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1. 发明授权

US06372944B1 Liquid withdrawing tray for purification column, purification column, and method for purification 有权
标题翻译：用于净化柱，净化柱和净化方法的抽出塔
公开(公告)号：US06372944B1
公开(公告)日：2002-04-16
申请号：US09667283
申请日：2000-09-22
申请人： Hajime Matsumoto , Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
发明人： Hajime Matsumoto , Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
IPC分类号： C07C5142
CPC分类号： C07C51/44 , B01D3/20 , B01D3/4205 , C07C67/54 , Y10S203/11 , C07C57/04 , C07C69/54
摘要： In the purification of an easily polymerizable compound such as (meth)acrylic acid by the use of a purification column adapted to withdraw a liquid from the middle portion of the column, a novel liquid withdrawing tray adapted to prevent the compound from polymerization effectively and permit the purification to be stably performed for a long time, a purification column using this tray, and a method for purifications using this purification column are provided. The liquid withdrawing tray for the purification column is composed of a liquid receiving plate and a liquid withdrawing tube for withdrawing the liquid from the liquid receiving plate.
摘要翻译：在通过使用用于从塔的中间部分抽出液体的净化塔来纯化易于聚合的化合物如（甲基）丙烯酸的方法中，适用于有效地防止化合物聚合的新型液体回收塔，并允许提供长时间稳定地进行的纯化，使用该托盘的纯化塔和使用该纯化塔的纯化方法。用于净化塔的液体排出托盘由液体接收板和用于从液体接收板中取出液体的液体抽出管构成。

2. 发明授权

US06566551B2 Method for preventing effluent gas pipe from blocking 有权
标题翻译：防止排气管阻塞的方法
公开(公告)号：US06566551B2
公开(公告)日：2003-05-20
申请号：US09724468
申请日：2000-11-29
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada , Harunori Hirao , Mamoru Takamura
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Misao Inada , Harunori Hirao , Mamoru Takamura
IPC分类号： C07C5116
CPC分类号： C07C51/252 , C07C57/04
摘要： For use in a process for the production of (meth)acrylic acid comprising at least a step for the reaction of (meth)acrylic acid by catalytic gas phase oxidation and a step for the absorption thereof, a method for preventing an effluent gas pipe from blocking is disclosed, which method is characterized by causing part or the whole of the gas discharged from the step for absorption, while being circulated via the effluent gas pipe to the step for the reaction or being discarded, to be subjected to temperature elevation and application of pressure and/or mist separation. Particularly by setting the temperature of the waste gas from the absorption column at a level in the range of 30-70° C., it is made possible to decrease the contents of water, low boiling substances, and subliming substances entrained by the waste gas and, coupled with the temperature elevation and the application of pressure implemented in the effluent gas pipe, attain effective prevention of the interior of the effluent gas pipe from blockage and corrosion.
摘要翻译：为了用于生产（甲基）丙烯酸的方法，至少包括通过催化气相氧化反应（甲基）丙烯酸的步骤和用于吸收的步骤，用于防止流出气体管道的方法公开了这种方法，其特征在于，使得从步骤吸收的气体的一部分或全部通过废气管循环到用于反应或被丢弃的步骤中，以进行升温和施加的压力和/或雾分离。特别是通过将来自吸收塔的废气的温度设定在30〜70℃的范围内，能够降低水，低沸点物质和由废气夹带的升华物质的含量再加上在排气管道中实施的温度升高和施加压力，有效防止排气管内部堵塞和腐蚀。

3. 发明授权

US06613196B2 Method for stopping purifying column 有权
公开(公告)号：US06613196B2
公开(公告)日：2003-09-02
申请号：US09901267
申请日：2001-07-09
申请人： Kei Hamamoto , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
发明人： Kei Hamamoto , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
IPC分类号： B01D342
CPC分类号： B01D3/343 , B01D3/14 , C07C51/44 , Y10S203/07 , Y10S203/22 , C07C57/04
摘要： A method for stopping a purifying column handling an easily polymerizing compound-containing solution is disclosed, which method is characterized by lowering the inner oxygen concentration of the column below the limit of oxygen concentration by supplying an inert gas to the column while the concentration of the gas of easily polymerizing compound is in the range of 100% to the lower limit of the flammable range in volume % of the purifying column or by further supplying a reflux liquid thereby cooling the interior of the column at a rate in the range of 0.01-10° C./min. This invention enjoys exceptionally high economic value in respect that it is capable of preventing the easily polymerizing compound from the occurrence of polymerization in the purifying column, precluding the interior of the purifying column from being clogged by adhesion of a polymer, and moreover avoiding the possibility of explosion.

4. 发明授权

US06676808B2 Method for starting up distilling column 有权
标题翻译：启动蒸馏塔的方法
公开(公告)号：US06676808B2
公开(公告)日：2004-01-13
申请号：US09871213
申请日：2001-05-31
申请人： Kei Hamamoto , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
发明人： Kei Hamamoto , Yukihiro Matsumoto , Sei Nakahara , Misao Inada
IPC分类号： B01D334
CPC分类号： C07C51/46 , B01D3/322 , B01D3/4227 , C07C51/50 , Y10S203/07 , Y10S203/22 , C07C57/04
摘要： A method for starting up a distilling column destined to handle an easily polymerizing compound-containing solution characterized by supplying at the start of the operation of the distilling column a polymerization inhibitor to the bottom liquid of the distilling column having a temperature of not higher than 80° C. Further, by supplying a reflux liquid through the top of the distilling column or the middle stage of the column prior to the start of the temperature elevation of the distilling column, thereby preventing the polymerization of the easily polymerizing compound more effectively.
摘要翻译：一种用于启动用于处理容易聚合的含化合物的溶液的蒸馏塔的方法，其特征在于，在蒸馏塔开始操作时将聚合抑制剂供入具有不高于80℃的蒸馏塔的底部液体 ℃。此外，在蒸馏塔开始升温之前，通过在蒸馏塔的顶部或塔的中间阶段供应回流液体，从而更有效地防止了容易聚合的化合物的聚合。

5. 发明申请

US20070003460A1 Reactor filled with solid particle and gas-phase catalytic oxidation with the reactor 有权
标题翻译：反应器用反应器填充固体颗粒和气相催化氧化
公开(公告)号：US20070003460A1
公开(公告)日：2007-01-04
申请号：US11498426
申请日：2006-08-03
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
IPC分类号： B01J8/04 , B01J8/08 , B01J10/00
CPC分类号： B01J8/067 , B01J8/001 , B01J2208/00044 , B01J2208/00061 , B01J2208/00212 , B01J2208/00513 , B01J2208/00539 , B01J2208/021 , B01J2208/025 , B01J2219/00777
摘要： A shell-and tube reactor including at least one reaction tube with a measuring means, substantially same solid particles being filled in the reaction tubes with or without the measuring means, a length of the filled solid particle layer, and a pressure drop thereof while passing a gas through the reaction tube, per each reaction tube, being substantially the same, respectively. By measuring the temperature of the catalyst particle layer, such a temperature as a representative can be gasped.
摘要翻译：包括具有测量装置的至少一个反应管的管壳式反应器，在具有或不具有测量装置的反应管中填充基本相同的固体颗粒，填充的固体颗粒层的长度及其通过时的压降通过反应管的每个反应管的气体分别基本相同。通过测量催化剂颗粒层的温度，可以将诸如代表性的温度气化。

6. 发明授权

US06651731B2 Method for cooling heating grade heat exchanger in unsteady state 有权
公开(公告)号：US06651731B2
公开(公告)日：2003-11-25
申请号：US10062239
申请日：2002-02-01
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Motomi Nakamura
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Motomi Nakamura
IPC分类号： F25B2900
CPC分类号： F28D7/0066 , B01D3/322 , B01J19/0013 , B01J19/18 , B01J2219/00063 , B01J2219/00069 , B01J2219/00094 , B01J2219/00164 , B01J2219/002 , B01J2219/00213 , B01J2219/00238
摘要： For a heat exchanger using a heating medium for the purpose of heating a fluid to be handled during a steady state, this invention provides a method for using relevant devices which enables the heat exchanger to be operated safely and infallibly without suffering the raw material or the reaction product to polymerize in the reactor or the pipes during an unsteady state, suffering the reactor or the pipes to sustain a fracture owing to a rise in the internal pressure of the vessel, and suffering the apparatus for production to sustain serious damage. This invention pertains, mainly in a heat exchanger admitting a heating medium and using it for the purpose of heating a fluid to be handled, to a method for using relevant devices during the unsteady state, characterized by introducing a cooling medium in the place of the heating medium mentioned above.

7. 发明授权

US07534339B2 Reactor filled with solid particle and gas-phase catalytic oxidation with the reactor 有权
标题翻译：反应器用反应器填充固体颗粒和气相催化氧化
公开(公告)号：US07534339B2
公开(公告)日：2009-05-19
申请号：US11498426
申请日：2006-08-03
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
IPC分类号： C10G51/06 , C07C27/10 , B01J8/00 , F28D7/00
CPC分类号： B01J8/067 , B01J8/001 , B01J2208/00044 , B01J2208/00061 , B01J2208/00212 , B01J2208/00513 , B01J2208/00539 , B01J2208/021 , B01J2208/025 , B01J2219/00777
摘要： A shell-and tube reactor including at least one reaction tube with a measuring means, substantially same solid particles being filled in the reaction tubes with or without the measuring means, a length of the filled solid particle layer, and a pressure drop thereof while passing a gas through the reaction tube, per each reaction tube, being substantially the same, respectively. By measuring the temperature of the catalyst particle layer, such a temperature as a representative can be gasped.
摘要翻译：包括具有测量装置的至少一个反应管的管壳式反应器，在具有或不具有测量装置的反应管中填充基本相同的固体颗粒，填充的固体颗粒层的长度及其通过时的压降通过反应管的每个反应管的气体分别基本相同。通过测量催化剂颗粒层的温度，可以将诸如代表性的温度气化。

8. 发明授权

US06891061B1 Packed column and polymerizable compound treating method using the same 有权
标题翻译：填充柱和使用其的可聚合化合物处理方法
公开(公告)号：US06891061B1
公开(公告)日：2005-05-10
申请号：US09688169
申请日：2000-10-16
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
IPC分类号： B01D3/16 , B01D3/14 , B01D3/32 , B01J10/00 , B01J19/30 , B01J19/32 , C07C51/44 , C07C57/07 , C07C67/54 , C07C69/54 , C07C67/48 , C07C51/42
CPC分类号： B01J19/305 , B01D3/324 , B01D3/326 , B01J19/325 , B01J2219/185 , B01J2219/3221 , B01J2219/32213 , B01J2219/32272 , B01J2219/32275 , B01J2219/3325
摘要： Provided are a packed column arranged so as to be capable of effectively preventing polymerization of a polymerizable compound such as a (meth)acrylic acid in treating the compound, and a method for treating a polymerizable compound using the packed column. The packed column, which is provided with a packing support plate and is filled with a packing on the packing support plate, is arranged so as to include a packing layer (B) having a greater percentage of voids than that of a packing layer (A), between the packing support plate and the packing layer (A).
摘要翻译：提供了一种填充柱，其布置成能够有效地防止在处理该化合物时诸如（甲基）丙烯酸之类的可聚合化合物的聚合，以及使用填充柱处理可聚合化合物的方法。填充柱设置有填充支撑板并且填充在填料支撑板上的填料，以包括具有比填充层（A（A））更大百分比的空隙的填充层（B）），在包装支撑板和包装层（A）之间。

9. 发明授权

US06848501B2 Method for preventing plate type heat exchanger from blockage 失效
标题翻译：防止板式换热器堵塞的方法
公开(公告)号：US06848501B2
公开(公告)日：2005-02-01
申请号：US10356428
申请日：2003-01-31
申请人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
发明人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
IPC分类号： B01J19/00 , F28D7/16 , F28D9/00 , F28F19/00 , F28F27/02
CPC分类号： F28D9/0068 , B01J19/002 , B01J2219/00252 , F28D7/1607 , F28D7/1623 , F28D9/0062 , F28F9/0278 , F28F19/00 , F28F2250/102
摘要： In an apparatus provided with a plate type heat exchanger as a heater and/or a cooler and operated to treat a gas containing an easily blocking substance, a method for preventing the plate type heat exchanger from being blocked is disclosed which is characterized by i) setting the width of a flow path on a plate of the plate type heat exchanger in the apparatus in a range of 6-25 mm and ii) setting the average flow rate of the gas passing the plate type heat exchanger in the apparatus per unit cross-sectional area of the flow path on the plate in the range of 3-15 m/s. In the exchange of heat of an easily blocking substance by the use of a plate type heat exchanger, a method for preventing the plate type heat exchanger from blockage is disclosed which has the plate type heat exchanger provided in the port for introducing a gas containing an easily blocking substance with a gas dispersion plate. This invention, in the heat exchange of an effluent gas emanating from a process for the production of (meth)acrylic acid or an ester thereof or the disposal of the gas, significantly allays blockage of the interior of the plate type heat exchanger.
摘要翻译：在设置有作为加热器和/或冷却器的板式热交换器并且被操作以处理含有易阻塞物质的气体的装置中，公开了一种防止板式热交换器被堵塞的方法，其特征在于i）将设备中板式热交换器的板上的流路宽度设置在6-25mm的范围内，以及ii）将通过板式热交换器的气体的平均流量设置在每单位十字的装置中板上流路的截面面积在3-15 m / s的范围内。在通过使用板式热交换器交换容易堵塞物质的热的情况下，公开了一种防止板式热交换器堵塞的方法，其具有设置在用于引入含有用气体分散板容易地堵塞物质。本发明在从（甲基）丙烯酸或其酯的制备方法产生的流出气体的热交换或气体的处理中显着地阻止了板式热交换器的内部堵塞。

10. 发明授权

US06588450B2 Storage tank for viscous oil containing easily polymerizable compounds 有权
标题翻译：含有容易聚合的化合物的粘性油储罐
公开(公告)号：US06588450B2
公开(公告)日：2003-07-08
申请号：US09788598
申请日：2001-02-21
申请人： Yuichi Ijiri , Yukihiro Matsumoto , Sei Nakahara , Fumio Munechika
发明人： Yuichi Ijiri , Yukihiro Matsumoto , Sei Nakahara , Fumio Munechika
IPC分类号： F17D114
CPC分类号： B65D88/10 , Y10T137/8342 , Y10T137/85954
摘要： This invention relates to a storage tank for a viscous oil containing easily polymerizable compounds. The storage tank of the present invention for storing viscous oil containing easily polymerizable compounds comprises a bottom plate, a side wall, a draw-off pipe and an inlet pipe. The bottom plate slopes downwardly toward the draw-off pipe, and an angle of downward inclination of the bottom plate is a gradient of at least 1/200. It becomes possible because of the storage tank to effectively prevent polymerization of easily polymerizable compounds contained in waste oil within the storage tank, and clogging of a pipe is suppressed considerably.
摘要翻译：本发明涉及一种含有容易聚合的化合物的粘稠油储罐。用于储存容易聚合的化合物的粘性油的本发明的储罐包括底板，侧壁，抽出管和入口管。底板朝向排出管向下倾斜，底板的向下倾斜角度为至少1/200的坡度。由于储罐能够有效地防止储罐内的废油中容易聚合的化合物的聚合，因此可以大幅度地抑制管堵塞。

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