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1. 发明授权

US08119552B2 Catalyst composition for hydrocracking and process of mild hydrocracking and ring opening 有权
标题翻译：用于加氢裂化的催化剂组合物和轻度加氢裂化和开环的方法
公开(公告)号：US08119552B2
公开(公告)日：2012-02-21
申请号：US12091706
申请日：2006-10-26
申请人： Götz Burgfels , Stephan Wellach , Josef Schönlinner , Friedrich Schmidt , Volker Kurth , Vebjorn Knut Grande , Jorunn Steinsland Rosvoll , Per Aksel Skjølsvik
发明人： Götz Burgfels , Stephan Wellach , Josef Schönlinner , Friedrich Schmidt , Volker Kurth , Vebjorn Knut Grande , Jorunn Steinsland Rosvoll , Per Aksel Skjølsvik
IPC分类号： C10G47/00
CPC分类号： C10G47/20 , B01J29/166 , B01J29/78 , B01J29/80 , B01J37/0009 , B01J2229/20 , B01J2229/42 , C10G45/64 , C10G65/12 , C10G2300/1059 , C10G2300/1074 , C10G2300/202 , C10G2300/301 , C10G2300/307 , C10G2300/308 , C10G2300/4018 , C10G2400/04
摘要： The present invention relates to a catalyst composition for the reaction of hydrocarbons comprising a zeolite with has a faujasite structure and a fibrous zeolite which comprises essentially non-crossing one-dimensional channels. Further, the catalyst composition comprises in a preferred embodiment a metal component selected from metals of the group VIB and VIII of the periodic table of elements and their compounds. The invention relates further to a process for the synthesis of such a catalyst composition and to a process for hydrocracking hydrocarbon feedstocks by using said catalyst composition.
摘要翻译：本发明涉及包含具有八面沸石结构的沸石和包含基本上非交叉的一维通道的纤维状沸石的烃的反应用催化剂组合物。此外，催化剂组合物在一个优选的实施方案中包括选自元素周期表第ⅥB族和第Ⅷ族金属及其化合物的金属组分。本发明进一步涉及合成这种催化剂组合物的方法和通过使用所述催化剂组合物加氢裂解烃原料的方法。

2. 发明申请

US20090301929A1 Catalyst Composition For Hydrocracking and Process of Mild Hydrocracking and Ring Opening 有权
标题翻译：催化剂组合物用于加氢裂化和轻度加氢裂化和开环过程
公开(公告)号：US20090301929A1
公开(公告)日：2009-12-10
申请号：US12091706
申请日：2006-10-26
申请人： Götz Burgfels , Stephan Wellsch , Josef Schönlinner , Friedrich Schmidt , Volker Kurth , Vebjorn Knut Grande , Jorunn Steinsland Rosvoll , Per Aksel Skjølsvik
发明人： Götz Burgfels , Stephan Wellsch , Josef Schönlinner , Friedrich Schmidt , Volker Kurth , Vebjorn Knut Grande , Jorunn Steinsland Rosvoll , Per Aksel Skjølsvik
IPC分类号： C10G47/00 , B01J29/06 , C10G47/02
CPC分类号： C10G47/20 , B01J29/166 , B01J29/78 , B01J29/80 , B01J37/0009 , B01J2229/20 , B01J2229/42 , C10G45/64 , C10G65/12 , C10G2300/1059 , C10G2300/1074 , C10G2300/202 , C10G2300/301 , C10G2300/307 , C10G2300/308 , C10G2300/4018 , C10G2400/04
摘要： The present invention relates to a catalyst composition for the reaction of hydrocarbons comprising a zeolite with has a faujasite structure and a fibrous zeolite which comprises essentially non-crossing one-dimensional channels. Further, the catalyst composition comprises in a preferred embodiment a metal component selected from metals of the group VIB and VIII of the periodic table of elements and their compounds. The invention relates further to a process for the synthesis of such a catalyst composition and to a process for hydrocracking hydrocarbon feedstocks by using said catalyst composition.
摘要翻译：本发明涉及包含具有八面沸石结构的沸石和包含基本上非交叉的一维通道的纤维状沸石的烃的反应用催化剂组合物。此外，催化剂组合物在一个优选的实施方案中包括选自元素周期表第ⅥB族和第Ⅷ族金属及其化合物的金属组分。本发明进一步涉及合成这种催化剂组合物的方法和通过使用所述催化剂组合物加氢裂解烃原料的方法。

3. 发明授权

US07244409B2 Process for producing synthetic zeolites with MFI structure 有权
标题翻译：用MFI结构生产合成沸石的方法
公开(公告)号：US07244409B2
公开(公告)日：2007-07-17
申请号：US11224841
申请日：2005-09-13
申请人： Götz Burgfels , Josef Schönlinner , Friedrich Schmidt
发明人： Götz Burgfels , Josef Schönlinner , Friedrich Schmidt
IPC分类号： C01B39/38
CPC分类号： C01B39/40 , B01J29/40 , B01J35/002 , B01J35/023 , B01J35/1019 , B01J35/1038 , B01J35/108 , C07C5/2737 , C07C2529/40 , Y02P20/52 , Y10S423/22 , C07C15/08
摘要： A process is described for producing synthetic zeolites useful as catalysts with a MFI structure, a Si/Al atomic ratio from about 8 to 45 to 1 and very small primary crystallites. A Si source, an Al source and an organic template are reacted with one another under hydrothermal conditions. The process is carried out in the presence of seed crystals with an average particle size from roughly 10 to 100 nm, preferably from 20 to 50 nm, prepared from an earlier batch of synthetic zeolites with a MFI structure, without separation from the mother liquor. The process further includes conversion by ion exchange of the zeolites into an H form. Moldings may also be produced by the addition of binders and optionally catalytically active base metal and/or precious metal components before or after the moldings are produced. The zeolites as claimed in the invention are characterized by the combination of the following features: (a) Si/Al atomic ratio 8 to 45:1 (b) Size of the primary crystallites roughly 0.01 to 0.05 microns; (c) Ratio between longest and shortest axis of the primary crystallites: roughly 1.0 to 1.5:1; (d) Ratio between the intensity of the x-ray diffraction line with the highest intensity (Dmax=3.865+/−0.015) and the intensity of the x-ray diffraction lines of ZSM 11-zeolite (Dmax=11.15 angstroms); mordenite (Dmax=9.06 angstroms); α-cristobalite (Dmax=3.345 angstroms); and analcim (Dmax=4.83 angstroms)>500:1.
摘要翻译：描述了用于制备可用作具有MFI结构的催化剂，约8至45比1的Si / Al原子比和非常小的初晶的合成沸石的方法。 Si源，Al源和有机模板在水热条件下彼此反应。该方法在存在从具有MFI结构的较早批次的合成沸石制备而不与母液分离的平均粒度为约10至100nm，优选20至50nm的晶种的情况下进行。该方法还包括通过沸石离子交换成H形式的转化。模制品也可以通过在制造模制品之前或之后添加粘合剂和任选的催化活性的贱金属和/或贵金属组分来生产。本发明所述的沸石的特征在于以下特征的组合：（a）Si / Al原子比为8至45：1（b）初级微晶的尺寸大约为0.01至0.05微米; （c）主晶体的最长和最短轴之间的比率：大约1.0至1.5:1; （d）具有最高强度（D max max = 3.865 +/- 0.015）的x射线衍射线的强度与ZSM 11-沸石的x射线衍射线的强度之比（D max max = 11.15埃）; 丝光沸石（D max max = 9.06埃）; α-方英石（D max max = 3.345埃）; 和Analcim（D max max = 4.83埃）> 500:1。

4. 发明授权

US06951638B1 Process for producing synthetic zeolites with an MFI structure 有权
公开(公告)号：US06951638B1
公开(公告)日：2005-10-04
申请号：US10111651
申请日：2000-10-11
申请人： Götz Burgfels , Josef Schönlinner , Friedrich Schmidt
发明人： Götz Burgfels , Josef Schönlinner , Friedrich Schmidt
IPC分类号： B01J20/18 , B01J20/30 , B01J29/40 , B01J29/44 , B01J35/10 , C01B39/36 , C01B39/40 , C07B61/00 , C07C5/27 , C07C15/04 , C07C15/08
CPC分类号： C01B39/40 , B01J29/40 , B01J35/002 , B01J35/023 , B01J35/1019 , B01J35/1038 , B01J35/108 , C07C5/2737 , C07C2529/40 , Y02P20/52 , Y10S423/22 , C07C15/08
摘要： A process is described for producing synthetic zeolites with a MFI structure, a Si/Al atomic ratio from roughly 8 to 45 and very small primary crystallites, a Si source, an Al source and an organic template being reacted with one another under hydrothermal conditions, the Si/Al atomic ratio being roughly 9 to 50 and the ratio between the longest and shortest axis of the primary crystallites being roughly 1.0 to 1.5:1; the process is characterized in that the reaction is carried out in the presence of seed crystals with an average particle size from roughly 10 to 100 nm, preferably from 20 to 50 nm from an earlier batch without separation from the mother liquor.The zeolites as claimed in the invention which are characterized by the combination of the following features: (a) Si/Al atomic ratio 8 to 45:1 (b) Size of the primary crystallites roughly 0.01 to 0.05 microns; (c) Ratio between longest and shortest axis of the primary crystallites: roughly 1.0 to 1.5:1; (d) Ratio between the intensity of the x-ray diffraction line with the highest intensity (Dmax=3.865+/−0.015) and the intensity of the x-ray diffraction lines of ZSM 11-zeolite (Dmax=11.15 angstroms); mordenite (Dmax=9.06 angstroms); α-cristobalite (Dmax=3.345 angstroms); and analcim (Dmax=4.83 angstroms)>500:1. One development of the process as claimed in the invention is characterized in that the reaction product is converted by ion exchange into the H form, moldings produced with the addition of binders and optionally catalytically active base metal and/or precious metal components are added before or after the moldings are produced.The synthetic zeolites can be used as catalysts, especially as catalysts for acid-catalyzed reactions, oxidation, reduction and adsorption.

5. 发明授权

US07229941B2 Catalysts based on crystalline aluminosilicate 有权
标题翻译：基于结晶硅铝酸盐的催化剂
公开(公告)号：US07229941B2
公开(公告)日：2007-06-12
申请号：US10725313
申请日：2003-12-01
申请人： Götz Burgfels , Karl Kochloefl , Jürgen Ladebeck , Michael Schneider , Friedrich Schmidt , Hans-Jürgen Wernicke , Josef Schönlinner
发明人： Götz Burgfels , Karl Kochloefl , Jürgen Ladebeck , Michael Schneider , Friedrich Schmidt , Hans-Jürgen Wernicke , Josef Schönlinner
IPC分类号： B01J29/06
CPC分类号： B01J29/40 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/1066 , B01J35/108 , B01J37/0009 , C10G3/49 , C10G2400/20
摘要： A catalyst is described based on crystalline aluminosilicates of the pentasil type, characterized in that it is constructed from primary crystallites with an average diameter of at least 0.01 μm and less than 0.1 μm, that are combined to at least 20% to agglomerates of 5 to 500 μm, in which the primary crystallites or agglomerates are bonded together by finely divided aluminum oxide, that its BET surface is 300 to 600 m2/g and its pore volume (determined according to mercury porosimetry) is 0.3 to 0.8 cm3/g, that it is present in H form and that the amount of finely divided aluminum oxide binder is 10 to 40 wt. %, referred to the total weight of the aluminosilicate, in which the finely divided aluminum oxide binder is used in the reaction charge as peptizable aluminum oxide hydrate, sodium aluminate being used as aluminum and alkali source, and primary synthesis of the crystalline aluminosilicate occurs without addition of acid. A method is also described for production of such a catalyst and its preferred applications.
摘要翻译：基于pentasil类型的结晶硅铝酸盐描述催化剂，其特征在于其由平均直径为至少0.01μm和小于0.1μm的初级微晶构成，其与至少20％的附聚物组合为5至 500微米，其中初级微晶或团聚体通过细碎的氧化铝结合在一起，其BET表面积为300-600m 2 / g，其孔体积（根据水银孔率法测定）为 0.3〜0.8cm 3 / g，以H形式存在，细分的氧化铝粘合剂的量为10〜40wt。％，以铝硅酸盐的总重量计，其中细分的氧化铝粘合剂用作反应电荷，作为可溶解的氧化铝水合物，铝酸钠用作铝和碱源，并且结晶硅铝酸盐的初步合成发生在没有加酸。还描述了用于生产这种催化剂及其优选应用的方法。

6. 发明申请

US20130266507A1 MECHANOCHEMICAL PRODUCTION OF ZEOLITES 审中-公开
标题翻译： ZEOLITES的机械化学生产
公开(公告)号：US20130266507A1
公开(公告)日：2013-10-10
申请号：US13988598
申请日：2011-11-28
申请人： Jürgen Ladebeck , Jürgen Koy , Stephen Wellach , Josef Schönlinner , Götz Burgfels
发明人： Jürgen Ladebeck , Jürgen Koy , Stephen Wellach , Josef Schönlinner , Götz Burgfels
IPC分类号： B01J29/70 , B01J29/40
CPC分类号： B01J29/7007 , B01J29/40 , B01J37/10 , C01B39/02 , C01B39/04 , C01B39/40 , C01B39/48
摘要： The subject of the invention is a method for the synthesis of zeolites, comprising the following steps: a) providing a silicon source; b) providing an aluminium source; c) optionally providing at least one template; d) mixing the silicon source, aluminium source and optional template in order to produce a synthesis gel; e) grinding the synthesis gel; f) treating the ground synthesis gel under hydrothermal conditions in order to produce crystalline zeolite, as well as zeolites that can be obtained according to this method. The products obtained according to the method can be used as catalysts or catalyst supports.
摘要翻译：本发明的主题是合成沸石的方法，包括以下步骤：a）提供硅源; b）提供铝源; c）任选地提供至少一个模板; d）将硅源，铝源和任选的模板混合以产生合成凝胶; e）研磨合成凝胶; f）在水热条件下处理研磨的合成凝胶，以产生结晶沸石，以及根据该方法得到的沸石。根据该方法获得的产物可用作催化剂或催化剂载体。

7. 发明申请

US20130053609A1 CATALYST BASED ON ZEOLITE FOR PRODUCING OLEFINS AND FOR OLIGOMERIZING OLEFINS 有权
标题翻译：基于沸石生产烯烃和低聚烯烃的催化剂
公开(公告)号：US20130053609A1
公开(公告)日：2013-02-28
申请号：US13575054
申请日：2011-01-26
申请人： Götz Burgfels , Stefan Klingelhöfer , Lay Hwa Ong , Roberta Olindo , Johannes A. Lercher , Friedrich Schmidt
发明人： Götz Burgfels , Stefan Klingelhöfer , Lay Hwa Ong , Roberta Olindo , Johannes A. Lercher , Friedrich Schmidt
IPC分类号： B01J29/06 , C07C2/12 , C07C1/22 , B01J29/70
CPC分类号： B01J29/40 , B01J29/06 , B01J35/1019 , B01J2229/42 , C07C1/20 , C07C2/12 , C07C11/02 , C07C2529/40 , C07C2529/70 , C10G3/49 , C10G50/00 , C10G2400/20 , Y02P30/20
摘要： The invention relates to a novel catalyst based on zeolite, the production of that catalyst, and the use of the catalyst in a method for producing lower olefins from oxygenates and for oligomerizing olefins. The novel catalyst has a SiO2/Al2O3 weight ratio of 2 to 9, a BET surface of 250 to 500 m2/g, and an Na content under 200 ppm. The catalyst includes a crystalline alumosilicate zeolite and a binder. The catalyst is characterized in that the ratio of the peak heights of its IR absorption bands v=3610 cm−1±20 cm−1/v=3680 cm−1±20 cm−1 is greater than 1.8.
摘要翻译：本发明涉及一种基于沸石的新型催化剂，该催化剂的生产，以及该催化剂在由含氧化合物制备低级烯烃和烯烃低聚物的方法中的用途。新型催化剂的SiO2 / Al2O3重量比为2〜9，BET表面积为250〜500m2 / g，Na含量为200ppm以下。催化剂包括结晶铝硅酸盐沸石和粘合剂。催化剂的特征在于其IR吸收带v = 3610cm-1±20cm-1 / v = 3680cm -1±20cm -1的峰高比大于1.8。

8. 发明授权

US09174204B2 Catalyst based on zeolite for producing olefins and for oligomerizing olefins 有权
标题翻译：基于用于制备烯烃和低聚烯烃的沸石的催化剂
公开(公告)号：US09174204B2
公开(公告)日：2015-11-03
申请号：US13575054
申请日：2011-01-26
申请人： Götz Burgfels , Stefan Klingelhöfer , Lay Hwa Ong , Roberta Olindo , Johannes A. Lercher , Friedrich Schmidt
发明人： Götz Burgfels , Stefan Klingelhöfer , Lay Hwa Ong , Roberta Olindo , Johannes A. Lercher , Friedrich Schmidt
IPC分类号： B01J29/06 , B01J29/40 , C07C11/02 , B01J35/10 , C07C1/20 , C07C2/12 , C10G50/00 , C10G3/00
CPC分类号： B01J29/40 , B01J29/06 , B01J35/1019 , B01J2229/42 , C07C1/20 , C07C2/12 , C07C11/02 , C07C2529/40 , C07C2529/70 , C10G3/49 , C10G50/00 , C10G2400/20 , Y02P30/20
摘要： The invention relates to a novel catalyst based on zeolite, the production of that catalyst, and the use of the catalyst in a method for producing lower olefins from oxygenates and for oligomerizing olefins. The novel catalyst has a SiO2/Al2O3 weight ratio of 2 to 9, a BET surface of 250 to 500 m2/g, and an Na content under 200 ppm. The catalyst includes a crystalline alumosilicate zeolite and a binder. The catalyst is characterized in that the ratio of the peak heights of its IR absorption bands v=3610 cm−1±20 cm−1/v=3680 cm−1±20 cm−1 is greater than 1.8.
摘要翻译：本发明涉及一种基于沸石的新型催化剂，该催化剂的生产，以及该催化剂在由含氧化合物制备低级烯烃和烯烃低聚物的方法中的用途。新型催化剂的SiO2 / Al2O3重量比为2〜9，BET表面积为250〜500m2 / g，Na含量为200ppm以下。催化剂包括结晶铝硅酸盐沸石和粘合剂。催化剂的特征在于其IR吸收带v = 3610cm-1±20cm-1 / v = 3680cm -1±20cm -1的峰高比大于1.8。

9. 发明授权

US09511361B2 Spherical zeolitic catalyst for converting methanol into olefins 有权
标题翻译：用于将甲醇转化为烯烃的球形沸石催化剂
公开(公告)号：US09511361B2
公开(公告)日：2016-12-06
申请号：US13509087
申请日：2010-11-16
申请人： Götz Burgfels , Manfred D. Frauenrath , Nadine Fromm , Angelika Glienke , Martin Rothämel , Sven Pohl
发明人： Götz Burgfels , Manfred D. Frauenrath , Nadine Fromm , Angelika Glienke , Martin Rothämel , Sven Pohl
IPC分类号： C07C1/20 , B01J29/06 , B01J37/00 , B01J29/40 , B01J35/02 , B01J35/08 , B01J35/10
CPC分类号： B01J37/0018 , B01J29/40 , B01J35/023 , B01J35/08 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/109 , B01J37/0009 , B01J37/0063 , B01J37/0072 , B01J2229/42 , C07C1/20 , C07C2529/06 , C07C2529/40 , Y02P20/52 , C07C11/02
摘要： A catalyst containing a pentasil-type alumosilicates and a binder, in the form of spheres having an average diameter between 0.3 and 7 mm, wherein the BET surface area of the catalyst ranges from 300 to 600 m2/g. Also disclosed is a method for producing the catalyst, wherein primary crystallites of the aluminosilicate having an average diameter of at least 0.01 μm and less than 0.1 μm are mixed with the binder, shaped into spheres having an average diameter between 0.3 and 7 mm, and subsequently calcined. Also disclosed is the use of the catalyst for converting methanol into olefins, in particular propylene. Also disclosed is a method for producing olefins from methanol, in which a feed gas is fed across the catalyst.
摘要翻译：含有平均粒径为0.3〜7mm的球形形式的pentasil型铝硅酸盐和粘合剂的催化剂，其中催化剂的BET表面积为300〜600m2 / g。还公开了一种制备催化剂的方法，其中平均直径为至少0.01μm且小于0.1μm的铝硅酸盐的初级微晶与粘合剂混合，成型为平均直径在0.3和7mm之间的球体，以及随后煅烧。还公开了使用催化剂将甲醇转化为烯烃，特别是丙烯。还公开了一种从甲醇制备烯烃的方法，其中进料气体通过催化剂进料。

10. 发明申请

US20120253090A1 SPHERICAL ZEOLITIC CATALYST FOR CONVERTING METHANOL INTO OLEFINS 有权
标题翻译：用于将甲醇转化成烯烃的球形活化催化剂
公开(公告)号：US20120253090A1
公开(公告)日：2012-10-04
申请号：US13509087
申请日：2010-11-16
申请人： Götz Burgfels , Manfred D. Frauenrath , Nadine Fromm , Angelika Glienke , Martin Rothämel , Sven Pohl
发明人： Götz Burgfels , Manfred D. Frauenrath , Nadine Fromm , Angelika Glienke , Martin Rothämel , Sven Pohl
IPC分类号： B01J29/40 , C07C1/20
CPC分类号： B01J37/0018 , B01J29/40 , B01J35/023 , B01J35/08 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/109 , B01J37/0009 , B01J37/0063 , B01J37/0072 , B01J2229/42 , C07C1/20 , C07C2529/06 , C07C2529/40 , Y02P20/52 , C07C11/02
摘要： A catalyst containing a pentasil-type alumosilicates and a binder, in the form of spheres having an average diameter between 0.3 and 7 mm, wherein the BET surface area of the catalyst ranges from 300 to 600 m2/g. Also disclosed is a method for producing the catalyst, wherein primary crystallites of the aluminosilicate having an average diameter of at least 0.01 μm and less than 0.1 μm are mixed with the binder, shaped into spheres having an average diameter between 0.3 and 7 mm, and subsequently calcined. Also disclosed is the use of the catalyst for converting methanol into olefins, in particular propylene. Also disclosed is a method for producing olefins from methanol, in which a feed gas is fed across the catalyst.
摘要翻译：含有平均粒径为0.3〜7mm的球形形式的pentasil型铝硅酸盐和粘合剂的催化剂，其中催化剂的BET表面积为300〜600m2 / g。还公开了一种制备催化剂的方法，其中平均直径为至少0.01μm且小于0.1μm的铝硅酸盐的初级微晶与粘合剂混合，成型为平均直径在0.3和7mm之间的球体，以及随后煅烧。还公开了使用催化剂将甲醇转化为烯烃，特别是丙烯。还公开了一种从甲醇制备烯烃的方法，其中进料气体通过催化剂进料。

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