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    • 4. 发明授权
    • Process for producing cobalt-containing ferromagnetic iron oxide powder
    • 含钴铁磁性氧化铁粉末的生产工艺
    • US4267207A
    • 1981-05-12
    • US39028
    • 1979-05-14
    • Koji SasazawaTatsuji KitamotoGoro AkashiKouichi MasakiShinichiro Dezawa
    • Koji SasazawaTatsuji KitamotoGoro AkashiKouichi MasakiShinichiro Dezawa
    • C01G49/00C01G49/02G11B5/706H01F1/11B05D5/12
    • G11B5/70694C01G49/02G11B5/70642C01P2006/42
    • A process for producing a cobalt-containing ferromagnetic iron oxide powder suitable for magnetic recording which comprises(a) mixing cobalt ion, ferrous ion and an alkali with an aqueous dispersion of acicular ferromagnetic iron oxide nuclei under non-oxidizing conditions at a temperature of about 50.degree. C. or less;(b) heating the dispersion to a temperature of at least about 60.degree. C. but below the boiling point of the dispersion under non-oxidizing conditions to cause a reaction; and(c) treating the dispersion at a temperature of at least about 60.degree. C. but below the boiling point of the dispersion under the following conditions:(1) initially treating the dispersion under non-oxidizing conditions for about 5 minutes or more;(2) subsequentially treating the dispersion under oxidizing conditions for about 5 minutes or more prior to the termination of the reaction; and(3) a total treating time under non-oxidizing conditions and oxidizing conditions of at least about 30 minutes.
    • 一种适用于磁记录的含钴铁磁性氧化铁粉末的制造方法,其特征在于,包括:(a)在非氧化条件下,将钴离子,亚铁离子和碱与针状铁磁性氧化铁核的水分散体混合, 50℃以下; (b)在非氧化条件下将分散体加热到至少约60℃但低于分散体的沸点以引起反应; 和(c)在以下条件下,在至少约60℃但低于分散体沸点的温度下处理分散体:(1)最初在非氧化条件下处理分散体约5分钟或更长时间; (2)在反应终止之前,在氧化条件下将分散体顺序处理约5分钟或更长时间; 和(3)在非氧化条件和氧化条件下的总处理时间为至少约30分钟。