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1. 发明申请

WO2014082086A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译：聚合树脂和碳材料的制备
公开(公告)号：WO2014082086A1
公开(公告)日：2014-05-30
申请号：PCT/US2013/072050
申请日：2013-11-26
申请人： GEORGIA-PACIFIC CHEMICALS LLC , ENERG2 TECHNOLOGIES, INC.
发明人： GERAMITA, Katharine , KRON, Benjamin E. , COSTANTINO, Henry R. , FEAVER, Aaron M. , SAKSHAUG, Avery , THOMPKINS, Leah A. , CHANG, Alan Tzu-Yang , DONG, Xing , QURESHI, Shahid P. , HINES, John B. , KNAZEK, Gerald A. , LUDVIK, Joseph Frank
IPC分类号： C01B31/02 , B01J6/00
CPC分类号： C01B32/30 , B01J6/00 , C01B32/00 , C01B32/05 , C01B32/312 , C01P2004/51 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , H01G11/04 , H01G11/34 , H01G11/38 , H01M4/583 , H01M4/587 , H01M4/96
摘要： Methods for making carbon materials are provided. In at least one specific embodiment, the method can include combining one or more polymer precursors with one or more liquids to produce a mixture. The mixture can be an emulsion, dispersion, or a suspension. The liquid can include hexane, pentane, cyclopentane, benzene, toluene, o-xylene, m-xylene, p-xylene, diethyl ether, ethylmethylketone, dichloromethane, tetrahydrofuran, mineral oils, paraffin oils, vegetable derived oils, or any mixture thereof. The method can also include aging the mixture at a temperature and time sufficient for the polymer precursor to react and form polymer gel particles having a volume average particle size (Dv,50) of the polymer particles in gel form greater than or equal to 1 mm. The method can also include heating the polymer gel particles to produce a carbon material.
摘要翻译：提供制造碳材料的方法。在至少一个具体实施方案中，该方法可以包括将一种或多种聚合物前体与一种或多种液体组合以产生混合物。混合物可以是乳液，分散体或悬浮液。液体可以包括己烷，戊烷，环戊烷，苯，甲苯，邻二甲苯，间二甲苯，对二甲苯，乙醚，乙基甲基酮，二氯甲烷，四氢呋喃，矿物油，石蜡油，植物衍生油或其任何混合物。该方法还可以包括在足以使聚合物前体反应的温度和时间下老化混合物，并形成凝胶形式的聚合物颗粒的体积平均粒径（Dv，50）大于或等于1mm的聚合物凝胶颗粒。该方法还可以包括加热聚合物凝胶颗粒以产生碳材料。

2. 发明申请

WO2013120009A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译：聚合树脂和碳材料的制备
公开(公告)号：WO2013120009A1
公开(公告)日：2013-08-15
申请号：PCT/US2013/025421
申请日：2013-02-08
申请人： GEORGIA-PACIFIC CHEMICALS LLC , ENERG2 TECHNOLOGIES, INC.
发明人： LUDVIK, Joseph, F. , DONG, Xing , QURESHI, Shahid, P. , HINES, John, B. , KNAZEK, Gerald , RICHARD, Renette, E. , GERAMITA, Katharine , KRON, Benjamin, E. , COSTANTINO, Henry, R. , FEAVER, Aaron, M. , SAKSHAUG, Avery , THOMPKINS, Leah, A. , CHANG, Alan, Tzu-Yang
IPC分类号： C08J3/12 , C08F2/00 , C01B31/00 , H01G9/04
CPC分类号： C01B31/10 , C01B32/336 , H01G11/24 , H01G11/34 , H01G11/42 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E60/13
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials can have enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries.
摘要翻译：本申请涉及制备凝胶形式的聚合物颗粒和由其制备的碳材料的方法。碳材料可以具有增强的电化学性质，并且可用于任何数量的电气装置，例如作为超级电容器或电池中的电极材料。

3. 发明公开

EP2812379A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译： [聚合物树脂和炭素材料
公开(公告)号：EP2812379A1
公开(公告)日：2014-12-17
申请号：EP13746702.3
申请日：2013-02-08
申请人： Georgia-Pacific Chemicals LLC , Energ2 Technologies, Inc.
发明人： LUDVIK, Joseph, F. , DONG, Xing , QURESHI, Shahid, P. , HINES, John, B. , KNAZEK, Gerald , RICHARD, Renette, E. , GERAMITA, Katharine , KRON, Benjamin, E. , COSTANTINO, Henry, R. , FEAVER, Aaron, M. , SAKSHAUG, Avery , THOMPKINS, Leah, A. , CHANG, Alan, Tzu-Yang
IPC分类号： C08J3/12 , C08F2/00 , C01B31/00 , H01G9/04
CPC分类号： C01B31/10 , C01B32/336 , H01G11/24 , H01G11/34 , H01G11/42 , H01M4/133 , H01M4/1393 , H01M4/587 , H01M4/625 , H01M10/0525 , Y02E60/13
摘要： The present application is directed to methods for preparation of polymer particles in gel form and carbon materials made therefrom. The carbon materials can have enhanced electrochemical properties and find utility in any number of electrical devices, for example, as electrode material in ultracapacitors or batteries.

4. 发明公开

EP2922786A1 PREPARATION OF POLYMERIC RESINS AND CARBON MATERIALS 审中-公开
标题翻译：聚合物树脂和碳材料的制备
公开(公告)号：EP2922786A1
公开(公告)日：2015-09-30
申请号：EP13857632.7
申请日：2013-11-26
申请人： Georgia-Pacific Chemicals LLC , Energ2 Technologies, Inc.
发明人： GERAMITA, Katharine , KRON, Benjamin E. , COSTANTINO, Henry R. , FEAVER, Aaron M. , SAKSHAUG, Avery , THOMPKINS, Leah A. , CHANG, Alan Tzu-Yang , DONG, Xing , QURESHI, Shahid P. , HINES, John B. , KNAZEK, Gerald A. , LUDVIK, Joseph Frank
IPC分类号： C01B31/02 , B01J6/00
CPC分类号： C01B32/30 , B01J6/00 , C01B32/00 , C01B32/05 , C01B32/312 , C01P2004/51 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , H01G11/04 , H01G11/34 , H01G11/38 , H01M4/583 , H01M4/587 , H01M4/96
摘要： Methods for making carbon materials are provided. In at least one specific embodiment, the method can include combining one or more polymer precursors with one or more liquids to produce a mixture. The mixture can be an emulsion, dispersion, or a suspension. The liquid can include hexane, pentane, cyclopentane, benzene, toluene, o-xylene, m-xylene, p-xylene, diethyl ether, ethylmethylketone, dichloromethane, tetrahydrofuran, mineral oils, paraffin oils, vegetable derived oils, or any mixture thereof. The method can also include aging the mixture at a temperature and time sufficient for the polymer precursor to react and form polymer gel particles having a volume average particle size (Dv,50) of the polymer particles in gel form greater than or equal to 1 mm. The method can also include heating the polymer gel particles to produce a carbon material.
摘要翻译：提供了制造碳材料的方法。在至少一个具体实施方案中，该方法可以包括将一种或多种聚合物前体与一种或多种液体混合以产生混合物。该混合物可以是乳液，分散体或悬浮液。液体可以包括己烷，戊烷，环戊烷，苯，甲苯，邻二甲苯，间二甲苯，对二甲苯，二乙醚，乙基甲基酮，二氯甲烷，四氢呋喃，矿物油，石蜡油，植物衍生油或其任何混合物。该方法还可包括在足以使聚合物前体反应并形成具有凝胶形式的聚合物颗粒的体积平均粒度（Dv，50）大于或等于1mm的聚合物凝胶颗粒的温度和时间下熟化该混合物。该方法还可以包括加热聚合物凝胶颗粒以产生碳材料。

5. 发明申请

WO2015175584A1 ACTIVATED CARBON PRODUCTS AND METHODS FOR MAKING AND USING SAME 审中-公开
标题翻译：活性炭产品及其制备和使用方法
公开(公告)号：WO2015175584A1
公开(公告)日：2015-11-19
申请号：PCT/US2015/030447
申请日：2015-05-13
申请人： GEORGIA-PACIFIC CHEMICALS LLC
发明人： DONG, Xing , TULL, Scott W.
IPC分类号： C01B31/08 , C01B31/12
CPC分类号： C01B31/08 , C01B32/30 , C01B32/336 , C01B32/342 , C01B32/348 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/80
摘要： Activated carbon products and methods for making same. In one example, activated carbon products can have a specific surface area of at least 3,050 m2/g to about 7,000 m2/g, a pore volume of about 3 cm3/g to about 10 cm3/g, and an average pore size of about 0.5 nm to about 150 nm. In one example, activated carbon products can be made by reacting a hydroxybenzene compound and an aldehyde compound in the presence of a solvent to produce a prepolymer. The prepolymer and an additive can be reacted to produce a wet gel product that can be dried, pyrolized, and activated to produce an activated carbon product. The activated carbon product can have a specific surface area of about 100 m2/g to about 7,000 m2/g, a pore volume of about 0.2 cm3/g to about 10 cm3/g, and/or an average pore size of about 0.5 nm to about 150 nm.
摘要翻译：活性炭产品及其制备方法。在一个实例中，活性炭产物可以具有至少3050m 2 / g至约7,000m 2 / g的比表面积，约3cm 3 / g至约10cm 3 / g的孔体积和约 0.5nm至约150nm。在一个实例中，活性炭产物可以通过在溶剂存在下使羟基苯化合物和醛化合物反应来制备预聚物。可以将预聚物和添加剂反应以产生可以干燥，热解和活化以产生活性炭产物的湿凝胶产物。活性炭产物可以具有约100m 2 / g至约7,000m 2 / g的比表面积，约0.2cm 3 / g至约10cm 3 / g的孔体积和/或约0.5nm的平均孔径至约150nm。

6. 发明申请

WO2015042271A1 METHODS FOR MAKING WET GELS AND DRIED GELS THEREFROM 审中-公开
标题翻译：用于制造湿凝胶和干凝胶的方法
公开(公告)号：WO2015042271A1
公开(公告)日：2015-03-26
申请号：PCT/US2014/056321
申请日：2014-09-18
申请人： GEORGIA-PACIFIC CHEMICALS LLC
发明人： DONG, Xing , QURESHI, Shahid P. , LEE, Christopher M. , SHOEMAKE, Kelly A. , LUDVIK, Joseph Frank
IPC分类号： C08J3/075 , C08G8/10
CPC分类号： C08G8/28 , C01B32/30 , C08G8/32 , C08G16/0225 , C08G16/0256 , C08G81/00 , C08J2201/0504 , C08J2205/022
摘要： Methods for making wet gels and dried gels therefrom are provided. The method for making a wet gel can include combining a hydroxybenzene compound, an aldehyde compound, and an additive to produce a reaction mixture. The additive can include a carboxylic acid, an anhydride, a homopolymer, a copolymer, or any mixture thereof. At least the hydroxybenzene compound and the aldehyde compound can be reacted to produce a wet gel. The reaction mixture can include about 10 wt% to about 65 wt% of the hydroxybenzene compound, about 5 wt% to about 25 wt% of the aldehyde compound, up to about 85 wt% of the carboxylic acid, up to about 40 wt% of the anhydride, up to about 40 wt% of the homopolymer, and up to about 40 wt% of the copolymer, where weight percent values are based on the combined weight of the hydroxybenzene compound, the aldehyde compound, and the additive.
摘要翻译：提供了制备湿凝胶和干凝胶的方法。制备湿凝胶的方法可以包括组合羟基苯化合物，醛化合物和添加剂以产生反应混合物。添加剂可以包括羧酸，酸酐，均聚物，共聚物或其任何混合物。至少可以使羟基苯化合物和醛化合物反应以产生湿凝胶。反应混合物可以包括约10重量％至约65重量％的羟基苯化合物，约5重量％至约25重量％的醛化合物，至多约85重量％的羧酸，至多约40重量％的酸酐，最多约40重量％的均聚物和至多约40重量％的共聚物，其中重量百分数值是基于羟基苯化合物，醛化合物和添加剂的总重量。

7. 发明申请

WO2014085603A1 PREPARATION OF PHENOL-FORMALDEHYDE RESIN BEADS USING SUSPENSION OR EMULSION POLYMERIZATION 审中-公开
标题翻译：使用悬浮或乳液聚合制备酚醛树脂珠粒
公开(公告)号：WO2014085603A1
公开(公告)日：2014-06-05
申请号：PCT/US2013/072258
申请日：2013-11-27
申请人： GEORGIA-PACIFIC CHEMICALS LLC
发明人： QURESHI, Shahid, P. , DONG, Xing , CHAN, Charles, C. , LUDVIK, Joseph, Frank
IPC分类号： C08G8/10 , C08J3/12 , C08J9/00
CPC分类号： C08G8/32 , C08G8/10 , C08G8/22 , C08G85/004 , C08J9/16 , C08J9/28 , C08J2201/026 , C08J2201/0482 , C08J2201/0502 , C08J2205/02 , C08J2361/06
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension polymerization are provided. In at least one specific embodiment, the method can include reacting a first reaction mixture comprising a phenolic monomer, an aldehyde monomer, and a first catalyst to produce a prepolymer. The method can also include combining the prepolymer with a carrier fluid and a second catalyst to produce a second reaction mixture. The second catalyst can include a dicarboxylic acid, an anhydride, a dihydroxybenzene, or any mixture thereof. The method can also include polymerizing the prepolymer to form polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮聚合制备凝胶形式的聚合物颗粒的方法。在至少一个具体实施方案中，该方法可以包括使包含酚单体，醛单体和第一催化剂的第一反应混合物反应以产生预聚物。该方法还可以包括将预聚物与载体流体和第二催化剂组合以产生第二反应混合物。第二催化剂可以包括二羧酸，酸酐，二羟基苯或其任何混合物。该方法还可包括聚合预聚物以形成凝胶形式的聚合物颗粒。

8. 发明申请

WO2013120028A1 METHODS FOR MAKING POLYMER PARTICULATES IN GEL FORM 审中-公开
标题翻译：在凝胶形式中制备聚合物颗粒的方法
公开(公告)号：WO2013120028A1
公开(公告)日：2013-08-15
申请号：PCT/US2013/025448
申请日：2013-02-08
申请人： GEORGIA PACIFIC CHEMICALS LLC , LUDVIK, Joseph , DONG, Xing
发明人： LUDVIK, Joseph , DONG, Xing
IPC分类号： C08J3/12 , C08F2/00 , C08F2/22 , C08J3/075
CPC分类号： C08L71/00 , C04B24/12 , C04B24/36 , C05C3/00 , C08F2/22 , C08G14/06 , C08G14/12 , C09B67/00 , F26B3/00
摘要： Methods for making polymer particles in gel form via an emulsion and/or suspension process are provided. The method can include preparing a reactant mixture comprising a carrier fluid and a monomer component containing one or more phenolic compounds and optionally one or more crosslinking compounds, a mixture of Maillard reactants, or a combination thereof. The monomer component can polymerize to form the polymer particles in gel form. The reactant mixture can be located within a reactor having one or more inner surfaces in contact with the reactant mixture during polymerization of the monomer component. The one or more inner surfaces limit a release of metal, metal ions, or a combination thereof into the reactant mixture to produce the polymer particles in gel form containing less than 1 wt% metal atoms, metal ions, or a combination thereof, based on the total weight of the polymer particles in gel form.
摘要翻译：提供了通过乳液和/或悬浮方法制备凝胶形式的聚合物颗粒的方法。该方法可以包括制备包含载体流体和含有一种或多种酚类化合物和任选的一种或多种交联化合物，美拉德反应物的混合物或其组合的单体组分的反应物混合物。单体组分可以聚合形成凝胶形式的聚合物颗粒。反应物混合物可以位于反应器内，所述反应器具有在单体组分聚合期间与反应物混合物接触的一个或多个内表面。一个或多个内表面将金属，金属离子或其组合的释放限制在反应物混合物中，以基于以下方式产生包含小于1重量％的金属原子，金属离子或其组合的凝胶形式的聚合物颗粒凝胶形式的聚合物颗粒的总重量。

9. 发明授权

EP3046950B1 METHODS FOR MAKING WET GELS AND DRIED GELS THEREFROM 有权
公开(公告)号：EP3046950B1
公开(公告)日：2019-07-24
申请号：EP14846257.5
申请日：2014-09-18
申请人： Georgia-Pacific Chemicals LLC
发明人： DONG, Xing , QURESHI, Shahid P. , LEE, Christopher M. , SHOEMAKE, Kelly A. , LUDVIK, Joseph Frank
IPC分类号： C08J3/075 , C08G16/02 , C08G8/28 , C08G8/32

10. 发明公开

EP3142968A1 ACTIVATED CARBON PRODUCTS AND METHODS FOR MAKING AND USING SAME 审中-公开
标题翻译：活性炭产品和方法进行生产及其用途
公开(公告)号：EP3142968A1
公开(公告)日：2017-03-22
申请号：EP15792216.2
申请日：2015-05-13
申请人： Georgia-Pacific Chemicals LLC
发明人： DONG, Xing , TULL, Scott W.
IPC分类号： C01B32/30 , C01B32/342
CPC分类号： C01B31/08 , C01B32/30 , C01B32/336 , C01B32/342 , C01B32/348 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/80
摘要： Activated carbon products and methods for making same. In one example, activated carbon products can have a specific surface area of at least 3,050 m2/g to about 7,000 m2/g, a pore volume of about 3 cm3/g to about 10 cm3/g, and an average pore size of about 0.5 nm to about 150 nm. In one example, activated carbon products can be made by reacting a hydroxybenzene compound and an aldehyde compound in the presence of a solvent to produce a prepolymer. The prepolymer and an additive can be reacted to produce a wet gel product that can be dried, pyrolized, and activated to produce an activated carbon product. The activated carbon product can have a specific surface area of about 100 m2/g to about 7,000 m2/g, a pore volume of about 0.2 cm3/g to about 10 cm3/g, and/or an average pore size of about 0.5 nm to about 150 nm.
摘要翻译：活性炭产品及其制造方法。在一个实施例，活性炭产品可具有至少3050米2 / g的比表面积为约7000平方米/克，约3cm 3 / g的孔体积至约10厘米3 /克，并在约平均孔径 0.5nm至在一个实施例约为150，活性炭产品可以通过使羟基苯化合物和醛化合物在溶剂的存在下，以产生预聚物纳米制成.. 将预聚物和添加剂可以反应以产生湿凝胶productsthat可以干燥，热解，和活化以产生活性碳上的产物。活性炭产物可以具有约100m 2 / g的比表面积以约7000米2 /克，约0.2厘米3 /克至约10 3 / g的孔体积，和/或至约0.5nm的平均孔尺寸至约150nm。

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