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1. 发明授权

US4430494A Melamine resins, a process for their preparation and their use and molding compositions produced from the resins 失效
标题翻译：三聚氰胺树脂，其制备方法及其用途和由树脂制备的模塑组合物
公开(公告)号：US4430494A
公开(公告)日：1984-02-07
申请号：US429464
申请日：1982-09-30
申请人： Hans Honel , Walter Michel , Steffen Piesch , Karin Schluter , Alfons Wolf
发明人： Hans Honel , Walter Michel , Steffen Piesch , Karin Schluter , Alfons Wolf
IPC分类号： C08G12/00 , C08G12/30 , C08G12/34 , C08G12/40 , C08G12/42 , C08L61/00 , C08L61/20 , C08L61/30 , C08L61/32
CPC分类号： C08L61/30 , C08G12/34 , C08G12/42 , C08L61/32
摘要： Modified melamine-formaldehyde resins having a melamine:formaldehyde molar ratio of 1:(1.27 to 0.7) are prepared by heating melamine in an aqueous solution or suspension with formaldehyde in a melamine:formaldehyde molar ratio of 1:(1.27 to 0.7) at a pH value of 8 to 11 and at temperatures of 105.degree. to 160.degree. C. until the finished resin has reached a dilutability with water of 1:(0.1 to 4) at 20.degree. C., and, before, during or after the condensation reaction, adding less than 25% by weight of a glycol ether of the formulaR(OCH.sub.2 CH.sub.2).sub.n OHin which R denotes alkyl having 1 to 4 C atoms and n denotes an integer from 1 to 5, and/or of p-toluenesulfonamide. The resins are used in particular for the production of molding compositions.
摘要翻译： PCT No.PCT / EP82 / 00013 Sec。 371日期1982年9月30日 102（e）1982年9月30日PCT申请日1982年1月25日PCT公布。出版物WO82 / 02717 日本1982年8月19日。具有三聚氰胺：甲醛摩尔比为1：（1.27〜0.7）的改性三聚氰胺 - 甲醛树脂通过以三聚氰胺：甲醛摩尔比为1：1的甲醛在水溶液或悬浮液中加热蜜胺来制备。（1.27〜0.7），pH值为8〜11，温度为105〜160℃，直到成品树脂在20℃下达到1：（0.1〜4）的水的稀释性，在缩合反应之前，期间或之后，加入少于25重量％的式R（OCH 2 CH 2）n OH的二醇醚，其中R表示具有1至4个C原子的烷基，n表示1至5的整数，以及 /或对甲苯磺酰胺。这些树脂特别用于生产模塑组合物。

2. 发明授权

US4430380A Bonded structures of textile materials 失效
标题翻译：纺织材料的粘结结构
公开(公告)号：US4430380A
公开(公告)日：1984-02-07
申请号：US360217
申请日：1982-03-22
申请人： Hans Honel , Walter Michel , Steffen Piesch , Karin Schluter , Manfred Seidel , Wolfgang Spieler
发明人： Hans Honel , Walter Michel , Steffen Piesch , Karin Schluter , Manfred Seidel , Wolfgang Spieler
IPC分类号： C08G12/32 , C08G12/34 , C08G12/40 , C08J5/24 , D04H1/435 , D04H1/587 , D04H1/64 , B32B7/00
CPC分类号： D04H1/587 , C08G12/32 , C08G12/34 , C08G12/40 , C08J5/24 , D04H1/435 , D04H1/64 , C08J2361/28 , Y10T442/2762 , Y10T442/2844 , Y10T442/2861 , Y10T442/2893 , Y10T442/2918
摘要： A bonded structure of textile materials bonded by a melamine-formaldehyde precondensate is produced by applying to a textile material a melamine-formaldehyde precondensate with a molar ratio of melamine to formaldehyde of 1:(0.8 to 1.26) to form a composite and then compressing the composite with an overpressure of 1 to 200 bars at temperature of from 130.degree. to 220.degree. C.
摘要翻译：通过将三聚氰胺 - 甲醛预缩合物结合的纺织材料的粘结结构体通过将摩尔比为三聚氰胺与甲醛的摩尔比为1：（0.8至1.26）的三聚氰胺 - 甲醛预缩合物一起应用于纺织材料而形成复合材料，然后压缩复合物在130〜220℃的温度下具有1〜200巴的超压。

3. 发明授权

US4081426A Preparation of aminoplasts 失效
标题翻译：氨基塑料的制备
公开(公告)号：US4081426A
公开(公告)日：1978-03-28
申请号：US677131
申请日：1976-04-15
申请人： Walter Michel , Hans Honel , Manfred Schon
发明人： Walter Michel , Hans Honel , Manfred Schon
IPC分类号： C07D251/18 , C07D251/64 , C07D251/70 , C08G12/00 , C08G12/30 , C08G12/32 , C08G12/42 , C08G12/26
CPC分类号： C08G12/30 , C07D251/64 , C08G12/425
摘要： Aminoplast preparation is greatly speeded by condensing an aminotriazine such as melamine with formaldehyde and etherifying alkanol under superatmospheric pressure and at a temperature between about 80.degree. and about 130.degree. C.
摘要翻译：通过在超大气压和约80℃至约130℃之间的温度下将氨基三嗪如三聚氰胺与甲醛和醚化链烷醇缩合，大大加快了氨基塑料的制备。

4. 发明授权

US4271286A Process for the preparation of etherified methylolaminotriazines 失效
标题翻译：制备醚化羟甲基氨基三嗪的方法
公开(公告)号：US4271286A
公开(公告)日：1981-06-02
申请号：US136416
申请日：1980-04-02
申请人： Walter Michel , Hans Honel , Manfred Schon , Wolfgang Kaiser
发明人： Walter Michel , Hans Honel , Manfred Schon , Wolfgang Kaiser
IPC分类号： C07D251/64 , C08G12/00 , C08G12/26 , C08G12/40 , C08G12/42 , C08G12/30
CPC分类号： C08G12/425 , C07D251/64
摘要： An improved process for the preparation of methylolaminotriazines etherified with alkanols and having per mol of the aminotriazine, an analytically determined average of 0.6 n to 2 n preferably 0.7 to 2 n methylol groups, which are etherified to the extent of 30 to 60%, n being the number of amino groups in the aminotriazine, wherein an aminotriazine is warmed to 80.degree. to 130.degree. C. with 0.7 n to 3 n mols of formaldehyde, 2 n to 10 n mols alkanol or a mixture of alkanols having 1 to 8 carbon atoms, the carbon chain of which, if having more than 2 carbon atoms, can also be interrupted by an oxygen atom, and 0 to 5 n mols of water, per mol of the aminotriazine, for 0.2 to 20 minutes, under elevated pressure, wherein the improvement comprises said aminotriazine being first heated to a temperature of 60.degree.-90.degree. C. in the presence of the formaldehyde and 0 to 30% by weight of the total amount of alkanol or alkanol mixture for 1 to 30 minutes at a pH 8 to 11 whereupon the remainder of the alkanol or alkanol mixture is added and the mixture is subsequently heated to 80.degree. to 130.degree. C. under elevated pressure in the presence of a strong inorganic or organic acid, at a pH of 3 to 8, for 0.2 to 20 minutes.
摘要翻译：制备用烷醇醚化并具有每摩尔氨基三嗪的羟甲基氨基三嗪的改进方法，分析测定的平均值为0.6n至2n，优选0.7至2个羟甲基，其醚化程度为30至60％，n 是氨基三嗪中的氨基数，其中氨基三嗪用0.7至3 n摩尔甲醛，2至10摩尔醇或1至8个碳原子的醇的混合物加热至80至130℃ 原子，如果碳原子数多于2个碳原子，碳原子数也可以被氧原子间隔，并且在高压下，每摩尔氨基三嗪为0至5微摩尔的水，为0.2至20分钟，其中所述改进包括在甲醛存在下将所述氨基三嗪首先加热至60〜90℃，在pH为0〜30％的条件下，将烷基醇或链烷醇混合物的总量为0〜30重量％加热1〜30分钟 8到11，其余的t 加入烷醇或链烷醇混合物，随后在强度无机或有机酸存在下，在3至8的pH下，在高压下将混合物加热至80至130℃，时间为0.2至20分钟。

5. 发明授权

US4223141A Preparation of methoxy-methyl melamines 失效
标题翻译：甲氧基甲基三聚氰胺的制备
公开(公告)号：US4223141A
公开(公告)日：1980-09-16
申请号：US51851
申请日：1979-06-25
申请人： Hans Honel , Karlfried Keller , Walter Michel , Manfred Schon
发明人： Hans Honel , Karlfried Keller , Walter Michel , Manfred Schon
IPC分类号： C07D251/64 , C08G12/42
CPC分类号： C07D251/64 , C08G12/427
摘要： This invention relates to a process for the manufacture of methanol-etherified methylolmelamines which are largely monomeric containing more than 5 mols of formaldehyde and more than 4 mols of methyl-etherified methylol groups, per mol of melamine, and having a viscosity of less than 20 pascal-seconds at 25.degree. C. and a solids content of at least 95%, comprising (a) methylolating melamine with formaldehyde at a molar melamine:formaldehyde ratio of 1:6.5 to 1:8 for 11/2 to 5 hours at 50.degree. C. to 85.degree. C., with the formaldehyde source being an aqueous solution of formalin containing 30 to 50% by weight of formaldehyde and having a pH of 6.7 to 7.3, and (b) etherifying the resulting suspension of methylolmelamine with 15 to 30 mols of methanol per mol of melamine at temperatures of 30.degree. C. to 60.degree. C. in the presence of a strong acid.
摘要翻译：本发明涉及甲醇醚化的羟甲基三聚氰胺的制备方法，其主要是单体含有超过5摩尔的甲醛和超过4摩尔的甲基醚化的羟甲基，每摩尔三聚氰胺，并且粘度小于20 在25℃下的帕斯卡 - 秒和至少95％的固体含量，其包含（a）三聚氰胺与甲醛以三聚氰胺：甲醛比为1:6.5至1:8的羟甲基化作用，在50℃下11/2至5小时甲醛源为甲醛水溶液，含有30至50重量％的甲醛，pH值为6.7至7.3，（b）将所得羟甲基三聚氰胺悬浮液用15份醚化至在强酸存在下，在30℃至60℃的温度下，每摩尔三聚氰胺30摩尔甲醇。

6. 发明授权

US4143016A Preparation of melamine derivatives 失效
标题翻译：梅林衍生物的制备
公开(公告)号：US4143016A
公开(公告)日：1979-03-06
申请号：US875307
申请日：1978-02-06
申请人： Hans Honel , Karlfried Keller , Walter Michel , Manfred Schon
发明人： Hans Honel , Karlfried Keller , Walter Michel , Manfred Schon
IPC分类号： C07D251/64 , C08L61/28
CPC分类号： C07D251/64
摘要： A process for the preparation of a substantially monomeric methylolmelamine etherified by methanol which contains per mol of melamine, more than 5 mols of formaldehyde and more than 4 mols of methyl-etherified methylol groups which has a viscosity of less than 10 Pa.s at 25.degree. C. at a solids content of at least 95%, said process comprising reacting melamine and formaldehyde in a molar ratio of from 1 : 6.2 to 1 : 8, at a temperature of from 40 to 60.degree. C., in the presence of a basic catalyst in a reaction mixture which contains from 10 to 40% by weight of water and from 40 to 20% by weight of methanol thereby producing a suspension of methylolmelamine, and then etherifying the methylol melamine in the presence of from 15 to 30 mols of methanol per mol of melamine, at a temperature of from 25 to 50.degree. C., in the presence of a strong acid.

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