缩醛II的降解形成，以及式IV和V的中间体以及在反应期间形成的任何柠檬醛产物; 在不存在或存在所述prenol的情况下，在100-200℃的温度下热处理所述式IV和V的中间体，以形成柠檬醛产物。

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