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1. 发明申请

WO9730144A3 TRANSITION-METAL COMPLEXES USED AS ACTIVATORS FOR PEROXY COMPOUNDS 审中-公开
标题翻译：过渡金属复合物用作过氧化合物的活化剂
公开(公告)号：WO9730144A3
公开(公告)日：1997-12-31
申请号：PCT/EP9700550
申请日：1997-02-07
申请人： HENKEL KGAA , BLUM HELMUT , MAYER BERND , PEGELOW ULRICH , SPECKMANN HORST DIETER , KREBS BERNT , DUDA MARK , NAZIKKOL CETIN , REIM JOERG
发明人： BLUM HELMUT , MAYER BERND , PEGELOW ULRICH , SPECKMANN HORST-DIETER , KREBS BERNT , DUDA MARK , NAZIKKOL CETIN , REIM JOERG
IPC分类号： B01J31/18 , C07D233/64 , C07F13/00 , C07F15/02 , C11D3/16 , C11D3/39
CPC分类号： C11D3/3932 , B01J31/1815 , B01J2531/16 , B01J2531/46 , B01J2531/56 , B01J2531/64 , B01J2531/72 , B01J2531/821 , B01J2531/842 , B01J2531/845 , C07F13/005 , C07F15/025
摘要： Described are complexes of the transition metals manganese, iron, cobalt, ruthenium, molybdenum, titanium, vanadium and/or copper containing one or more ligands of general formula (I) ou (II) in which R is a direct bond or an optionally amin-group-substituted alkylene group with 1 to 4 C-atoms, A is a condensed or non-condensed ring system containing at least one nitrogen atom, B is hydrogen, an OH-group or the same as A, and X is a phenyl ring optionally substituted with hydroxy and/or C1-4 alkyl or an optionally hydroxy-substituted C1-4 alkylene group. The complexes are suitable for use as activators or peroxy compounds in oxidative washing, cleaning and disinfectant solutions, washing and cleaning agents preferably containing 0.0025 to 0.25 % by wt. of such activator complexes.
摘要翻译： PCT No.PCT / EP97 / 00550 Sec。 371日期：1998年9月16日 102（e）1998年9月16日PCT PCT 1997年2月7日提交PCT公布。公开号WO97 / 30144 PCT 日期1997年8月21日描述了含有一种或多种通式（I）ou（II）的配体的过渡金属锰，铁，钴，钌，钼，钛，钒和/或铜的络合物，其中R是直接键或任选具有1至4个C原子的氨基取代的亚烷基，A是含有至少一个氮原子的缩合或非稠合环系，B是氢，OH基或与A相同，并且X是任选地被和/或C 1-4烷基或任选羟基取代的C 1-4亚烷基取代的苯环。该配合物适合用作氧化洗涤，清洁和消毒溶液中的活化剂或过氧化合物，优选含有0.0025至0.25重量％的洗涤和清洁剂。的这种活化剂复合物。

2. 发明申请

WO0174742A3 METHOD FOR OXIDIZING HYDROCARBONS 审中-公开
标题翻译： PROCESS氧化烃类
公开(公告)号：WO0174742A3
公开(公告)日：2002-02-14
申请号：PCT/EP0103289
申请日：2001-03-22
申请人： CREAVIS TECH & INNOVATION GMBH , KUEHNLE ADOLF , DUDA MARK , SHELDON ROGER ARTHUR , SASIDHARAN MANICKAM , ARENDS ISABELLA W C E , SCHIFFER THOMAS , FRIES GUIDO , KIRCHHOFF JOCHEN
发明人： KUEHNLE ADOLF , DUDA MARK , SHELDON ROGER ARTHUR , SASIDHARAN MANICKAM , ARENDS ISABELLA W C E , SCHIFFER THOMAS , FRIES GUIDO , KIRCHHOFF JOCHEN
IPC分类号： C07B41/00 , C07B61/00 , C07C27/12 , C07C29/50 , C07C35/02 , C07C35/20 , C07C37/08 , C07C45/28 , C07C45/36 , C07C47/54 , C07C49/385 , C07C49/78 , C07C409/08 , C07C409/10 , C07C409/14
CPC分类号： C07B41/00 , C07C29/50 , C07C45/36 , C07C407/00 , C07C409/08 , C07C409/10 , C07C409/14 , C07C2601/14 , C07C2601/18 , C07C2601/20 , C07C2602/10 , C07C2602/28 , C07C33/20 , C07C35/02 , C07C35/20 , C07C35/205 , C07C409/04 , C07C409/40
摘要： The invention relates to a method for oxidizing substrates such as hydrocarbons, waxes or soot. The method involves the use of a compound of formula (I) in which: R and R represent H, an aliphatic or aromatic alkoxy radical, carboxyl radical, alkoxycarbonyl radical or hydrocarbon radical, each having 1 to 20 hydrocarbon atoms, SO3H, NH2, OH, F, Cl, Br, I and/or NO2, whereby R and R designate identical or different radicals or R and R can be linked to one another via a covalent bonding; Q1 and Q2 represent C, CH, N, CR , each being the same or different; X and Z represent C, S, CH2, each being the same or different; Y represents O and OH; k = 0, 1, 2; l = 0, 1, 2; m = 1 to 3, and; R represents one of the meanings of R . Said compound is used as a catalyst in the presence of a radical initiator, whereby the molar ratio of the catalyst to the hydrocarbon is less than 10 mol %. Peroxy compounds or azo compounds can be used as the radical initiator. Preferred substrates are aliphatic or aromatic hydrocarbons.
摘要翻译：本发明涉及一种用于基片的氧化方法，例如烃类，蜡类或炭黑，其中，作为催化剂的式（I）中R <1>，R <2> = H，脂族或芳族烷氧基基团，羧基基团，烷氧基羰基或烃基的化合物，各自具有1至20个碳原子，SO 3 H，NH 2，OH，氟，氯，Br，I和/或NO 2，其中R <1>和R <2>中，相同的或不同的基团表示或R <1>和R <2> 可以通过共价键Q1被链接在一起，Q2 = C，CH，N，CR <5>各自相同或不同，X，Z = C，S，CH 2，相同或不同，Y = O，OH， K = 0，1，2，L = 0，1，2，M = 1至3，R <5>，R <1>的含义之一，采用在自由基引发剂的存在下，其中所述催化剂的摩尔比至烃小于10摩尔％。自由基引发剂过氧或者可以使用偶氮化合物。优选的基材是脂族或芳族烃。

3. 发明申请

WO03078310A8 METHOD FOR THE PRODUCTION OF A CATALYST CONTAINING VANADIUM, PHOSPHORUS, AND OXYGEN 审中-公开
标题翻译：用于生产钒，磷和氧的含催化剂
公开(公告)号：WO03078310A8
公开(公告)日：2004-11-11
申请号：PCT/EP0302502
申请日：2003-03-12
申请人： BASF AG , WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
发明人： WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/08 , B01J37/14 , B01J37/18 , C07C51/215 , C07C51/25 , C07C57/145
CPC分类号： B01J8/10 , B01J8/067 , B01J19/22 , B01J27/198 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/08 , B01J37/14 , B01J37/18 , B01J2208/00849 , B01J2208/00876 , B01J2219/182 , C07C51/215 , C07C51/252 , C07C57/145
摘要： Disclosed is a method for producing a catalyst containing vanadium, phosphorus, and oxygen, which is used for oxidizing the gas phase of a hydrocarbon having at least four carbon atoms to maleic anhydride. According to the inventive method, a corresponding catalyst precursor which contains vanadium, phosphorus, and oxygen and is provided with particles having an average diameter of at least 2 mm is converted into a catalytically active form by means of calcination, and a flow of the catalyst precursor is transported on a conveyor belt across at least one calcination area over a distance ln at an essentially steady speed in order to be calcinated. The variation over time of the gas temperature in relation to the set point value amounts to
摘要翻译：一种用于生产一种适用于具有至少四个碳原子的烃的非均相催化气相氧化马来酸酐，含有钒，磷和氧的催化剂，其中含有相应的钒，磷，和具有氧的催化剂前体的方法，其中具有至少2mm的平均直径的颗粒，换算通过煅烧成催化活性形式，其中通过至少一个煅烧区，长度LN N，进行在传送带上以基本上恒定的速度进行煅烧的催化剂前体的电流，其中在该范围内的任何点与设定值的气体温度的时间变化催化剂前体的煅烧区的LN / 2在每种情况下的长度的一半后的流<= 5℃，并在气体温度的任何点之间在催化剂前体的流的区域中的局部差异 s为煅烧LN / 2的每个<= 5°C后一半的长度。

4. 发明申请

WO2004014833A2 METHOD FOR PRODUCING MALEIC ANHYDRIDE 审中-公开
标题翻译：制备马来酸酐的方法
公开(公告)号：WO2004014833A2
公开(公告)日：2004-02-19
申请号：PCT/EP0307982
申请日：2003-07-22
申请人： BASF AG , WEIGUNY JENS , RUPPEL WILHELM , DUDA MARK
发明人： WEIGUNY JENS , RUPPEL WILHELM , DUDA MARK
IPC分类号： C07B61/00 , C07D307/60 , C07C51/00
CPC分类号： C07D307/60
摘要： The invention relates to a method for producing maleic anhydride by the heterogeneous catalytic gas phase oxidation of hydrocarbons comprising at least four carbon atoms with gases containing oxygen, in the presence of a volatile phosphorus compound, on a catalyst containing vanadium, phosphor and oxygen in a multitube flow reactor unit with at least one reaction zone that is cooled by a heat-transfer medium, at a temperature ranging between 350 and 500 °C. In the first reaction zone, in relation to the educt supply, the supply temperature and/or the supply quantity is set in such a way that the average temperature of the heat transfer medium in the first reaction zone TSB(1st zone), said temperature being produced by the average value formation of the supply temperature and the drainage temperature of the heat-transfer medium, fulfils the formulas (I) and (II): (I) TSB(1st zone)
摘要翻译：一种用于通过具有在挥发性含磷化合物的催化剂在具有钒，磷和氧在管束反应器单元的至少一个的温度在所述范围由载热介质的反应区中冷却的存在下与含氧气体的至少四个碳原子的烃的非均相催化气相氧化制备马来酸酐的方法从350至500℃，其中，在其中进料的温度和/或载热介质的供给量相对于被调节到反应物供应，在第一反应区，使得在第一反应区TSB载热介质的平均温度（第一区），其通过平均入口温度和载热介质的流动温度，式（I）和（II）得到的：TSB（第一区）<= TD（1个区） - TSafety（1个区）（I）... ; TSB，λ最大（1个区） - TA <= TSB（第一区）<= TSB，λ最大+ TB（II）被满足，其中TD（1（1区）（1个区）（1个区）。。。。用于第一反应区的通过温度; TSafety（第一区）代表第一反应区的安全温度，为1°C; （1个区）TSB，λ最大是在第一反应区中的载热介质，其中，在TSB（第一区）的范围内的平均温度<= TD最大产率在马来酸酐实现。（1个区）; TA（第一区）为20°C; 和TB（第一区）是10℃

5. 发明申请

WO03078310A2 METHOD FOR THE PRODUCTION OF A CATALYST CONTAINING VANADIUM, PHOSPHORUS, AND OXYGEN 审中-公开
标题翻译：用于生产钒，磷和氧的含催化剂
公开(公告)号：WO03078310A2
公开(公告)日：2003-09-25
申请号：PCT/EP0302502
申请日：2003-03-12
申请人： BASF AG , WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
发明人： WEIGUNY JENS , STORCK SEBASTIAN , DUDA MARK , DOBNER CORNELIA , FELDER RAIMUND
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/08 , B01J37/14 , B01J37/18 , C07C51/215 , C07C51/25 , C01B3/38
CPC分类号： B01J8/10 , B01J8/067 , B01J19/22 , B01J27/198 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/08 , B01J37/14 , B01J37/18 , B01J2208/00849 , B01J2208/00876 , B01J2219/182 , C07C51/215 , C07C51/252 , C07C57/145
摘要： Disclosed is a method for producing a catalyst containing vanadium, phosphorus, and oxygen, which is used for oxidizing the gas phase of a hydrocarbon having at least four carbon atoms to maleic anhydride. According to the inventive method, a corresponding catalyst precursor which contains vanadium, phosphorus, and oxygen and is provided with particles having an average diameter of at least 2 mm is converted into a catalytically active form by means of calcination, and a flow of the catalyst precursor is transported on a conveyor belt across at least one calcination area over a distance ln at an essentially steady speed in order to be calcinated. The variation over time of the gas temperature in relation to the set point value amounts to
摘要翻译：一种用于生产一种适用于具有至少四个碳原子的烃的非均相催化气相氧化马来酸酐，含有钒，磷和氧的催化剂，其中含有相应的钒，磷，和具有氧的催化剂前体的方法，其中具有至少2mm的平均直径的颗粒，换算通过煅烧成催化活性形式，其中通过至少一个煅烧区，长度LN N，进行在传送带上以基本上恒定的速度进行煅烧的催化剂前体的电流，其中在该范围内的任何点与设定值的气体温度的时间变化催化剂前体的煅烧区的LN / 2在每种情况下的长度的一半后的流<= 5℃，并在气体温度的任何点之间在催化剂前体的流的区域中的局部差异 s为煅烧LN / 2的每个<= 5°C后一半的长度。

6. 发明申请

WO0234387A8 CATALYST AND METHOD FOR PRODUCING MALEIC ANHYDRIDE 审中-公开
标题翻译：催化剂及其生产顺酐
公开(公告)号：WO0234387A8
公开(公告)日：2002-05-23
申请号：PCT/EP0112445
申请日：2001-10-26
申请人： BASF AG , STORCK SEBASTIAN , WEIGUNY JENS , DUDA MARK , COX GERHARD
发明人： STORCK SEBASTIAN , WEIGUNY JENS , DUDA MARK , COX GERHARD
IPC分类号： C07D307/60 , B01J27/198 , B01J35/02 , B01J37/08 , C07B61/00 , C07C51/215 , C07C51/225 , C07C57/145
CPC分类号： B01J37/08 , B01J27/198 , B01J35/026 , C07C51/215 , C07C57/145
摘要： The invention relates to a vanadium-, phosphorus- and oxygen-containing catalyst that is used for producing maleic anhydride by heterogeneous catalytic gas phase oxidation of a hydrocarbon carrying at least four carbon atoms in which the ratio of phosphorus/vanadium is 0.9 to 1.5. Said catalyst comprises particles with an average diameter of at least 2 mm and the composition has a x-ray powder diffraction pattern, obtained by irradiation with CuK alpha radiation ( lambda = 1.54 10 m), that produces in the 2 theta range of 10 DEG to 70 DEG a signal/noise ratio of
摘要翻译： Vnadium，磷和催化剂用于通过具有至少四个碳原子的烃，其中所述磷/钒比为0.9〜1.5的非均相催化气相氧化制备马来酸酐，具有含氧，其具有至少2mm的平均直径的颗粒且其中使用CuKα辐射的组合物（拉姆达= 1.54。10- <10>米）的粉末XRöntgenbeugungsdiagram结果的θ2在10°〜70°时，信号/背景比将含有钒和磷相位所有衍射线可以归因，包括

7. 发明专利

DE19605688A1 未知
公开(公告)号：DE19605688A1
公开(公告)日：1997-08-21
申请号：DE19605688
申请日：1996-02-16
申请人： HENKEL KGAA
发明人： BLUM HELMUT , MAYER BERND , PEGELOW ULRICH , SPECKMANN HORST-DIETER , KREBS BERNT , DUDA MARK , NAZIKKOL CETIN , REIM JOERG
IPC分类号： B01J31/18 , C07D233/64 , C07F13/00 , C07F15/02 , C11D3/16 , C11D3/39 , C07B33/00 , C07F19/00 , C07F9/6503 , C11D1/83 , C11D3/395 , D06L3/02 , B01J31/22 , C07D213/36 , C07D401/14 , C07D235/20
摘要： Described are complexes of the transition metals manganese, iron, cobalt, ruthenium, molybdenum, titanium, vanadium and/or copper containing one or more ligands of general formula (I) ou (II) in which R is a direct bond or an optionally amin-group-substituted alkylene group with 1 to 4 C-atoms, A is a condensed or non-condensed ring system containing at least one nitrogen atom, B is hydrogen, an OH-group or the same as A, and X is a phenyl ring optionally substituted with hydroxy and/or C1-4 alkyl or an optionally hydroxy-substituted C1-4 alkylene group. The complexes are suitable for use as activators or peroxy compounds in oxidative washing, cleaning and disinfectant solutions, washing and cleaning agents preferably containing 0.0025 to 0.25 % by wt. of such activator complexes.

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