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1. 发明授权

US4228126A Diacetylene time-temperature indicators 失效
标题翻译：乙炔时间温度指标
公开(公告)号：US4228126A
公开(公告)日：1980-10-14
申请号：US854933
申请日：1977-11-25
申请人： Gordhanbhai N. Patel , Kwok C. Yee
发明人： Gordhanbhai N. Patel , Kwok C. Yee
IPC分类号： G01K3/04 , G01T1/04 , G01N21/06
CPC分类号： G01K3/04 , G01T1/04
摘要： An improved recording device is described, useful for measuring the integrated time-temperature or integrated radiation-dosage history of an article, comprising a substrate onto which an acetylenic compound, containing at least two conjugated C.tbd.C groups, in an inactive form, is deposited. The inactive form is capable of being converted by melt or solvent recrystallization to an active form, which undergoes 1,4-addition polymerization resulting in an irreversible, progressive color change. The color change produced at any given point in time represents an integrated time-temperature history of thermal annealing or integrated radiation-dosage history of exposure to actinic radiation to which an article has been exposed.Also described is a process for producing an inactive form of the acetylenic compound. A film and a fiber, made from the inactive form of an acetylenic compound are also described.
摘要翻译：描述了一种改进的记录装置，用于测量制品的综合时间温度或综合放射剂量历史，其包含基底，其中含有至少两个共轭的C 3 O C基团的炔属化合物为非活性形式，其为存放无活性形式能够通过熔体或溶剂重结晶转化为活性形式，其进行1,4-加成聚合，导致不可逆的逐渐变色。在任何给定时间点产生的颜色变化表示热退火或暴露于物品曝光的光化辐射的综合辐射剂量历史的综合时间 - 温度历史。还描述了制备炔属化合物的无活性形式的方法。还描述了由惰性形式的炔属化合物制成的膜和纤维。

2. 发明授权

US4339951A Tempeature measurement and display of indicia using thermochromic polyacetylenes 失效
标题翻译：温度测量和使用热变色聚乙炔的标记显示
公开(公告)号：US4339951A
公开(公告)日：1982-07-20
申请号：US34112
申请日：1979-04-30
申请人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
发明人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
IPC分类号： C08F38/00 , G01K11/16
CPC分类号： G01K11/16 , C08F38/00
摘要： Certain polyacetylenes exhibit reversible color changes at transition temperatures in the range -180.degree. to 220.degree. C., wherein the thermochromic cycles can be repeated many times with no apparent degradation and little change in spectroscopic properties.These thermochromic polyacetylenes are useful in temperature-indicator and indicia-display device applications.A process for laser-beam recording of images is described employing a thermochromic polyacetylene, in which the hysteresis properties of the polyacetylene can be suitably altered allowing for selectively storing or erasing the formed image.
摘要翻译：某些聚乙炔在-180°至220℃范围内的转变温度下表现出可逆的颜色变化，其中热变色循环可以重复多次，没有明显的降解和光谱性质的变化很小。这些热变色聚乙炔可用于温度指示器和标记显示装置。使用热变色聚乙炔描述图像的激光束记录方法，其中可以适当地改变聚乙炔的滞后特性，允许选择性地存储或擦除形成的图像。

3. 发明授权

US4242440A Thermochromic polyacetylenes used in laser beam recording method 失效
标题翻译：用于激光束记录方法的热变色聚乙炔
公开(公告)号：US4242440A
公开(公告)日：1980-12-30
申请号：US34111
申请日：1979-04-30
申请人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
发明人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
IPC分类号： G01D15/10 , G01K11/16 , G03C1/73 , G03C5/04
CPC分类号： G01K11/16 , G01D15/10 , G03C1/73 , G03C1/733 , Y10S430/166
摘要： Certain polyacetylenes exhibit reversible color changes at transition temperatures in the range -180.degree. to 220.degree. C., wherein the thermochromic cycles can be repeated many times with no apparent degradation and little change in spectroscopic properties.These thermochromic polyacetylenes are useful in temperature-indicator and indicia-display device applications.A process for laser-beam recording of images is described employing a thermochromic polyacetylene, in which the hysteresis properties of the polyacetylene can be suitably altered allowing for selectively storing or erasing the formed image.
摘要翻译：某些聚乙炔在-180°至220℃范围内的转变温度下表现出可逆的颜色变化，其中热变色循环可以重复多次，没有明显的降解和光谱性质的变化很小。这些热变色聚乙炔可用于温度指示器和标记显示装置。使用热变色聚乙炔描述图像的激光束记录方法，其中可以适当地改变聚乙炔的滞后特性，允许选择性地存储或擦除形成的图像。

4. 发明授权

US4215208A Thermochromic polyacetylenes containing urethane groups 失效
标题翻译：含有氨基甲酸酯基团的热变性聚乙炔
公开(公告)号：US4215208A
公开(公告)日：1980-07-29
申请号：US839678
申请日：1977-10-05
申请人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
发明人： Kwok C. Yee , Anthony F. Preziosi , Gordhanbhai N. Patel , Ronald R. Chance , Granville G. Miller , Ray H. Baughman
IPC分类号： C08F38/00 , G01K11/16 , C08L49/00
CPC分类号： G01K11/16 , C08F38/00 , Y10S252/962 , Y10S430/146
摘要： Certain polyacetylenes exhibit reversible color changes at transition temperatures in the range -180.degree. to 220.degree. C., wherein the thermochromic cycles can be repeated many times with no apparent degradation and little change in spectroscopic properties.These thermochromic polyacetylenes are useful in temperature-indicator and indicia-display device applications.A process for laser-beam recording of images is described employing a thermochromic polyacetylene, in which the hysteresis properties of the polyacetylene can be suitably altered allowing for selectively storing or erasing the formed image.
摘要翻译：某些聚乙炔在-180°至220℃范围内的转变温度下表现出可逆的颜色变化，其中热变色循环可以重复多次，没有明显的降解和光谱性质的变化很小。这些热变色聚乙炔可用于温度指示器和标记显示装置。使用热变色聚乙炔描述图像的激光束记录方法，其中可以适当地改变聚乙炔的滞后特性，允许选择性地存储或擦除形成的图像。

5. 发明授权

US08278631B2 Time-temperature, UV exposure and temperature indicator 失效
标题翻译：时间，紫外线和温度指示
公开(公告)号：US08278631B2
公开(公告)日：2012-10-02
申请号：US12293322
申请日：2006-10-06
申请人： Gordhanbhai N. Patel
发明人： Gordhanbhai N. Patel
IPC分类号： G01N21/91 , G01N21/00
CPC分类号： G01J1/50 , G01K3/04
摘要： Disclosed is a device for monitoring one or more of integral value of time and temperature, UV light exposure and a pre-determined temperature of an item. The device is useful for monitoring items or materials which are sensitive to time-temperature, UV light and/or a pre-determined temperature. Radiation sensitive devices such as self-indicating instant radiation alert dosimeters (SIRAD) can be accidentally, inadvertently or intentionally over exposed to time-temperature, UV light and a pre-determined higher temperature. Such over exposure can provide a false positive or false negative signal. A device based on polymerization of diacetylenes and melting of partially polymerized diacetylenes, both of which are associated with color changes, are proposed as false positive, false negative, and tamper indicator.
摘要翻译：公开了一种用于监测时间和温度的整体值，UV曝光和物品的预定温度中的一个或多个的装置。该装置可用于监测对时间温度，紫外线和/或预定温度敏感的物品或材料。诸如自我指示即时辐射警报剂量计（SIRAD）的辐射敏感设备可能会意外地，无意地或有意地暴露于时间 - 温度，紫外线和预先确定的较高温度。这种过度曝光可以提供假阳性或假阴性信号。提出了基于二乙炔的聚合和部分聚合的二乙炔的熔融的装置，两者都与颜色变化相关联，被假设为假阳性，假阴性和篡改指示剂。

6. 发明授权

US07476874B2 Self indicating radiation alert dosimeter 失效
标题翻译：自我指示辐射警报剂量计
公开(公告)号：US07476874B2
公开(公告)日：2009-01-13
申请号：US10545796
申请日：2004-02-26
申请人： Gordhanbhai N. Patel
发明人： Gordhanbhai N. Patel
IPC分类号： G03C1/72
CPC分类号： G01T1/06 , G01T1/04
摘要： Described as a self-indicating instant radiation dosimeter (1001) for monitoring high energy radiations, such as X-ray. The dosimeter contains a radiation sensitive, color changing, indicating composition (10), e.g., a diacetylene (R—C≡C—C≡C—R′, where R and R′ are substituents groups) or a radiochromic dye, a polymeric binder (20) and optionally a shelf life extender (50) or an activator (40). The radiation sensitive composition (10) changes color instantly when exposed to high energy radiation. The dose is estimated by comparing the color with a color reference chart or more accurately with a spectrophotometer or an optical densitometer. The radiation sensitive composition (10) is protected from low energy radiation such as UV light, by a layer of low energy absorbing materials, such as UV absorbers.
摘要翻译：描述为用于监测诸如X射线的高能量辐射的自我指示即时辐射剂量计（1001）。剂量计包含辐射敏感的变色指示组合物（10），例如二乙炔（RC≡CC≡C-R'，其中R和R'是取代基基团）或放射性色素染料，聚合物粘合剂（20）和任选的保质期延长剂（50）或活化剂（40）。辐射敏感组合物（10）在暴露于高能量辐射时立即改变颜色。通过使用分光光度计或光密度计将颜色与颜色参考图比较或更准确地估计剂量。辐射敏感组合物（10）通过诸如UV吸收剂的低能量吸收材料层来保护免受诸如UV光的低能量辐射。

7. 发明授权

US4452995A Dialkoxycarbonylmethyleneurethane diynes 失效
标题翻译：二烷氧基羰基亚甲基二胺
公开(公告)号：US4452995A
公开(公告)日：1984-06-05
申请号：US364590
申请日：1982-04-02
申请人： Gordhanbhai N. Patel , Dawn M. Ivory
发明人： Gordhanbhai N. Patel , Dawn M. Ivory
IPC分类号： C08F38/00 , G01K11/16 , C07C125/073
CPC分类号： C08F38/00 , G01K11/16
摘要： Polydiacetylene gel compositions, comprised of a polydiacetylene and a gel-forming liquid therefor, are described which undergo a change in color and in physical state to a solution when heated to a predetermined temperature. The gel compositions exhibit hysteresis temperature characteristics which allow the original color change to be maintained and recorded until the solution is cooled below the predetermined temperature. Thus, the gel compositions are useful in temperature-indicating devices for reversibly monitoring a wide range of temperatures. A novel class of polydiacetylene compounds is also described, useful in forming the gel compositions, formed from monomeric diacetylenediol bis(alkoxycarbonylmethylurethanes).
摘要翻译：描述了由聚二乙炔及其形成凝胶的液体组成的聚二乙炔凝胶组合物，其在加热到预定温度时经历颜色变化和物理状态下的溶液。凝胶组合物显示滞后温度特性，其允许维持和记录原始的颜色变化，直到溶液冷却到预定温度以下。因此，凝胶组合物可用于温度指示装置，用于可逆地监测宽范围的温度。还描述了一类新型的聚二乙炔化合物，可用于形成由单体二乙炔二醇双（烷氧基羰基甲基氨基甲酸酯）形成的凝胶组合物。

8. 发明授权

US4235108A Device for measuring temperature using co-crystallized acetylenic compositions 失效
标题翻译：使用共结晶炔属组合物测量温度的装置
公开(公告)号：US4235108A
公开(公告)日：1980-11-25
申请号：US960507
申请日：1978-11-13
申请人： Gordhanbhai N. Patel
发明人： Gordhanbhai N. Patel
IPC分类号： C09K9/02 , G01K3/04 , G01K11/16 , G01K11/12 , G01K11/20
CPC分类号： G01K11/16 , C09K9/02 , G01K3/04 , Y10S252/962
摘要： A composition is described comprising at least two co-crystallized acetylenic compounds, of different chemical structures, each containing at least one --C.tbd.C--C.tbd.C-- group and substituents selected from the group consisting of sulfonate, urethane and alcohol radicals, at least one of the compounds capable of undergoing a contrasting color change upon exposure to actinic radiation or thermal annealing, wherein the composition exhibits a substantially different thermogram than the sum of thermograms of the individual components as obtained by differential scanning calorimetry.A device is also described useful for measuring the time-temperature or radiation-dosage history of an article comprising a substrate having deposited thereon the described composition.A process is also described for producing the composition of this invention.
摘要翻译：描述了一种组合物，其包含不同化学结构的至少两个共结晶炔属化合物，每个化合物包含至少一个-C 3BOND CC 3BOND C基团和选自磺酸酯，氨基甲酸酯和醇基团的取代基，至少一个的化合物，其在暴露于光化辐射或热退火时能够经历对比色变化，其中所述组合物显示出通过差示扫描量热法获得的各组分的热分析图之和基本上不同的热分析图。还描述了用于测量包含其上沉积有所述组合物的基底的制品的时间温度或辐射剂量历史的装置。还描述了制备本发明组合物的方法。

9. 发明授权

US4189399A Co-crystallized acetylenic compounds 失效
标题翻译：共结晶炔属化合物
公开(公告)号：US4189399A
公开(公告)日：1980-02-19
申请号：US817069
申请日：1977-07-19
申请人： Gordhanbhai N. Patel
发明人： Gordhanbhai N. Patel
IPC分类号： C07C33/04 , C07C309/66 , C07C309/73 , G01K11/16 , G01N33/02 , C09K9/02
CPC分类号： C07C33/04 , C07C309/66 , C07C309/73 , G01K11/16 , G01N33/02
摘要： A composition is described comprising at least two co-crystallized acetylenic compounds, of different chemical structures, each containing at least one --C.tbd.C--C.tbd.C-- group and substituents selected from the group consisting of sulfonate, urethane and alcohol radicals, at least one of the compounds capable of undergoing a contrasting color change upon exposure to actinic radiation or thermal annealing, wherein the composition exhibits a substantially different thermogram than the sum of thermograms of the individual components as obtained by differential scanning calorimetry.A device is also described useful for measuring the time-temperature or radiation-dosage history of an article comprising a substrate having deposited thereon the described composition.A process is also described for producing the composition of this invention.
摘要翻译：描述了一种组合物，其包含不同化学结构的至少两个共结晶炔属化合物，每个化合物包含至少一个-C 3BOND CC 3BOND C基团和选自磺酸酯，氨基甲酸酯和醇基团的取代基，至少一个的化合物，其在暴露于光化辐射或热退火时能够经历对比色变化，其中所述组合物显示出通过差示扫描量热法获得的各组分的热分析图之和基本上不同的热分析图。还描述了用于测量包含其上沉积有所述组合物的基底的制品的时间温度或辐射剂量历史的装置。还描述了制备本发明组合物的方法。

10. 发明授权

US4164458A Production of radiation crosslinked polymeric compositions using diacetylenes 失效
标题翻译：使用二乙炔生产辐射交联聚合物组合物
公开(公告)号：US4164458A
公开(公告)日：1979-08-14
申请号：US775150
申请日：1977-03-07
申请人： Gordhanbhai N. Patel
发明人： Gordhanbhai N. Patel
IPC分类号： C08F255/00 , C08F291/00 , C08K5/205 , H01L21/312 , B01J1/10
CPC分类号： H01L21/312 , C08F255/00 , C08F291/00 , C08K5/205
摘要： Crosslinked polymeric compositions, useful as electrical insulators, heat shrinkable packaging, and lightweight foam plastics, are described. The crosslinked polymeric compositions are produced by admixing a diacetylene monomer, oligomer, polymer or mixture thereof, wherein the monomer has the formula, RNHCO--O--CH.sub.2 --C.tbd.C--C.tbd.C--CH.sub.2 --O--OCNHR' in which R and R' are the same or different and are alkyl containing 1 to 20 carbon atoms, with a thermoplastic crosslinkable polymer and then subjecting the resulting mixture to actinic radiation.
摘要翻译：描述了可用作电绝缘体，热收缩包装和轻质泡沫塑料的交联聚合物组合物。交联的聚合物组合物通过混合二乙炔单体，低聚物，聚合物或其混合物来制备，其中所述单体具有下式：RNHCO-O-CH 2 -C 3 ON CC 3BOND C-CH 2 -O-OCNHR'，其中R和R' 相同或不同，是含有1至20个碳原子的烷基，和热塑性交联聚合物，然后将所得混合物进行光化辐射。

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