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1. 发明授权

US06300508B1 Thickened aqueous surfactant solutions 失效
标题翻译：增稠水性表面活性剂溶液
公开(公告)号：US06300508B1
公开(公告)日：2001-10-09
申请号：US09109341
申请日：1998-06-30
申请人： Hans-Christian Raths , Norman Milstein , Werner Seipel
发明人： Hans-Christian Raths , Norman Milstein , Werner Seipel
IPC分类号： C07C5100
CPC分类号： C11D1/83 , C07C67/26 , C11D1/143 , C11D1/146 , C11D1/662 , C11D1/74 , C11D1/825 , C07C69/28 , C07C69/003
摘要： Fatty acid esters of alkylene glycols corresponding to the formula R1COO(AlkO)nH are thickeners for aqueous surfactant solutions, particularly for personal care products.
摘要翻译：对应于式R1COO（AlkO）nH的亚烷基二醇的脂肪酸酯是水性表面活性剂溶液的增稠剂，特别是用于个人护理产品。

2. 发明授权

US5936107A Process for the production of fatty acid polyethylene glycol esters 失效
标题翻译：生产脂肪酸聚乙二醇酯的方法
公开(公告)号：US5936107A
公开(公告)日：1999-08-10
申请号：US767123
申请日：1996-12-09
申请人： Hans-Christian Raths , Ansgar Behler , Norman Milstein
发明人： Hans-Christian Raths , Ansgar Behler , Norman Milstein
IPC分类号： B01J31/02 , C07C67/26 , C07C69/28 , C07C69/52 , C08G65/26 , C07C51/00
CPC分类号： C08G65/2672 , C07C67/26 , C08G65/2615
摘要： Fatty acid polyethylene glycol esters of the formula (I):R.sup.1 CO(CH.sub.2 CH.sub.2 O).sub.n H (I)wherein R.sup.1 CO is a linear or branched, aliphatic, saturated and/or unsaturated acyl group having from about 6 to about 22 carbon atoms and n is a number from 0.5 to 1.5 are made by reacting ethylene oxide and a fatty acid in the presence of an alkanolamine in a homogeneous reaction medium.
摘要翻译：式（I）的脂肪酸聚乙二醇酯：R1CO（CH2CH2O）nH（I）其中R1CO是具有约6至约22个碳原子的直链或支链，脂族，饱和和/或不饱和的酰基，n是在均一的反应介质中，在链烷醇胺存在下使环氧乙烷和脂肪酸反应制备0.5至1.5的数。

3. 发明授权

US5473089A Process for the production of ammonium fatty acid hydroxyalkanesulfonates 失效
标题翻译：生产铵型脂肪酸羟基烷基磺酸盐的方法
公开(公告)号：US5473089A
公开(公告)日：1995-12-05
申请号：US227846
申请日：1994-04-14
申请人： Bernhard Gutsche , Timothy J. Cassady , Lutz Jeromin , Gerhard Wollmann , Norman Milstein , Hans-Christian Raths
发明人： Bernhard Gutsche , Timothy J. Cassady , Lutz Jeromin , Gerhard Wollmann , Norman Milstein , Hans-Christian Raths
IPC分类号： C07C303/32 , C07C309/12 , C07B45/00
CPC分类号： C07C303/32
摘要： Ammonium fatty acid hydroxyalkanesulfonates are made by a process in which (a) ammonium hydroxyalkanesulfonate corresponding to general formula (I):HO--(C.sub.n H.sub.2n)--SO.sub.3 NH.sub.4 (I)wherein n=2 to 4, is subjected to the esterification reaction with a fatty acid corresponding to the formula (II)R--COOH (II)wherein RCO is an aliphatic, linear or branched acyl radical containing 6 to 18 carbon atoms, in the presence of an esterification catalyst, characterized in that (a) before the esterification reaction, the starting compounds corresponding to formulae (I) and (II) are dried at a temperature of 120.degree. C. to 160.degree. C. and under a pressure of 100 to 700 mbar; (b) the esterification reaction is carried out at a temperature above 160.degree. C. to 195.degree. C. and under a pressure of 250 mbar to atmospheric pressure; (c) water of solution and water of reaction formed are directly removed from the reaction mixture; (d) the catalyst is neutralized with a base on completion of the reaction.
摘要翻译：脂肪酸羟基烷基磺酸铵通过以下方法制备：（a）对应于通式（I）的羟基链烷磺酸铵：其中n = 2至4的HO-（CnH2n）-SO3NH4（I）与脂肪进行酯化反应对应于式（II）R-COOH（II）的酸，其中RCO是含有6至18个碳原子的脂族，直链或支链酰基，在酯化催化剂存在下，其特征在于（a）酯化反应对应于式（I）和（II）的起始化合物在120℃至160℃的温度和100至700毫巴的压力下干燥; （b）酯化反应在160℃至195℃和250毫巴至大气压的压力下进行; （c）直接从反应混合物中除去所形成反应的溶液和水; （d）催化剂在反应完成时用碱中和。

4. 发明授权

US07387786B2 Food additive compositions containing sterol esters, solubilizing agents, dispersants and antioxidants 失效
标题翻译：含有甾醇酯，增溶剂，分散剂和抗氧化剂的食品添加剂组合物
公开(公告)号：US07387786B2
公开(公告)日：2008-06-17
申请号：US10702316
申请日：2003-11-05
申请人： Norman Milstein , Manfred Biermann , Peter Leidl , Rainer Von Kries
发明人： Norman Milstein , Manfred Biermann , Peter Leidl , Rainer Von Kries
IPC分类号： A61K47/00 , A61K31/56
CPC分类号： A23D9/013 , A23D9/007 , A23L33/11 , Y10S426/804
摘要： A food additive useful for lowering serum cholesterol in humans contains a sterol or stanol ester of a fatty acid or a dicarboxylic acid ester of a sterol or stanol made by reacting a sterol, stanol and a carboxylic acid in the presence of an effective amount of a catalyst selected from the group consisting of calcium oxide, calcium hydroxide, a calcium salt of a carboxylic acid, magnesium hydroxide and combinations thereof described herein below.
摘要翻译：可用于降低人体血清胆固醇的食品添加剂含有通过使甾醇，甾烷醇和羧酸在有效量的存在下进行反应制得的固醇或甾烷醇的脂肪酸或二醇酸酯的甾醇或甾烷醇酯催化剂选自氧化钙，氢氧化钙，羧酸钙盐，氢氧化镁及其组合，如下文所述。

5. 发明授权

US5763632A Process for making isethionate ester salts 失效
标题翻译：制备羟乙基磺酸酯盐的方法
公开(公告)号：US5763632A
公开(公告)日：1998-06-09
申请号：US598159
申请日：1996-02-07
申请人： Timothy John Cassady , Norman Milstein , Richard P. Crews
发明人： Timothy John Cassady , Norman Milstein , Richard P. Crews
IPC分类号： C07C303/02 , C07C303/32 , C07C309/68 , C11D1/12 , C07C303/00
CPC分类号： C07C303/22 , C07C303/32 , C11D1/126
摘要： Fatty acid esters of isethionate salts are made by reacting ethylene oxide and a bisulfite salt in an aqueous solution while maintaining the pH in the range of from about 5.5 to about 6.5 and while maintaining the temperature in the range of from 25.degree. C. to 85.degree. C. to form an isethionate salt. The isethionate salt is then esterified with a fatty acid to produce a product having little or no unwanted fatty acid esters of ethylene glycol.
摘要翻译：羟乙基磺酸盐的脂肪酸酯是通过环氧乙烷和亚硫酸氢盐在水溶液中反应而制成的，同时保持pH在约5.5至约6.5的范围内，同时保持温度在25℃至85℃ DEG以形成羟乙基磺酸盐。然后将羟乙基磺酸盐用脂肪酸酯化，得到很少或没有不需要的乙二醇脂肪酸酯的产物。

6. 发明授权

US07220432B2 Vegetable substitute for lanolin 失效
标题翻译：蔬菜替代羊毛脂
公开(公告)号：US07220432B2
公开(公告)日：2007-05-22
申请号：US10686478
申请日：2003-10-15
申请人： Gary J. Dee , Norman Milstein , Barry A. Salka , Judy Zhuang , Stefan Bruening
发明人： Gary J. Dee , Norman Milstein , Barry A. Salka , Judy Zhuang , Stefan Bruening
IPC分类号： A61K9/00 , A61K7/00
CPC分类号： A61K8/39 , A61K8/375 , A61K8/63 , A61K8/922 , A61K8/97 , A61K31/74 , A61Q19/00
摘要： Lanolin-free lanolin substitute compositions comprising: A) from about 5 to about 95% by weight, of at least one plant sterol fatty acid ester; B) from about 1 to about 20% by weight, of at least one polyglyceryl di-polyhydroxy fatty acid ester; C) from about 1 to about 20% by weight, of at least one polyglyceryl di-fatty acid ester; D) from about 0.25 to about 10% by weight of at least one glyceryl fatty acid ester; and E) optionally, from about 1 to 80% by weight of an additive containing a mixture of (i) a vegetable oil, (ii) a hydrogenated vegetable oil, and (iii) a non-petroleum derived wax.
摘要翻译：无羊毛脂的羊毛脂替代组合物，其包含：A）约5至约95重量％的至少一种植物甾醇脂肪酸酯; B）约1至约20重量％的至少一种聚甘油二 - 多羟基脂肪酸酯; C）约1至约20重量％的至少一种聚甘油二脂肪酸酯; D）约0.25至约10重量％的至少一种甘油脂肪酸酯; 和E）任选地，约1至80重量％的添加剂，其含有（i）植物油，（ii）氢化植物油和（iii）非石油衍生的蜡的混合物。

7. 发明授权

US07247606B2 Branched reaction products 有权
标题翻译：分支反应产物
公开(公告)号：US07247606B2
公开(公告)日：2007-07-24
申请号：US10265004
申请日：2002-10-04
申请人： Stephen F. Gross , Norman Milstein
发明人： Stephen F. Gross , Norman Milstein
IPC分类号： B01F17/46 , B01D19/04 , C07C217/04 , C07C217/28 , C09D11/00 , C10M173/00 , C09K3/00
CPC分类号： C07C217/50 , C07C217/28 , C09D5/024 , C11D1/002 , C11D1/44
摘要： A compound of formula: wherein each R group independently is C6-C10 arylene group, a straight or branched chain C2-C°alkylene group optionally containing an arylene group, or a C4-C20 straight chain alkylene group containing one or more —NH— groups in the alkylene chain, each X is —O—, —S—, or —NR5— where R5 is hydrogen or C1-C6 alkyl, each AO group is independently ethyleneoxy, 1,2-propyleneoxy, or 1,2-butyleneoxy, n, m and p is from 1 to 50 and the sum of n, m and p is from 4 to 50, and the R4 is independently —CH2-CH(OH)—R9, wherein each R9 independently represents a C4-C18 saturated or unsaturated, substituted or unsubstituted hydrocarbon group. The compound has surfactant and defoaming properties and is useful in latex paint, an ink, an adhesive, or a metal working compositions.
摘要翻译：下式化合物：其中每个R基团独立地为C 6 -C 10亚芳基，直链或支链C 2 -C 任选地含有亚芳基的亚烷基或含有一个或多个-NH-基团的C 4-14 -C 20直链亚烷基亚烷基链，每个X是-O - ， - S - 或-NR 5 - ，其中R 5是氢或C 1 -C 每个AO基团独立地是乙烯氧基，1,2-亚丙氧基或1,2-亚丁基氧基，n，m和p是1至50，并且n，m和p的和是 4至50，且R 4独立地为-CH 2 -CH（OH）-R 9，其中每个R 9独立地表示饱和或不饱和的，取代或未取代的烃基的C 4-14 -C 18亚烷基。该化合物具有表面活性剂和消泡性能，并且可用于乳胶漆，油墨，粘合剂或金属加工组合物。

8. 发明授权

US5939081A Esters of alkyl and/or alkenyl oligoglycosides with fatty acids 失效
标题翻译：烷基和/或烯基低聚糖苷与脂肪酸的酯
公开(公告)号：US5939081A
公开(公告)日：1999-08-17
申请号：US806878
申请日：1997-02-26
申请人： Achim Ansmann , Rolf Kawa , Annette Kreisig , Norman Milstein
发明人： Achim Ansmann , Rolf Kawa , Annette Kreisig , Norman Milstein
IPC分类号： A61K8/60 , A61Q19/00 , A61K7/00 , A61K7/48
CPC分类号： A61K8/604 , A61K8/06 , A61Q19/00 , Y10S514/937 , Y10S514/938
摘要： A process for thickening a water-in-oil and oil-in-water emulsion involving adding to the emulsion a thickening agent consisting of an alkyl or alkenyl oligoglucoside ester formed by esterifying an alkyl or alkenyl oligoglycoside corresponding to formula I:R.sup.1 O--�G!.sub.p (I)wherein R.sup.1 is an alkyl or alkenyl oligoglucoside containing from about 4 to about 22 carbon atoms, G is a sugar unit containing from 5 to 6 carbon atoms, and p is a number having a value of from 1 to about 10, with a fatty acid corresponding to formula II:R.sup.2 CO--OH (II)wherein R.sup.2 CO is an aliphatic acyl radical containing from about 6 to about 22 carbon atoms, and up to about 3 double bonds.
摘要翻译：一种用于增稠油包水和水包油乳液的方法，包括向乳液中加入由通过酯化对应于式I的烷基或烯基低聚糖苷形成的烷基或烯基低聚葡糖苷酯组成的增稠剂：R 1 O- [G ] p（I）其中R1是含有约4至约22个碳原子的烷基或烯基低聚葡糖苷，G是含有5至6个碳原子的糖单元，p是1至约10的数值与对应于式II的脂肪酸：R2CO-OH（II），其中R2CO是含有约6至约22个碳原子的脂族酰基，以及至多约3个双键。

9. 发明授权

US5110981A Process for making alkyl naphthalene sulfonate surfactants 失效
标题翻译：制备烷基萘磺酸盐表面活性剂的方法
公开(公告)号：US5110981A
公开(公告)日：1992-05-05
申请号：US717131
申请日：1991-06-18
申请人： Norman Milstein
发明人： Norman Milstein
IPC分类号： B01F17/12 , C07C309/37 , C11D1/22
CPC分类号： C11D1/22
摘要： Incremental alternating additions of sulfonating agent acids and alkylating alcohols give superior results in the synthesis of alkyl naphthalene sulfonate surfactant products from naphthalene starting material.
摘要翻译：磺化剂酸和烷基化醇的增量交替添加在萘原料合成烷基萘磺酸盐表面活性剂产物方面提供了优异的结果。

10. 发明授权

US07217432B2 Vegetable substitute for lanolin 失效
标题翻译：蔬菜替代羊毛脂
公开(公告)号：US07217432B2
公开(公告)日：2007-05-15
申请号：US10393149
申请日：2003-03-20
申请人： Gary J. Dee , Norman Milstein , Barry A. Salka
发明人： Gary J. Dee , Norman Milstein , Barry A. Salka
IPC分类号： A61K9/00 , A61K7/00
CPC分类号： A61K8/375 , A61K8/39 , A61K8/63 , A61K8/97 , A61Q19/00
摘要： Lanolin-free lanolin substitute compositions comprising: A) from about 50 to about 95% by weight, of at least one plant sterol fatty acid ester; B) from about 1 to about 10% by weight, of at least one polyglyceryl di-polyhydroxy fatty acid ester; C) from about 1 to about 10% by weight, of at least one polyglyceryl di-fatty acid ester; and D) from about 0.25 to about 2% by weight of at least one glyceryl fatty acid ester.
摘要翻译：无羊毛脂的羊毛脂替代组合物，其包含：A）约50至约95重量％的至少一种植物甾醇脂肪酸酯; B）约1至约10重量％的至少一种聚甘油二 - 多羟基脂肪酸酯; C）约1至约10重量％的至少一种聚甘油二脂肪酸酯; 和D）约0.25至约2重量％的至少一种甘油脂肪酸酯。

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