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    • 1. 发明授权
    • Process and device for simulated moving bed separation with a reduced number of valves and lines
    • 用于模拟移动床分离的过程和装置,阀和线路数量减少
    • US07582208B2
    • 2009-09-01
    • US12073697
    • 2008-03-07
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Aügier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Aügier
    • B01D15/08
    • G01N30/38B01D15/1842B01D53/0423B01D53/06B01D2257/7027B01D2259/4148C07C1/26C07C17/10C07C2529/40G01N30/02C07C9/00C07C19/075B01D15/1821
    • The invention concerns a simulated moving bed adsorption separation device comprising a limited number of valves. According to the invention, the device comprises a column with a plurality of sectors Sk with 2 superimposed plates Pi with a single distribution network, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a plate valve Vi. Each line Lk comprises a flow limitation means and is connected to each of the fluid networks via a single valve.Further, the connectors of lines Lk onto the column are offset by at most 20° inside Sk to limit the volume of lines Lk, and are offset by a mean angle in the range 70° to 110° between two neighbouring sectors Sk and Sk+1 so as not to weaken the column mechanically. The plates preferably comprise panels DMEi,j with parallel segments the direction of which varies from plate to plate or per group of 2 plates.The invention also concerns a separation process using said device, in particular to separate para-xylene or meta-xylene from an aromatic C8 cut.
    • 本发明涉及包括有限数量的阀的模拟移动床吸附分离装置。 根据本发明,该装置包括具有多个扇区Sk的列,具有具有单个分配网络的2个叠加板Pi,每个扇区Sk包括经由板阀Vi连接到Sk的每个板Pi的外部主旁路管线Lk。 每条线路Lk包括流量限制装置,并通过单个阀连接到每个流体网络。 此外,线路Lk到列上的连接器在Sk内部偏移至多20°以限制线路Lk的体积,并且被两个相邻扇区之间的平均角度偏移在70°至110°之间Sk和Sk + 1,以免机械地削弱色谱柱。 板优选地包括具有平行段的面板DMEi,j,其平行段的方向从板到板或每组2个板变化。 本发明还涉及使用所述装置的分离方法,特别是将芳族C8馏分的对二甲苯或间二甲苯分离出来。
    • 2. 发明授权
    • Process and device for simulated moving bed separation with a reduced number of valves
    • 用于模拟移动床分离的过程和装置,减少阀门数量
    • US07582206B2
    • 2009-09-01
    • US11890526
    • 2007-08-07
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/08
    • G01N30/6069B01D15/1842B01D53/0423B01D53/0446B01D2256/24B01D2257/7027B01D2259/4148C07C7/12G01N30/02G01N30/44C07C15/08B01D15/1821
    • A simulated moving bed (SMB) separation device comprising a column, beds Ai of adsorbent separated by plates Pi with a single distribution and extraction network for fluids, in particular feed F, desorbant D, raffinate R and extract B, and a plurality of two-way valves for distribution of said fluids, said valves being limited in number compared with the prior art. The column is divided into a plurality of sectors Sk with 2 or 3 superimposed plates, each sector Sk comprising an external bypass line Lk connected to each plate Pi of Sk via a connector comprising a plate valve Vi. Each line Lk comprises a controlled means for limiting its internal flow, and is connected to each of the fluid networks F, D, R, E via a single line comprising a single controlled two-way isolation valve to supply for sequential supply or withdrawal of the corresponding fluid F, D, R or E towards or from the sector Sk under consideration. The SMB device may be used for the separation of para-xylene or meta-xylene from an aromatic C8 cut.
    • 包括柱的模拟移动床(SMB)分离装置,具有用于流体的单个分配和提取网络的板Pi分离的吸附剂的吸附剂Ai,特别是进料F,脱硫剂D,萃余液R和萃取物E,以及多个二 用于分配所述流体的通道阀,与现有技术相比,所述阀的数量受到限制。 该列被分成具有2或3个叠加板的多个扇区Sk,每个扇区Sk包括通过包括板阀Vi的连接器连接到Sk的每个板Pi的外部旁路管线Lk。 每条线路Lk包括用于限制其内部流动的受控装置,并且经由包括单个受控双向隔离阀的单个管线连接到每个流体网络F,D,R,E,以供供应连续供应或撤出 相应的液体F,D,R或E朝向或来自所考虑的部分Sk。 SMB装置可用于从芳香C8馏分分离对二甲苯或间二甲苯。
    • 3. 发明授权
    • Process and device for simulated moving bed separation with a reduced number of large diameter valves
    • 具有减少数量的大直径阀门的模拟移动床分离的过程和装置
    • US07582207B2
    • 2009-09-01
    • US11907625
    • 2007-10-15
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/08
    • B01D15/1842C07C7/13G01N30/44C07C15/08
    • The invention concerns a simulated moving bed (SMB) separation device and process comprising a column, beds Ai of adsorbent separated by plates Pi with a single distribution and extraction network for fluids, in particular feed F, desorbant D, raffinate R and extract E, and a plurality of two-way valves for distribution of said fluids, said valves being limited in number and in particular with dimensions that are smaller than in the prior art. According to the invention, the column is divided into a plurality of sectors Sk with 2 superimposed plates, each sector Sk comprising an external principal bypass line Lk connected to each plate P1 of Sk via a large diameter plate valve V1 and an external secondary bypass line Mk comprising a small diameter valve VMk connected to the adjacent sector Sk−1. Each line Lk comprises a flow limitation means, and is connected to each of the fluid networks F, D, R, E via a single large diameter valve for sequential supply or withdrawal of the corresponding fluid F, D, R or E to or from the sector Sk under consideration.
    • 本发明涉及一种模拟移动床(SMB)分离装置和方法,该装置包括一个柱,吸附剂分离的吸附剂的吸附剂Ai用具有单一分布的流体分离和萃取网络,特别是进料F,脱硫剂D,萃余液R和提取物E, 以及用于分配所述流体的多个二通阀,所述阀的数量受到限制,特别是尺寸小于现有技术中的尺寸。 根据本发明,列被分成具有2个叠加板的多个扇区Sk,每个扇区Sk包括通过大直径板阀Vi连接到Sk的每个板Pi的外部主旁路管线Lk和外部辅助旁路管线 Mk包括连接到相邻扇区Sk-1的小直径阀VMk。 每条线路Lk包括流量限制装置,并经由单个大直径阀连接到每个流体网络F,D,R,E,用于将相应的流体F,D,R或E顺序地供给或从其中取出 正在考虑的部门Sk。
    • 4. 发明申请
    • PROCESS AND DEVICE FOR SIMULATED MOVING BED SEPARATION WITH A REDUCED NUMBER OF LARGE DIAMETER VALVES AND A REDUCED LINE VOLUME
    • 用于模拟移动床分离的过程和装置,具有减少的大直径阀和减少的线体积
    • US20080217232A1
    • 2008-09-11
    • US12044306
    • 2008-03-07
    • Gerard HOTIERPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HOTIERPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/08
    • B01D15/1842C07C7/12C07C15/08C07C9/00
    • The invention concerns a simulated moving bed adsorption separation device comprising a limited number of large diameter valves. According to the invention, the device comprises a column with a plurality of sectors Sk with 2 superimposed plates Pi with a single distribution network, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a large diameter plate valve Vi and an external secondary bypass line Mk comprising a small diameter valve VMk connected to the adjacent sector Sk−1. Each line Lk comprises a flow rate limitation means and is connected to each fluid network via a single large diameter valve. Further, the connectors of lines Lk onto the column are offset by at most 20° inside Sk to limit the volume of lines Lk, and are offset by a mean angle in the range 70° to 110° between two neighbouring sectors Sk and Sk+1 so as not to weaken the column mechanically. The plates preferably comprise panels DMEi,j with parallel segments the direction of which varies from plate to plate or per group of 2 plates.The invention also concerns a separation process using said device.
    • 本发明涉及包含有限数量的大直径阀的模拟移动床吸附分离装置。 根据本发明,该装置包括具有多个扇区Sk的列,具有具有单个分配网络的2个叠加板Pi,每个扇区Sk包括通过大直径板阀连接到每个Sk板的Pi的外部主旁路管线Lk Vi和外部辅助旁路管线Mk,其包括连接到相邻扇区Sk-1的小直径阀VMk。 每条线路Lk包括流量限制装置,并通过单个大直径阀连接到每个流体网络。 此外,线路Lk到列上的连接器在Sk内部偏移至多20°以限制线路Lk的体积,并且被两个相邻扇区之间的平均角度偏移在70°至110°之间Sk和Sk + 1,以免机械地削弱色谱柱。 板优选地包括具有平行段的面板DMEi,j,其平行段的方向从板到板或每组2个板变化。 本发明还涉及使用所述装置的分离方法。
    • 5. 发明申请
    • Process and device for simulated moving bed separation with a reduced number of large diameter valves
    • 具有减少数量的大直径阀门的模拟移动床分离的过程和装置
    • US20080121586A1
    • 2008-05-29
    • US11907625
    • 2007-10-15
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/08
    • B01D15/1842C07C7/13G01N30/44C07C15/08
    • The invention concerns a simulated moving bed (SMB) separation device and process comprising a column, beds Ai of adsorbent separated by plates Pi with a single distribution and extraction network for fluids, in particular feed F, desorbant D, raffinate R and extract E, and a plurality of two-way valves for distribution of said fluids, said valves being limited in number and in particular with dimensions that are smaller than in the prior art. According to the invention, the column is divided into a plurality of sectors Sk with 2 superimposed plates, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a large diameter plate valve Vi and an external secondary bypass line Mk comprising a small diameter valve VMk connected to the adjacent sector Sk−1. Each line Lk comprises a flow limitation means, and is connected to each of the fluid networks F, D, R, E via a single large diameter valve for sequential supply or withdrawal of the corresponding fluid F, D, R or E to or from the sector Sk under consideration.
    • 本发明涉及一种模拟移动床(SMB)分离装置和方法,该装置包括一列,通过单独的分配和提取网络由板分离的吸附剂分离的吸附剂床 流体,特别是进料F,脱硫剂D,萃余液R和萃取物E,以及用于分配所述流体的多个二通阀,所述阀的数量受到限制,特别是尺寸小于现有技术中的尺寸。 根据本发明,列被分成具有2个叠加板的多个扇区S N,每个扇区S N包括外部主旁路线L k 通过大直径平板阀V I和外部次级旁通管线M'连接到S< S>的每个板P i i / 其包括连接到相邻扇区S k-1的小直径阀V M k N N。 每条线路包括流量限制装置,并且通过单个大直径阀连接到每个流体网络F,D,R,E,以顺序地供应或取出相应的流体F, D,R或E到或来自所考虑的部门Sk。
    • 6. 发明授权
    • Process and device for simulated moving bed separation with a reduced number of large diameter valves and a reduced line volume
    • 用于模拟移动床分离的过程和装置,减少了大直径阀门的数量和减少的管线体积
    • US07569141B2
    • 2009-08-04
    • US12044306
    • 2008-03-07
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/08
    • B01D15/1842C07C7/12C07C15/08C07C9/00
    • The invention concerns a simulated moving bed adsorption separation device comprising a limited number of large diameter valves. According to the invention, the device comprises a column with a plurality of sectors Sk with 2 superimposed plates Pi with a single distribution network, each sector Sk comprising an external principal bypass line Lk connected to each plate Pi of Sk via a large diameter plate valve Vi and an external secondary bypass line Mk comprising a small diameter valve VMk connected to the adjacent sector Sk−1. Each line Lk comprises a flow rate limitation means and is connected to each fluid network via a single large diameter valve. Further, the connectors of lines Lk onto the column are offset by at most 20° inside Sk to limit the volume of lines Lk, and are offset by a mean angle in the range 70° to 110° between two neighbouring sectors Sk and Sk+1 so as not to weaken the column mechanically. The plates preferably comprise panels DMEi,j with parallel segments the direction of which varies from plate to plate or per group of 2 plates.The invention also concerns a separation process using said device.FIG. 2 to be published.
    • 本发明涉及包含有限数量的大直径阀的模拟移动床吸附分离装置。 根据本发明,该装置包括具有多个扇区Sk的列,具有具有单个分配网络的2个叠加板Pi,每个扇区Sk包括通过大直径板阀连接到每个Sk板的Pi的外部主旁路管线Lk Vi和外部辅助旁路管线Mk,其包括连接到相邻扇区Sk-1的小直径阀VMk。 每条线路Lk包括流量限制装置,并通过单个大直径阀连接到每个流体网络。 此外,线路Lk到列上的连接器在Sk内部偏移至多20°以限制线路Lk的体积,并且被两个相邻扇区之间的平均角度偏移在70°至110°之间Sk和Sk + 1,以免机械地削弱色谱柱。 板优选地包括具有平行段的面板DMEi,j,其平行段的方向从板到板或每组2个板变化。 本发明还涉及使用所述装置的分离方法。 2 发布。
    • 8. 发明申请
    • Process and device for simulated moving bed seperation with a reduced number of valves
    • 用于模拟移动床分离的过程和装置,阀门数量减少
    • US20080041788A1
    • 2008-02-21
    • US11890526
    • 2007-08-07
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • Gerard HotierPhilibert LeflaiveSylvain LouretFrederic Augier
    • B01D15/10B01D53/04B01J8/04
    • G01N30/6069B01D15/1842B01D53/0423B01D53/0446B01D2256/24B01D2257/7027B01D2259/4148C07C7/12G01N30/02G01N30/44C07C15/08B01D15/1821
    • The invention concerns a simulated moving bed (SMB) separation device comprising a column, beds Ai of adsorbent separated by plates Pi with a single distribution and extraction network for fluids, in particular feed F, desorbant D, raffinate R and extract E, and a plurality of two-way valves for distribution of said fluids, said valves being limited in number compared with the prior art. According to the invention, the column is divided into a plurality of sectors Sk with 2 or 3 superimposed plates, each sector Sk comprising an external bypass line Lk connected to each plate Pi of Sk via a connector comprising a plate valve Vi. Each line Lk comprises a controlled means for limiting its internal flow, and is connected to each of the fluid networks F, D, R, E via a single line comprising a single controlled two-way isolation valve to supply for sequential supply or withdrawal of the corresponding fluid F, D, R or E towards or from the sector Sk under consideration. The invention also concerns a separation process using said device or the use of said device for the separation of para-xylene or meta-xylene from an aromatic C8 cut.
    • 本发明涉及一种包括柱的模拟移动床(SMB)分离装置,具有通过单个分配的板Pi和用于流体的提取网络,特别是进料F,脱附剂D,萃余液R和萃取物E分离的吸附剂的吸附剂Ai,以及 用于分配所述流体的多个二通阀,与现有技术相比,所述阀的数量受到限制。 根据本发明,列被分成具有2或3个重叠板的多个扇区Sk,每个扇区Sk包括通过包括板阀Vi的连接器连接到Sk的每个板Pi的外部旁路管线Lk。 每条线路Lk包括用于限制其内部流动的受控装置,并且经由包括单个受控双向隔离阀的单个管线连接到每个流体网络F,D,R,E,以供供应连续供应或撤出 相应的液体F,D,R或E朝向或来自所考虑的部分Sk。 本发明还涉及使用所述装置的分离方法或所述装置用于从芳族C8馏分分离对二甲苯或间二甲苯的分离方法。