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1. 发明授权

US4291147A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4291147A
公开(公告)日：1981-09-22
申请号：US137748
申请日：1980-04-07
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

2. 发明授权

US4363710A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4363710A
公开(公告)日：1982-12-14
申请号：US316797
申请日：1981-10-30
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00 , C25D13/06
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formlula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

3. 发明授权

US4340714A Preparation of curable polyadducts, containing basic nitrogen groups, and use of the products 失效
标题翻译：制备含碱性氮基的可固化聚合物，以及产品的使用
公开(公告)号：US4340714A
公开(公告)日：1982-07-20
申请号：US266363
申请日：1981-05-22
申请人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
发明人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
IPC分类号： C08G59/00 , C08G14/06 , C08G59/14 , C08G59/64 , C08L63/00 , C09D5/44 , C09D163/00 , C08G59/28
CPC分类号： C08L63/00 , C08G14/06 , C08G59/64 , C09D163/00 , C09D5/4419
摘要： A process for the preparation of curable polyadducts, possessing basic nitrogen groups, wherein (A) monophenols and/or polyphenols, which contain groups of the general formula (I): ##STR1## where R.sup.1 and R.sup.2 are identical or different and each is hydrogen or methyl are reacted with (B) amines having one or more primary and/or secondary amino groups, and the adduct formed is reacted with (C) epoxide compounds having from 1 to 4 epoxide groups per molecule and having a molecular weight of at most 2,500, the ratio of the phenolic hydroxyl groups of (A) to epoxide groups of (C) being from 1:0.5 to 1:2 and the amine (B) being employed in such amount that the resulting polyadduct of (A), (B) and (C) contains from 0.1 to 5% by weight of basic nitrogen, and the use of the products, after protonation with an acid, as binders for the production of coatings, especially for the cathodic electrocoating of metal articles.
摘要翻译：一种制备具有碱性氮基团的可固化聚合物的方法，其中（A）单酚和/或多酚，其含有通式（I）的基团：其中R 1和R 2相同或不同，各自为氢或甲基与（B）具有一个或多个伯和/或仲氨基的胺反应，并且所形成的加合物与（C）每分子具有1至4个环氧基的环氧化物化合物反应，分子量至多为（A）的酚羟基与（C）的环氧基的比例为1:0.5至1:2，胺（B）的使用量使得所得的（A），（ B）和（C）含有0.1至5重量％的碱性氮，并且在用酸质子化后使用该产物作为用于制备涂料的粘合剂，特别是用于金属制品的阴极电泳涂层。

4. 发明授权

US4315840A Preparation of cathodic electrocoating binders 失效
标题翻译：阴极电泳涂料的制备
公开(公告)号：US4315840A
公开(公告)日：1982-02-16
申请号：US85965
申请日：1979-10-18
申请人： Fritz E. Kempter , Eberhard Schupp , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Erich Gulbins
IPC分类号： C08G18/00 , C08G18/08 , C08G18/65 , C08G18/66 , C08G18/80 , C09D5/44 , C09D175/08 , C08G18/48 , C08J3/04 , C08L91/00
CPC分类号： C08G18/0814 , C08G18/8061 , C09D5/4465 , Y10S524/901
摘要： A process for the preparation of self-crosslinking, cathodic electrocoating binders by reacting polyether-polyols, which may or may not contain thio groups, with semi-blocked diisocyanates or partially blocked polyisocyanates, wherein the reaction products (A), containing blocked isocyanate groups, are reacted with a polyamine (B), some of whose amino groups may or may not be in the form of ketimine groups, in such a way that one or more amino groups of the polyamine (B) form a urea group with a blocked isocyanate group of the reaction product (A), and the self-cross-linking reaction product of (A) and (B) is converted into a water-dilutable form in the conventional manner by protonization with an acid.The coating binders prepared according to the invention may be used for cathodic electrocoating of metal articles.
摘要翻译：一种制备自交联阴极电泳涂料粘合剂的方法，该方法是将可能含有或不含有硫基的聚醚多元醇与半封端二异氰酸酯或部分封闭的多异氰酸酯反应，其中含有封端异氰酸酯基团的反应产物（A）与多胺（B）反应，其一些氨基可以是或可以不是酮亚胺基的形式，使得多胺（B）的一个或多个氨基形成具有封闭的脲基团反应产物（A）的异氰酸酯基和（A）和（B）的自交联反应产物以常规方式通过用酸质子化转化成水可稀释形式。根据本发明制备的涂料粘合剂可用于金属制品的阴极电泳涂覆。

5. 发明授权

US4310645A Polyadducts of ammonia and epoxide compounds, processes for their modification, and their use 失效
标题翻译：氨和环氧化合物的加合物，其改性方法及其用途
公开(公告)号：US4310645A
公开(公告)日：1982-01-12
申请号：US213174
申请日：1980-12-04
申请人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
发明人： Fritz E. Kempter , Eberhard Schupp , Hans-Uwe Schenck , Erich Gulbins
IPC分类号： C08G12/00 , C08G12/02 , C08G12/46 , C08G59/00 , C08G59/14 , C08G59/40 , C08G65/26 , C08K5/29 , C09D5/44 , C09D163/00
CPC分类号： C08G12/46 , C08G12/00 , C08G12/02 , C08G59/1405 , C08G59/4014 , C08G65/2624 , C09D5/4438 , Y10S524/901 , Y10T428/2933
摘要： Polyadducts, free from epoxide groups, are obtained from ammonia and epoxide compounds by reacting 1 mole of ammonia with from 1.2 to 2.0 equivalents of epoxide, so that if diepoxide compounds are used products of the general formula (I) ##STR1## are obtained, while if triepoxides and/or tetraepoxide compounds are used, by themselves, or together with diepoxide compounds, products of the general formula II ##STR2## are produced; in these formulae, the E.sup.1 's are identical or different hydroxyl-containing divalent radicals and the E.sup.2 's are identical or different hydroxyl-containing trivalent or tetravalent radicals, resulting from the opening of the oxirane rings of epoxide compounds containing two, three or four epoxide groups in the molecule, n.sup.1, n.sup.3 and n.sup.5 are from 0 to 3, n.sup.2 and n.sup.4 are from 1 to 3 and X is 0 or 1, and one or more of the divalent radicals E.sup.1 in the general formula (II) may or may not be replaced by polyvalent radicals E.sup.2.The novel polyadducts can be modified by reaction with aldehydes, ketones, monoepoxide compounds, carboxylic acids, carboxylic acid esters or isocyanates, or by protonation with an acid, and may be used, for example, for the cathodic electrocoating of metallic articles.
摘要翻译：通过使1摩尔氨与1.2-2.0当量的环氧化物反应，从氨和环氧化合物得到不含环氧基的多元加成物，因此如果使用二环氧化合物，则得到通式（I）的产物而如果三环氧化物和/或四环氧化合物本身或与二环氧化合物一起使用，则制备通式II的产物（II）; 在这些式中，E1是相同或不同的含羟基的二价基团，并且E2是相同或不同的含羟基的三价或四价基团，其由环氧乙烷环的环氧化物环开放，所述环氧化物包含两个，三个或四个环氧基团分子n1，n3和n5为0〜3，n2和n4为1〜3，X为0或1，通式（II）中的一个或多个二价基团E1可以是也可以不是由多价基团E2代替。可以通过与醛，酮，单环化合物，羧酸，羧酸酯或异氰酸酯的反应或通过用酸质子化来改变新的多加合物，并且可以用于例如金属制品的阴极电泳涂层。

6. 发明授权

US4336116A Polyadducts containing unsaturated amide groups and their use in coatings 失效
标题翻译：含有不饱和酰胺基团的多元加成物及其在涂料中的应用
公开(公告)号：US4336116A
公开(公告)日：1982-06-22
申请号：US198226
申请日：1980-10-17
申请人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
发明人： Eberhard Schupp , Fritz E. Kempter , Erich Gulbins
IPC分类号： C08G59/00 , C08G59/14 , C08G59/56 , C08G59/62 , C09D5/44 , C09D163/00 , C08G59/28 , C08J3/28
CPC分类号： C08G59/56 , C08G59/621 , C09D163/00 , C09D5/4434 , Y10S524/901
摘要： The invention concerns polyadducts and their use.The polyadducts, possessing nitrogen-basic groups, have a mean molecular weight of from 500 to 10,000 and contain groups, attached to aromatic rings, of the general formula (I) ##STR1## where R.sup.1 and R.sup.2 are identical or different and each is hydrogen or methyl.In particular, these polyadducts are used, after protonizing with an acid, as binders for the cathodic electrocoating of metal articles.
摘要翻译：本发明涉及多加合物及其用途。具有氮 - 碱性基团的多元加成物的平均分子量为500〜10,000，并且含有通式（I）的芳环上的基团，其中R 1和R 2相同或不同，各自为氢或甲基。特别地，这些聚加成物在用酸质子化之后用作金属制品的阴极电涂层的粘合剂。

7. 发明授权

US4137213A Pigment formulations for use in surface-coating binders 失效
标题翻译：用于表面涂层粘合剂的颜料配方
公开(公告)号：US4137213A
公开(公告)日：1979-01-30
申请号：US764196
申请日：1977-01-31
申请人： Fritz E. Kempter , Erich Gulbins , Armin Haag , Ruprecht Kroker
发明人： Fritz E. Kempter , Erich Gulbins , Armin Haag , Ruprecht Kroker
IPC分类号： C09D5/44 , C09C3/00 , C09C3/10 , C09D7/45 , C09D17/00 , C08K9/04
CPC分类号： C09D17/002 , C09D7/02
摘要： Pigment formulations and their use.The formulations contain pigments, organic solvents and from 10 to 80% by weight of a wetting agent consisting of a non-ionic organic compound which has a viscosity of from 500 to 10,000 mPa.s and has been produced by reacting an alkylated amide/formaldehyde reaction product and an epoxy resin, which may or may not be modified, in a weight ratio of from 9:1 to 1:9. They are used as additives in surface-coating binders, especially in cationic electrocoating finishes.
摘要翻译：颜料配方及其用途。

8. 发明授权

US4134932A Surface-coating binders for cathodic electrocoating 失效
标题翻译：用于阴极电泳的表面涂层粘合剂
公开(公告)号：US4134932A
公开(公告)日：1979-01-16
申请号：US884909
申请日：1978-03-09
申请人： Fritz E. Kempter , Heinrich Hartmann , Erich Gulbins
发明人： Fritz E. Kempter , Heinrich Hartmann , Erich Gulbins
IPC分类号： C08G18/00 , C08G59/00 , C08G59/62 , C08L63/00 , C08L75/00 , C09D5/44 , C09D175/00
CPC分类号： C09D5/4419 , C08G59/623 , C08L63/00
摘要： Surface-coating binders for cathodic electrocoating which comprise a protonized heat-curable reaction product (A), substantially free from epoxide groups, of(a) one or more Mannich bases, prepared from(a.sub.1) one or more polyhydric condensed phenols which may or may not contain ether groups.(a.sub.2) one or more secondary amines which contain one or more hydroxyalkyl groups, with or without one or more secondary amines which do not contain such groups, and(a.sub.3) formaldehyde or a formaldehyde donor, with(b) one or more epoxy resins,Which binder also contains from 1 to 40% by weight, based on the total of (A) + (B), of a water-insoluble non-ionic resin (B), free from epoxide groups and containing urethane groups, which resin has been obtained by reacting a partially blocked diisocyanate or higher polyisocyanate with a reaction product of a polyepoxide and one or more low molecular weight compounds containing SH and/or OH groups.These surface-coating binders are especially used for the cathodic electrocoating of metal articles.
摘要翻译：包含基本上不含环氧基团的质子化热固化反应产物（A）的（A）一种或多种曼尼希碱的质子化可热固化反应产物（A）的表面涂层粘合剂，其由（A1）一种或多种多元稠合的酚制成，其可以是可能不包含以下组。

9. 发明授权

US4260697A Surface-coating binders 失效
标题翻译：表面涂层粘合剂
公开(公告)号：US4260697A
公开(公告)日：1981-04-07
申请号：US932466
申请日：1978-08-10
申请人： Fritz E. Kempter , Heinrich Hartmann , Erich Gulbins
发明人： Fritz E. Kempter , Heinrich Hartmann , Erich Gulbins
IPC分类号： B29C37/00 , B29C45/00 , C08G18/00 , C08G18/54 , C08G59/00 , C08G59/40 , C08L63/00 , C09D5/44 , C09D163/00 , C09D175/00
CPC分类号： C09D5/4419 , C08G59/4028 , C09D163/00
摘要： Surface-coating binders based on a reaction product of Mannich bases, obtained from polyhydric phenols, secondary amines and formaldehyde, with epoxy resins. The Mannich bases and/or the epoxy resins carry hydroxyl groups, bonded to aliphatic structures, which have been converted to urethane groups by reaction with partially blocked polyisocyanates. When protonized and diluted with water, the surface-coating binders may be used as cationic electrocoatings.
摘要翻译：基于由多元酚，仲胺和甲醛获得的曼尼希碱的反应产物与环氧树脂的表面涂层粘合剂。曼尼希碱和/或环氧树脂携带羟基，与脂肪族结构键合，其通过与部分封端的多异氰酸酯反应而转化为氨基甲酸酯基团。当质子化并用水稀释时，表面涂层粘合剂可以用作阳离子电涂层。

10. 发明授权

US4376849A Polyadduct/polycondensate containing basic nitrogen groups, its preparation and its use 失效
标题翻译：含有碱性氮基团的多元/缩聚物，其制备及其用途
公开(公告)号：US4376849A
公开(公告)日：1983-03-15
申请号：US281891
申请日：1981-07-09
申请人： Fritz E. Kempter , Eberhard Schupp
发明人： Fritz E. Kempter , Eberhard Schupp
IPC分类号： C08C19/36 , C08G14/06 , C08G14/14 , C08G59/40 , C08G59/62 , C09D5/44 , C09D163/00 , C08G8/30 , C08L63/00 , C08L63/10
CPC分类号： C09D5/4488 , C08C19/36 , C08G14/06 , C08G14/14 , C08G59/4042 , C08G59/623 , C09D163/00 , C09D5/4403
摘要： A polyadduct/polycondensate which is water-dilutable when protonated with an acid, and which contains basic nitrogen groups, the groups being of the general formula (I) ##STR1## and/or of the general formula (II) ##STR2## as well as of the formula (III) ##STR3## where R.sup.1 and R.sup.2 are hydrogen or methyl, R.sup.3 and R.sup.4 are hydrogen, alkyl or a radical bonded to a phenol or phenolether, R.sup.5 and R.sup.6 are alkyl, hydroxyalkyl or alkoxyalkyl or are linked to one another to form a 5-membered or 6-membered ring, R.sup.7 is a polydienyl radical, n.sup.1 = from 0.5 to 3 and n.sup.2 = from 0.05 to 1.0, and its method of preparation.The polyadduct/polycondensate can be used, for example, as a surface-coating binder for the cathodic electrocoating of metal articles.
摘要翻译：当用酸质子化并且含有碱性氮基团时可水稀释的多元加聚物/缩聚物，通式（I）和/或通式（II）的基团

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