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1. 发明授权

US5064875A Process for the preparation of heat-stable polyurethane urea elastomers 失效
标题翻译：制备耐热聚氨酯脲弹性体的方法
公开(公告)号：US5064875A
公开(公告)日：1991-11-12
申请号：US620986
申请日：1990-11-30
申请人： Gerhard Grogler , Urs Thiery , Andreas Ruckes , Richard Kopp , Heinrich Hess
发明人： Gerhard Grogler , Urs Thiery , Andreas Ruckes , Richard Kopp , Heinrich Hess
IPC分类号： C08G18/10 , C08G18/32 , C08G18/65
CPC分类号： C08G18/6529 , C08G18/10 , C08G18/3243 , C08G2101/0008 , C08G2101/0016 , C08G2101/0033 , C08G2120/00
摘要： This invention relates to a process for preparing polyurethane urea elastomers by reacting (a) compounds containing at least two isocyanate-reactive groups and having a molecular weight in the range from about 400 to about 10,000; (b) polyisocyanates; and (c) aromatic diamines corresponding to the formula ##STR1## wherein R.sup.1 and R.sup.2 are independently hydrogen or alkyl.
摘要翻译：本发明涉及通过使（a）含有至少两个异氰酸酯反应性基团并且分子量在约400至约10,000范围内的化合物反应来制备聚氨酯脲弹性体的方法; （b）多异氰酸酯; 和（c）对应于式 + TR 的芳族二胺，其中R 1和R 2独立地是氢或烷基。

2. 发明授权

US5159046A Process for the preparation of highly elastic plastics 失效
标题翻译：制备高弹性塑料的方法
公开(公告)号：US5159046A
公开(公告)日：1992-10-27
申请号：US543649
申请日：1990-06-26
申请人： Gerhard Grogler , Andreas Ruckes , Richard Kopp , Heinrich Hess , Robert Eiben , James M. Barnes
发明人： Gerhard Grogler , Andreas Ruckes , Richard Kopp , Heinrich Hess , Robert Eiben , James M. Barnes
IPC分类号： C07C275/62 , C07C273/18 , C08G18/70 , C08G18/78 , C08G18/80
CPC分类号： C07C273/1809 , C07C273/1872 , C08G18/703 , C08G18/707 , C08G18/7818 , C08G18/8045
摘要： The present invention relates to a process for the preparation of a modified 1,5-naphthylene diisocyanate containing urea and biuret groups comprising reacting(a) 1,5-naphthylene diisocyanate in molten form with(b) a mixture comprising about 0.02 to about 0.5 mole of water per mole of 1,5-naphthylene diisocyanate and about 1 to about 10 parts for each part of water of an organic solvent.The present invention further relates to a process for the preparation of elastomeric moldings comprising reacting by the one-shot or prepolymer process at an isocyanate index of 70 to 130 a modified 1,5-naphthylene diisocyanate containing urea and biuret groups with compounds containing at least two isocyanate-reactive groups and having a molecular weight in the range from about 500 to about 10,000 and, optionally, organic compounds containing isocyanate-reactive groups and having a molecular weight in the range from 60 to 499.
摘要翻译：本发明涉及一种制备含脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯的方法，包括使（a）熔融形式的1,5-亚萘基二异氰酸酯与（b）约0.02至约0.5的混合物摩尔水/摩尔1,5-亚萘基二异氰酸酯和约1至约10份的每份有机溶剂的水。本发明还涉及一种制备弹性体模制品的方法，其包括通过一步或预聚物方法在异氰酸酯指数为70至130的情况下使含有脲和缩二脲基团的改性的1,5-亚萘基二异氰酸酯与至少含有化合物两个异氰酸酯反应性基团，分子量在约500至约10,000的范围内，以及任选的含有异氰酸酯反应性基团并且分子量在60至499范围内的有机化合物。

3. 发明授权

US4851567A N,N'-bis(5-isocyanatonaphthyl)urea, a process for its production, and its use 失效
标题翻译： N，N'-双（5-异氰酸基萘基）脲，其制备方法及其用途
公开(公告)号：US4851567A
公开(公告)日：1989-07-25
申请号：US295636
申请日：1989-01-10
申请人： Andreas Ruckes , Gerhard Grogler , Richard Kopp , Heinrich Hess
发明人： Andreas Ruckes , Gerhard Grogler , Richard Kopp , Heinrich Hess
IPC分类号： C07C273/18 , C07C275/40 , C08G18/10 , C08G18/46 , C08G18/78 , C08G18/80
CPC分类号： C08G18/8045 , C07C275/40 , C08G18/10 , C08G18/4615 , C08G18/4623 , C08G18/7825
摘要： This invention relates to N,N'-bis(5-isocyanatonaphthyl)urea and a process for its preparation by hydrolysis of naphthalene-1,5-diisocyanate. This invention also relates to a method for preparing a polyurethane or polyurea comprising reacting N,N'-bis(5-isocyanatonaphthyl)urea with an NCO-reactive compound.
摘要翻译：本发明涉及N，N'-双（5-异氰酸基萘基）脲及其通过水解萘-1,5-二异氰酸酯制备的方法。本发明还涉及一种制备聚氨酯或聚脲的方法，包括使N，N'-双（5-异氰酸基萘基）脲与NCO-反应性化合物反应。

4. 发明授权

US4882411A Process for the production of cold-setting polyurethane urea elastomers 失效
标题翻译：生产冷凝聚氨酯脲弹性体的方法
公开(公告)号：US4882411A
公开(公告)日：1989-11-21
申请号：US245877
申请日：1988-09-16
申请人： Gerhard Grogler , Andreas Ruckes , Heinrich Hess , Richard Kopp
发明人： Gerhard Grogler , Andreas Ruckes , Heinrich Hess , Richard Kopp
IPC分类号： C08G18/66 , C08G18/10 , C08G18/48 , C08G18/65
CPC分类号： C08G18/4837 , C08G18/10
摘要： The present invention relates to a process for the production of polyurethane urea elastomers from(a) NCO-terminated prepolymers based on polyisocyanates and polyethers having a molecular weight of 400 to about 10,000 and an ethylene oxide content of about 10 to 60 mole-% and(b) solid diaminodiphenyl ureas corresponding to the formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 may be the same or different and represent hydrogen or C.sub.1 -C.sub.6 alkyl radicals and wherein the amino groups are in the m-and/or p-position to the urea group,characterized in that the NCO prepolymers are reacted with the diaminodiphenyl ureas in powder-form in a heterogeneous phase at temperatures of about 5.degree. to 40.degree. C.The present invention is also directed to the polyurethane urea elastomers prepared by this process.
摘要翻译：本发明涉及从（a）基于聚异氰酸酯和聚醚的分子量为400至约10,000并且环氧乙烷含量为约10至60摩尔％的NCO封端的预聚物制备聚氨酯脲弹性体的方法，以及（b）对应于式“IMAGE”的固体二氨基二苯脲，其中R 1，R 2，R 3和R 4可以相同或不同，表示氢或C 1 -C 6烷基，并且其中氨基在m-和/或p 位置，其特征在于NCO预聚物与二氨基二苯基脲在非常相中以粉末形式在约5℃至40℃的温度下反应。本发明还涉及制备的聚氨酯脲弹性体通过这个过程。

5. 发明授权

US4882409A Process for the production of heat-resistant polyurethane urea elastomers 失效
标题翻译：生产耐热聚氨酯脲弹性体的方法
公开(公告)号：US4882409A
公开(公告)日：1989-11-21
申请号：US245880
申请日：1988-09-16
申请人： Gerhard Grogler , Andreas Ruckes , Heinrich Hess
发明人： Gerhard Grogler , Andreas Ruckes , Heinrich Hess
IPC分类号： C08G18/10 , C08G18/32
CPC分类号： C08G18/10 , C08G2101/0008 , C08G2101/0016 , C08G2101/0033
摘要： The present invention is directed to a process for the production of a polyurethane urea elastomer which comprises preparing a heterogeneous mixture of(a) a diaminodiphenylurea corresponding to the formula ##STR1## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4, which may be the same or different, represent hydrogen or a C.sub.1 -C.sub.6 alkyl radical and wherein the amino groups are in the meta and/or para position to the urea group and(b) polyisocyanates and NH.sub.2 -or OH-groups containing compounds or a NCO-terminated prepolymer prepared from a polyisocyanate and a polyhydroxyl compound having a molecular weight of 400 to about 10,000, and subsequently reacting the heterogeneous system to form a polyurethane urea elastomer by heating the mixture to a temperature below the melting point of said diaminodiphenylurea.The present invention is also directed to heterogeneous reaction mixtures based on the above diaminodiphenylureas suspended in the above NCO-terminated prepolymers.
摘要翻译：本发明涉及一种制备聚氨酯脲弹性体的方法，其包括制备（a）对应于式“IMAGE”的二氨基二苯脲的不均匀混合物，其中R 1，R 2，R 3和R 4可以相同或不同，不同的，代表氢或C1-C6烷基，其中氨基位于脲基的间位和/或对位，和（b）含有多异氰酸酯和含NH 2或OH基的化合物或NCO封端的预聚物来自多异氰酸酯和分子量为400至约10,000的多羟基化合物，随后通过将所述混合物加热至低于所述二氨基二苯基脲的熔点的温度，随后使所述非均相体系反应形成聚氨酯脲弹性体。本发明还涉及基于悬浮在上述NCO封端的预聚物中的上述二氨基二苯基脲的不均匀反应混合物。

6. 发明授权

US4902825A N,N'-bis(trans-4-isocyanatocyclohexyl)urea, a process for its preparation and its use 失效
标题翻译： N，N'-双（反式-4-异氰酸根合环己基）脲，其制备方法及其用途
公开(公告)号：US4902825A
公开(公告)日：1990-02-20
申请号：US255915
申请日：1988-10-11
申请人： Andreas Ruckes , Werner Rasshofer , Richard Kopp , Gerhard Grogler
发明人： Andreas Ruckes , Werner Rasshofer , Richard Kopp , Gerhard Grogler
IPC分类号： C07C67/00 , C07C239/00 , C07C275/26 , C08G18/46 , C08G18/50 , C08G18/78 , C08G18/80
CPC分类号： C08G18/8045 , C07C275/26 , C08G18/4615 , C08G18/4623 , C08G18/5048 , C08G18/7825
摘要： The present invention relates to N,N'-bis-(4-isocyanatocyclohexyl)urea obtained from the reaction with water of cyclohexane-1,4-diisocyanate having a high trans isomer content. This invention further relates to the process for preparing the N,N'-bis(4-isocyanatocyclohexyl)urea and to its use in the synthesis of polyurethanes.
摘要翻译：本发明涉及由与反式异构体含量高的环己烷-1,4-二异氰酸酯与水的反应得到的N，N'-双（4-异氰酸根合环己基）脲。本发明还涉及制备N，N'-双（4-异氰酸根合环己基）脲的方法及其在合成聚氨酯中的用途。

7. 发明授权

US4882361A Process for the production of polyurethane urea elastomers 失效
标题翻译：生产聚氨酯脲弹性体的方法
公开(公告)号：US4882361A
公开(公告)日：1989-11-21
申请号：US245846
申请日：1988-09-16
申请人： Andreas Ruckes , Gerhard Grogler , Richard Kopp
发明人： Andreas Ruckes , Gerhard Grogler , Richard Kopp
IPC分类号： C08G18/65 , C08G18/00 , C08G18/08 , C08G18/38 , C08G101/00 , C08J9/14
CPC分类号： C08G18/3829 , C08G2120/00
摘要： The present invention is directed to a process for the production of compact or cellular, elastomeric moldings having a compact skin based on polyurethane urea elastomers prepared from(a) organic polyisocyanates,(b) relatively high molecular weight polyhydroxyl or polyamino compounds containing at least two reactive hydrogen atoms,(c) diaminodiphenyl ureas as chain-extending agents and optionally,(d) catalysts,(e) small quantities of ethylene glycol,(f) other chain-extending agents and/or cross-linking agents,(g) blowing agents and(h) auxiliaries and/or additives, which is characterized in that the chain-extending agents (c) are diaminodiphenyl ureas corresponding to formula I ##STR1## wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 may be the same or different and represent hydrogen or a C.sub.1 -C.sub.6 alkyl radical and wherein the NH.sub.2 groups are in the m- and/or p-position to the urea group.The present invention is also directed to the RIM elastomers produced by this process.
摘要翻译：本发明涉及一种生产紧凑型或细胞型弹性体模制品的方法，其具有基于由（a）有机多异氰酸酯制备的聚氨酯脲弹性体的紧密表皮，（b）相对高分子量的多羟基或聚氨基化合物，其含有至少两个反应性氢原子，（c）作为扩链剂的二氨基二苯基脲和任选的（d）催化剂，（e）少量乙二醇，（f）其它增链剂和/或交联剂，（g）发泡剂和（h）助剂和/或添加剂，其特征在于扩链剂（c）是对应于式I的二氨基二苯基脲（I），其中R 1，R 2，R 3和R 4可以相同或不同的并且表示氢或C 1 -C 6烷基，并且其中NH 2基团与脲基团的m-位和/或p-位。本发明还涉及通过该方法制备的RIM弹性体。

8. 发明授权

US4994611A Process for the production of N,N'-bis-(3-aminophenyl)-ureas 失效
标题翻译：制备N，N'-二 - （3-氨基苯基） - 脲的方法
公开(公告)号：US4994611A
公开(公告)日：1991-02-19
申请号：US436393
申请日：1989-11-14
申请人： Andreas Ruckes , Gerhard Grogler , Richard Kopp
发明人： Andreas Ruckes , Gerhard Grogler , Richard Kopp
IPC分类号： C07C273/18 , C07C275/40
CPC分类号： C07C273/1854
摘要： The present invention is directed to a process for the preparation of N,N'-bis-(3-aminophenyl)-ureas corresponding to formula (I) ##STR1## wherein R represents a linear or branched C.sub.1 -C.sub.6 alkyl group which is in the 2-, 4- and/or 6-position,characterized in that the corresponding phenylene diamines are reacted with urea in a molar ratio of greater than 2:1 in chlorobenzene as solvent.
摘要翻译：本发明涉及一种制备对应于式（I）的N，N'-双 - （3-氨基苯基） - 脲的方法，其中R表示直链或支链的C 1 -C 6烷基其位于2-，4-和/或6-位，其特征在于相应的亚苯基二胺在氯苯作为溶剂中以大于2:1的摩尔比与脲反应。

9. 发明授权

US5109096A Polyurethane-based one-component reactive adhesives 失效
标题翻译：基于聚氨酯的单组分反应性粘合剂
公开(公告)号：US5109096A
公开(公告)日：1992-04-28
申请号：US535802
申请日：1990-06-11
申请人： Heinrich Hess , Richard Kopp , Gerhard Grogler , Horst Stepanski , Gunter Arend , Hans Tups
发明人： Heinrich Hess , Richard Kopp , Gerhard Grogler , Horst Stepanski , Gunter Arend , Hans Tups
IPC分类号： C08G18/50 , C08G18/65 , C08G18/66 , C08G18/78 , C08G18/79 , C09J175/00 , C09J175/04 , C09J175/12
CPC分类号： C08G18/6529 , C08G18/5024 , C08G18/5036 , C08G18/6677 , C08G18/6685 , C08G18/7825 , C08G18/798 , C09J175/12
摘要： The present invention is directed to a reactive polyurethane mixture comprising:A) at least one polyisocyanate,B) a polyol mixture comprising:B1) at least one polyol containing three or more hydroxyl groups and having a molecular weight in the range from 800 to 6,000,B2) at least one polyol containing three or more hydroxyl groups and having a molecular weight in the range from 400 to 799 andB3) at least one polyol containing three or more hydroxyl groups and having a molecular weight in the range from 92 to 399, andC) at least one polyamine.
摘要翻译：本发明涉及一种反应性聚氨酯混合物，其包含：A）至少一种多异氰酸酯，B）多元醇混合物，其包含：B1）至少一种含有三个或更多个羟基且分子量在800至6000 ，B2）至少一种含有三个或多个羟基并且分子量在400至799范围内的多元醇和B3）至少一种含有三个或更多个羟基且分子量在92至399范围内的羟基的多元醇，和C）至少一种多胺。

10. 发明授权

US5100998A Process for improving the flowability of dimerized 2,4-tolylenediisocyanate 失效
标题翻译：提高二甲基亚砜的流动性的方法
公开(公告)号：US5100998A
公开(公告)日：1992-03-31
申请号：US638879
申请日：1991-01-08
申请人： Richard Kopp , Gerhard Grogler , Heinrich Hess , Lutz Georgias , Helmut Hurnik , Hans D. Thomas
发明人： Richard Kopp , Gerhard Grogler , Heinrich Hess , Lutz Georgias , Helmut Hurnik , Hans D. Thomas
IPC分类号： B01J13/00 , C01B33/18 , C07D229/00 , C08G18/79 , C08K3/36 , C08K5/04
CPC分类号： C08G18/798 , C07D229/00
摘要： The invention relates to a process for improving the flowability and preventing the agglomeration of finely divided dimerized 2,4-toluene diisocyanate in which a precipitated silicas and/or pyrogenic silica having a hydrophobic surface is added to the finely divided dimerized 2,4-toluene diisocyanate. The invention also relates to the finely divided dimerized 2,4-toluene diisocyanate prepared by this process.
摘要翻译：本发明涉及一种改善流动性并防止细碎的二聚2,4-甲苯二异氰酸酯团聚的方法，其中将沉淀的二氧化硅和/或具有疏水表面的热解二氧化硅加入到细碎的二聚2,4-甲苯二异氰酸酯。本发明还涉及通过该方法制备的细碎的二聚2,4-甲苯二异氰酸酯。

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