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    • 5. 发明授权
    • Method for preparing hydroxygallium phthalocyanine crystals and
electrophotographic photoreceptor using the crystals
    • 使用该晶体制备羟基镓酞菁晶体和电子照相感光体的方法
    • US5545733A
    • 1996-08-13
    • US288079
    • 1994-08-10
    • Katsumi DaimonKatsumi NukadaYasuo SakaguchiRyosaku Igarashi
    • Katsumi DaimonKatsumi NukadaYasuo SakaguchiRyosaku Igarashi
    • C09B67/12C09B67/50G03G5/06C09B47/04
    • C09B67/0016C09B67/0026
    • A method for preparing hydroxygallium phthalocyanine crystals wherein hydroxygallium phthalocyanine crystals having distinct diffraction peaks at 7.0.degree., 13.4.degree., 16.6.degree., 26.0.degree. and 26.7.degree. of the Bragg angle (2.theta..+-.0.2.degree.) with respect to CuK.alpha. characteristics X-ray in the X-ray diffraction spectrum are crystal-transferred by solvent treatment. The crystals after crystal-transfer have distinct diffraction peaks at (i) 7.7.degree., 16.5.degree., 25.1.degree. and 26.6.degree., (ii) 7.9.degree., 16.5.degree., 24.4.degree. and 27.6.degree., (iii) 7.0.degree., 7.5.degree., 10.5.degree., 11.7.degree., 12.7.degree., 17.3.degree., 18.1.degree., 24.5.degree., 26.2.degree. and 27.1, (iv) 7.5.degree., 9.9.degree., 12.5.degree., 16.3.degree., 18.6.degree., 25.1.degree. and 28.8.degree. or (v) 6.8.degree., 12.8.degree., 15.8.degree. and 26.0.degree. of the Bragg angle (2.theta..+-.0.2.degree. C.) with respect to CuK.alpha. characteristics X-ray in the X-ray diffraction spectrum. An electrophotographic photoreceptor having a light-sensitive layer on a electroconductive substrate wherein the light-sensitive layer contains at least one of the hydroxygallium phthalocyanine crystals.
    • 一种制备羟基镓酞菁晶体的方法,其中具有相对于CuKα特征X的布拉格角(2θ+/- 0.2°)的7.0°,13.4°,16.6°,26.0°和26.7°处具有不同衍射峰的羟基镓酞菁晶体 X-射线衍射光谱中的-ray通过溶剂处理进行结晶转移。 结晶转移后的晶体在(i)7.7°,16.5°,25.1°和26.6°,(ii)7.9°,16.5°,24.4°和27.6°,(iii)7.0°,7.5°, 10.5°,11.7°,12.7°,17.3°,18.1°,24.5°,26.2°和27.1°,(iv)7.5°,9.9°,12.5°,16.3°,18.6°,25.1°和28.8°或(v) 相对于X射线衍射光谱中的CuKα特征X射线,布拉格角(2θ+/- 0.2℃)的6.8°,12.8°,15.8°和26.0°。 在导电性基体上具有感光层的电子照相感光体,其中感光层含有至少一种羟基镓酞菁晶体。