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1. 发明授权

US08394988B2 Production of acetic acid with high conversion rate 有权
标题翻译：生产乙酸，转化率高
公开(公告)号：US08394988B2
公开(公告)日：2013-03-12
申请号：US12892348
申请日：2010-09-28
申请人： G. Paull Torrence , Brian W. Hokkanen , Michael O. Nutt , Tianshu Pan , Ronald David Shaver
发明人： G. Paull Torrence , Brian W. Hokkanen , Michael O. Nutt , Tianshu Pan , Ronald David Shaver
IPC分类号： C07C51/12
CPC分类号： C07C51/12 , B01J19/00 , C07C51/44 , C07C53/08
摘要： A process for producing acetic acid comprising the steps of reacting carbon monoxide and at least one of methanol and a methanol derivative in a first reactor under conditions effective to produce a crude acetic acid product; separating the crude acetic acid product into at least one derivative stream, at least one of the at least one derivative stream comprising residual carbon monoxide; and reacting at least a portion of the residual carbon monoxide with at least one of methanol and a methanol derivative over a metal catalyst in a second reactor to produce additional acetic acid.
摘要翻译：一种生产乙酸的方法，包括以下步骤：使一氧化碳与甲醇和甲醇衍生物中的至少一种在有效产生粗乙酸产物的条件下在第一反应器中反应; 将粗乙酸产物分离成至少一种衍生物流，所述至少一种衍生物物流中的至少一种包含残余的一氧化碳; 以及在第二反应器中使至少一部分残留的一氧化碳与甲醇和甲醇衍生物中的至少一种在金属催化剂上反应，以产生另外的乙酸。

2. 发明申请

US20120078012A1 PRODUCTION OF ACETIC ACID WITH HIGH CONVERSION RATE 有权
标题翻译：生产具有高转化率的乙酸
公开(公告)号：US20120078012A1
公开(公告)日：2012-03-29
申请号：US12892348
申请日：2010-09-28
申请人： G. Paull Torrence , Brian W. Hokkanen , Michael O. Nutt , Tianshu Pan , Ronald David Shaver
发明人： G. Paull Torrence , Brian W. Hokkanen , Michael O. Nutt , Tianshu Pan , Ronald David Shaver
IPC分类号： C07C51/12 , B01J8/02 , B01J8/00
CPC分类号： C07C51/12 , B01J19/00 , C07C51/44 , C07C53/08
摘要： A process for producing acetic acid comprising the steps of reacting carbon monoxide and at least one of methanol and a methanol derivative in a first reactor under conditions effective to produce a crude acetic acid product; separating the crude acetic acid product into at least one derivative stream, at least one of the at least one derivative stream comprising residual carbon monoxide; and reacting at least a portion of the residual carbon monoxide with at least one of methanol and a methanol derivative over a metal catalyst in a second reactor to produce additional acetic acid.
摘要翻译：一种生产乙酸的方法，包括以下步骤：使一氧化碳与甲醇和甲醇衍生物中的至少一种在有效产生粗乙酸产物的条件下在第一反应器中反应; 将粗乙酸产物分离成至少一种衍生物流，所述至少一种衍生物物流中的至少一种包含残余的一氧化碳; 以及在第二反应器中使至少一部分残留的一氧化碳与甲醇和甲醇衍生物中的至少一种在金属催化剂上反应，以产生另外的乙酸。

3. 发明授权

US08877963B2 Production of acetic acid with high conversion rate 有权
标题翻译：生产乙酸，转化率高
公开(公告)号：US08877963B2
公开(公告)日：2014-11-04
申请号：US13231205
申请日：2011-09-13
申请人： Brian W. Hokkanen , Michael Nutt , Tianshu Pan , Ronald David Shaver , G. Paull Torrence
发明人： Brian W. Hokkanen , Michael Nutt , Tianshu Pan , Ronald David Shaver , G. Paull Torrence
IPC分类号： C07C51/12 , C07C51/44
CPC分类号： C07C51/12 , C07C51/44 , C07C53/08
摘要： The present invention is to a process for producing acetic acid comprising the step of reacting a carbon monoxide feed and methanol and/or a methanol derivative in a first reactor to produce a crude acetic acid product. The carbon monoxide may comprise less than 99.5 mol % carbon monoxide. The process further comprises the step of purging a carbon monoxide purge stream comprising a first amount of residual carbon monoxide and one or more impurities. Preferably, the first amount is greater than 20 mol %. The process further comprises the step of separating the crude acetic acid product into at least one derivative stream comprising a second amount of residual carbon monoxide. The process further comprises the step of reacting at least a portion of the second amount of residual carbon monoxide and methanol and/or a methanol derivative in a second reactor to produce additional acetic acid.
摘要翻译：本发明涉及一种生产乙酸的方法，包括使一氧化碳原料与甲醇和/或甲醇衍生物在第一反应器中反应生成粗乙酸产物的步骤。一氧化碳可以包含小于99.5mol％的一氧化碳。该方法还包括吹扫包含第一量残余一氧化碳和一种或多种杂质的一氧化碳吹扫流的步骤。优选地，第一量大于20摩尔％。该方法还包括将粗乙酸产物分离成至少一种包含第二量残余一氧化碳的衍生物物流的步骤。该方法还包括使第二量的残留一氧化碳和甲醇和/或甲醇衍生物的至少一部分在第二反应器中反应以产生另外的乙酸的步骤。

4. 发明申请

US20120083623A1 Production of Acetic Acid with High Conversion Rate 有权
标题翻译：高转化率生产乙酸
公开(公告)号：US20120083623A1
公开(公告)日：2012-04-05
申请号：US13231205
申请日：2011-09-13
申请人： Brian W. Hokkanen , Michael Nutt , Tianshu Pan , Ronald David Shaver , G. Paull Torrence
发明人： Brian W. Hokkanen , Michael Nutt , Tianshu Pan , Ronald David Shaver , G. Paull Torrence
IPC分类号： C07C51/12
CPC分类号： C07C51/12 , C07C51/44 , C07C53/08
摘要： The present invention is to a process for producing acetic acid comprising the step of reacting a carbon monoxide feed and methanol and/or a methanol derivative in a first reactor to produce a crude acetic acid product. The carbon monoxide may comprise less than 99.5 mol % carbon monoxide. The process further comprises the step of purging a carbon monoxide purge stream comprising a first amount of residual carbon monoxide and one or more impurities. Preferably, the first amount is greater than 20 mol %. The process further comprises the step of separating the crude acetic acid product into at least one derivative stream comprising a second amount of residual carbon monoxide. The process further comprises the step of reacting at least a portion of the second amount of residual carbon monoxide and methanol and/or a methanol derivative in a second reactor to produce additional acetic acid.
摘要翻译：本发明涉及一种生产乙酸的方法，包括使一氧化碳原料与甲醇和/或甲醇衍生物在第一反应器中反应生成粗乙酸产物的步骤。一氧化碳可以包含小于99.5mol％的一氧化碳。该方法还包括吹扫包含第一量残余一氧化碳和一种或多种杂质的一氧化碳吹扫流的步骤。优选地，第一量大于20摩尔％。该方法还包括将粗乙酸产物分离成至少一种包含第二量残余一氧化碳的衍生物物流的步骤。该方法还包括使第二量的残留一氧化碳和甲醇和/或甲醇衍生物的至少一部分在第二反应器中反应以产生另外的乙酸的步骤。

5. 发明授权

US08569551B2 Alcohol production process integrating acetic acid feed stream comprising water from carbonylation process 有权
标题翻译：乙醇生产工艺将含有羰基化过程的水的乙酸进料流整合
公开(公告)号：US08569551B2
公开(公告)日：2013-10-29
申请号：US13094580
申请日：2011-04-26
申请人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Mark O. Scates , Ronald David Shaver , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
发明人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Mark O. Scates , Ronald David Shaver , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
IPC分类号： C07C29/80
CPC分类号： C07C29/80 , C07C29/149 , C07C29/76 , C07C51/12 , C07C51/44 , Y02P20/582 , C07C31/08 , C07C53/08
摘要： In one embodiment, the invention is to a process for producing ethanol, comprising the step of providing from a distillation column in a carbonylation process a purified acetic acid stream comprising up to 25 wt. % water. The process further comprises the step of hydrogenating acetic acid of the purified acetic acid stream in the presence of a catalyst and under conditions effective to form a crude ethanol product comprising ethanol and water. Ethanol is recovered from the crude ethanol product.
摘要翻译：在一个实施方案中，本发明涉及一种生产乙醇的方法，其包括以下步骤：在羰基化过程中从蒸馏塔提供纯化的乙酸流，其包含至多25重量％％水。该方法还包括在催化剂存在下和有效形成包含乙醇和水的粗乙醇产物的条件下，将纯化的乙酸物流的乙酸氢化的步骤。从粗乙醇产物中回收乙醇。

6. 发明申请

US20120059197A1 ALCOHOL PRODUCTION PROCESS INTEGRATING ACETIC ACID FEED STREAM COMPRISING WATER FROM CARBONYLATION PROCESS 有权
标题翻译：酒精生产工艺从碳化过程中积聚含有水的醋酸饲料流
公开(公告)号：US20120059197A1
公开(公告)日：2012-03-08
申请号：US13094580
申请日：2011-04-26
申请人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Mark O. Scates , Ronald David Shaver , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
发明人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Mark O. Scates , Ronald David Shaver , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
IPC分类号： C07C29/80
CPC分类号： C07C29/80 , C07C29/149 , C07C29/76 , C07C51/12 , C07C51/44 , Y02P20/582 , C07C31/08 , C07C53/08
摘要： In one embodiment, the invention is to a process for producing ethanol, comprising the step of providing from a distillation column in a carbonylation process a purified acetic acid stream comprising up to 25 wt. % water. The process further comprises the step of hydrogenating acetic acid of the purified acetic acid stream in the presence of a catalyst and under conditions effective to form a crude ethanol product comprising ethanol and water. Ethanol is recovered from the crude ethanol product.
摘要翻译：在一个实施方案中，本发明涉及一种生产乙醇的方法，其包括以下步骤：在羰基化过程中从蒸馏塔提供纯化的乙酸流，其包含至多25重量％％水。该方法还包括在催化剂存在下和有效形成包含乙醇和水的粗乙醇产物的条件下，将纯化的乙酸物流的乙酸氢化的步骤。从粗乙醇产物中回收乙醇。

7. 发明授权

US09249081B2 Processes for the production of acrylic acids and acrylates 有权
标题翻译：用于生产丙烯酸和丙烯酸酯的方法
公开(公告)号：US09249081B2
公开(公告)日：2016-02-02
申请号：US13328231
申请日：2011-12-16
申请人： Ilias S. Kotsianis , Sean Mueller , Dick Nagaki , Tianshu Pan , Craig J. Peterson , Josefina T. Chapman
发明人： Ilias S. Kotsianis , Sean Mueller , Dick Nagaki , Tianshu Pan , Craig J. Peterson , Josefina T. Chapman
IPC分类号： C07C51/42 , C07C51/44
CPC分类号： C07C51/42 , C07C51/44
摘要： In one embodiment, the invention is to a process for producing an acrylate product. The process comprises the step of dehydrating a crude alkylenating agent stream to form a dehydrated alkylenating agent stream and a water stream. The process further comprises reacting acetic acid with at least a portion of the dehydrated alkylenating agent stream to form a crude acrylate product stream comprising acrylate product and alkylenating agent stream. The dehydrating of the crude alkylenating stream is accomplished using at least one evaporator or at least one distillation column.
摘要翻译：在一个实施方案中，本发明涉及一种生产丙烯酸酯产物的方法。该方法包括使粗亚烷基化剂流脱水以形成脱水亚烷基化剂流和水流的步骤。该方法还包括使乙酸与脱水亚烷基化剂物流的至少一部分反应以形成包含丙烯酸酯产物和亚烷基化剂物流的粗丙烯酸酯产物流。使用至少一个蒸发器或至少一个蒸馏塔来实现粗烷基化流的脱水。

8. 发明授权

US08309773B2 Process for recovering ethanol 有权
标题翻译：回收乙醇的方法
公开(公告)号：US08309773B2
公开(公告)日：2012-11-13
申请号：US12852227
申请日：2010-08-06
申请人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Lincoln Sarager , R. Jay Warner , Heiko Weiner , Josefina Chapman , Robert Cunningham , Gerald Grusendorf , Trinity Horton
发明人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , Lincoln Sarager , R. Jay Warner , Heiko Weiner , Josefina Chapman , Robert Cunningham , Gerald Grusendorf , Trinity Horton
IPC分类号： C07C29/149
CPC分类号： C07C29/80 , C07C29/149 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude ethanol products are employed to allow recovery of ethanol and remove impurities.
摘要翻译：从乙酸氢化得到的粗乙醇产物中回收乙醇。使用粗乙醇产物的分离和纯化方法来回收乙醇并除去杂质。

9. 发明申请

US20120010439A1 PROCESS FOR RECOVERING ALCOHOL PRODUCED BY HYDROGENATING AN ACETIC ACID FEED STREAM COMPRISING WATER 失效
标题翻译：通过氢化包含水的乙酸饲料回收生产的酒精的方法
公开(公告)号：US20120010439A1
公开(公告)日：2012-01-12
申请号：US13094610
申请日：2011-04-26
申请人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
发明人： Radmila Jevtic , Victor J. Johnston , Tianshu Pan , R. Jay Warner , Heiko Weiner , Josefina T. Chapman
IPC分类号： C07C29/74 , C07C29/80
CPC分类号： C07C29/149 , C07C29/76 , C07C29/80 , C07C51/12 , C07C31/08 , C07C53/08
摘要： Purifying and/or recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid from an feed stream comprising water. The presence of water does not significantly impact acid conversion or selectivity to ethanol. Further the addition of water allows for improved recovery of ethanol.
摘要翻译：从从含有水的进料流中乙酸氢化获得的粗乙醇产物中纯化和/或回收乙醇。水的存在不会显着影响酸转化率或对乙醇的选择性。此外，添加水可以提高乙醇的回收率。

10. 发明申请

US20110275862A1 PROCESS FOR PURIFYING A CRUDE ETHANOL PRODUCT 有权
标题翻译：净化乙醇产品的方法
公开(公告)号：US20110275862A1
公开(公告)日：2011-11-10
申请号：US12889813
申请日：2010-09-24
申请人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
发明人： Victor J. Johnston , Josefina T. Chapman , Radmila Jevtic , Heiko Weiner , Tianshu Pan , R. Jay Warner , Gerald Grusendorf , Nathan Bower , Lincoln M. Sarager
IPC分类号： C07C29/80
CPC分类号： C07C29/149 , C07C29/88 , C07C31/08
摘要： Recovery of ethanol from a crude ethanol product obtained from the hydrogenation of acetic acid. Separation and purification processes of the crude ethanol products are employed to allow recovery of ethanol and remove acetal impurities.
摘要翻译：从乙酸氢化得到的粗乙醇产物中回收乙醇。使用粗乙醇产物的分离和纯化方法以回收乙醇并除去缩醛杂质。

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