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1. 发明授权

US10227238B2 Production and use of polysilicate particulate materials 有权
公开(公告)号：US10227238B2
公开(公告)日：2019-03-12
申请号：US11397134
申请日：2006-04-04
申请人： Francois Batllo , Brian T. Holland , John M. Krasniewski , Kim M. Long , Michael A. Romba , Sascha Welz , David P. Workman
发明人： Francois Batllo , Brian T. Holland , John M. Krasniewski , Kim M. Long , Michael A. Romba , Sascha Welz , David P. Workman
IPC分类号： B01J21/12 , B01J35/10 , B01J37/03 , C09C1/30 , C01B33/18 , C01B33/26 , D21H17/67 , C01B33/143 , C01B33/146 , B82Y30/00 , B41M5/52 , A23L2/80 , D21H17/68 , D21H19/38 , D21H19/40 , D21H21/52
摘要： A method of preparing a particulate material comprising the steps of adding silicic acid solution, optionally doped with aluminum, optionally added to a slurry of pre-existing nanoparticles at a neutral to slightly acidic pH of no more than seven, and at a temperature of about 20° to 30° C. This yields a polysilicate particulate dispersion. Then, the pH of the dispersion is raised to greater than seven, to stabilize/reinforce particles of the particulate dispersion. Optionally, the particles may be dried, and have increased porosity and surface area.

2. 发明申请

US20100068519A1 SILICEOUS MATERIALS HAVING TUNABLE POROSITY AND SURFACE MORPHOLOGY AND METHODS OF SYNTHESIZING SAME 有权
标题翻译：具有可调节孔隙度和表面形态的硅质材料及其合成方法
公开(公告)号：US20100068519A1
公开(公告)日：2010-03-18
申请号：US12209790
申请日：2008-09-12
申请人： Brian T. Holland , Sascha Welz
发明人： Brian T. Holland , Sascha Welz
IPC分类号： C01B33/00 , B32B5/18 , B32B5/16
CPC分类号： C01B33/126 , C01B33/193 , C01P2006/12 , C01P2006/14 , C01P2006/16 , Y10T428/2982 , Y10T428/2991
摘要： Non-spherical siliceous particles having a plurality of porous branches are disclosed and claimed. The porous branches are randomly oriented and elongated, ring-like, and/or aggregated. An additive introduced during synthesis of the particles modifies pore volume and morphology. The tunability of the pore volume includes an inner diameter ranging from about 2 Å to about 50,000 Å. Synthesizing the particles includes mixing under constant or intermittent stirring in a reaction vessel an aqueous silicic acid solution with an acidic heel solution to form a mixture. The stirring may optionally be performed at a variable speed. An additive is introduced into the mixture at a controlled rate, wherein the additive imposes a pH change from a lower pH to a higher pH to the mixture to induce siliceous particle precipitation. Optionally, a metal dopand may be introduced into the particles and/or at least a portion of an outer surface located outside of the pores and/or an inner surface located inside of the pores may be modified.
摘要翻译：公开并要求保护具有多个多孔分支的非球形硅质颗粒。多孔分支是随机取向的并且是细长的，环状的和/或聚集的。在合成颗粒期间引入的添加剂改变孔体积和形态。孔体积的可调性包括范围从约2到约50,000的内径。合成颗粒包括在反应容器中在恒定或间歇搅拌下混合含水硅酸溶液与酸性鞋底溶液以形成混合物。可以可选地以可变速度进行搅拌。将添加剂以受控的速率引入混合物中，其中添加剂将pH从较低的pH升高到较高的pH至混合物以诱导硅质颗粒沉淀。任选地，可以将金属掺杂物引入颗粒中，和/或位于孔外部的外表面的至少一部分和/或位于孔内部的内表面可以被修饰。

3. 发明授权

US08790608B2 Siliceous materials having tunable porosity and surface morphology and methods of synthesizing same 有权
标题翻译：具有可调孔性和表面形态的硅质材料及其合成方法
公开(公告)号：US08790608B2
公开(公告)日：2014-07-29
申请号：US12209790
申请日：2008-09-12
申请人： Brian T. Holland , Sascha Welz
发明人： Brian T. Holland , Sascha Welz
IPC分类号： C01B33/00 , C01B33/12
CPC分类号： C01B33/126 , C01B33/193 , C01P2006/12 , C01P2006/14 , C01P2006/16 , Y10T428/2982 , Y10T428/2991
摘要： Non-spherical siliceous particles having a plurality of porous branches are disclosed and claimed. The porous branches are randomly oriented and elongated, ring-like, and/or aggregated. An additive introduced during synthesis of the particles modifies pore volume and morphology. The tunability of the pore volume includes an inner diameter ranging from about 2 Å to about 50,000 Å. Synthesizing the particles includes mixing under constant or intermittent stirring in a reaction vessel an aqueous silicic acid solution with an acidic heel solution to form a mixture. The stirring may optionally be performed at a variable speed. An additive is introduced into the mixture at a controlled rate, wherein the additive imposes a pH change from a lower pH to a higher pH to the mixture to induce siliceous particle precipitation. Optionally, a metal dopand may be introduced into the particles and/or at least a portion of an outer surface located outside of the pores and/or an inner surface located inside of the pores may be modified.
摘要翻译：公开并要求保护具有多个多孔分支的非球形硅质颗粒。多孔分支是随机取向的并且是细长的，环状的和/或聚集的。在合成颗粒期间引入的添加剂改变孔体积和形态。孔体积的可调性包括范围从约2到约50,000的内径。合成颗粒包括在反应容器中在恒定或间歇搅拌下混合含水硅酸溶液与酸性鞋底溶液以形成混合物。可以可选地以可变速度进行搅拌。将添加剂以受控的速率引入混合物中，其中添加剂将pH从较低的pH升高到较高的pH至混合物以诱导硅质颗粒沉淀。任选地，可以将金属掺杂物引入颗粒中，和/或位于孔外部的外表面的至少一部分和/或位于孔内部的内表面可以被修饰。

4. 发明申请

US20090220446A1 METHOD FOR TREATING HAIR 审中-公开
标题翻译：治疗头发的方法
公开(公告)号：US20090220446A1
公开(公告)日：2009-09-03
申请号：US12041081
申请日：2008-03-03
申请人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Welz , Xiaojin Li
发明人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Welz , Xiaojin Li
IPC分类号： A61K8/72 , A61Q5/00
CPC分类号： A61K8/817 , A61K8/8147 , A61Q5/12
摘要： A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts.
摘要翻译：公开了一种处理一个或多个毛发轴的方法，每个毛发轴包括角质层和包围在角质层中的皮质。该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施用到所述毛干来处理毛干。

5. 发明申请

US20180221833A1 SYSTEMS AND METHODS TO NITROGEN-INFUSE AND DISPENSE BEVERAGES 审中-公开
公开(公告)号：US20180221833A1
公开(公告)日：2018-08-09
申请号：US15941869
申请日：2018-03-30
申请人： Robert D. Hyde , James G. Neighbors , Brian T. Holland , Jackie Fendley , Robert F. Hoskin
发明人： Robert D. Hyde , James G. Neighbors , Brian T. Holland , Jackie Fendley , Robert F. Hoskin
IPC分类号： B01F5/04 , A47J31/46 , A47J31/40 , A23L2/54 , B01F3/04 , B01F15/00 , B67D1/00
摘要： In a method for infusing a gas from a gas source into a liquid beverage, liquid beverage is driven from a beverage container into a liquid inlet port of a venturi mixing device. Nitrogen is infused into the liquid beverage by driving nitrogen through a gas inlet port of the venturi mixing device, thereby delivering nitrogen-infused liquid beverage to a discharge port of the venturi mixing device. The nitrogen-infused liquid beverage is poured from the discharge port through a faucet.

6. 发明授权

US07097031B2 Lubricious liners and methods for their use 有权
标题翻译：润滑衬垫及其使用方法
公开(公告)号：US07097031B2
公开(公告)日：2006-08-29
申请号：US10711428
申请日：2004-09-17
申请人： Brian T. Holland , Gregory T. Robitaille , Jim J. Hilarides
发明人： Brian T. Holland , Gregory T. Robitaille , Jim J. Hilarides
IPC分类号： B65G15/60
CPC分类号： B65G17/40 , B65G45/02 , B65G2201/0244 , B65G2201/0252
摘要： Conveyor systems and methods for transporting articles, such as containers, using the conveyor systems are provided. The conveyor systems include a lubricious liner adhesively attached to a surface of a conveyor or an article for transport on the conveyor, such that the liner is disposed between the article and the surface. The lubricious liners facilitate the transport of the articles by the conveyor systems.
摘要翻译：提供了使用输送机系统输送物品（例如容器）的输送系统和方法。输送机系统包括粘附在输送机表面上的润滑衬套或用于在输送机上运输的制品，使得衬垫设置在制品和表面之间。润滑衬垫有助于输送机系统运输物品。

7. 发明申请

US20120125233A1 ORGANICALLY MODIFIED SILICA AND USE THEREOF 有权
标题翻译：有机改性二氧化硅及其用途
公开(公告)号：US20120125233A1
公开(公告)日：2012-05-24
申请号：US13360238
申请日：2012-01-27
申请人： Brian T. Holland , Ji Cui , Timothy S. Keizer
发明人： Brian T. Holland , Ji Cui , Timothy S. Keizer
IPC分类号： C09D7/12 , B32B5/16 , B82Y99/00
CPC分类号： C07F7/1804 , C07B2200/11 , Y10T428/2982
摘要： Disclosed and claimed is a novel protective coating for metal surfaces. The protective coating includes one part by weight of the organosilane-modified silica nanoparticles made by the disclosed process and further includes from 0.3 to 3 parts by weight of the reaction product of (1) a compound comprising a polyamine in which a plurality of amine groups are bonded to at least one radical selected from the group consisting of hydrocarbon and hydrocarbon ether groups that separate nitrogen atoms of said amine groups by at least four intermediate atoms in a chain, and (2) a silane which carries a plurality of silicon-bonded hydrolyzable groups and a silicon-bonded organic group that is covalently reactive to and which bonds with said amine group, said silane also comprising hydrolyzable groups, to provide a reaction product molecule which comprises an average of 2.5 to 3.5 silane groups per molecule.
摘要翻译：公开并要求保护的是用于金属表面的新型保护涂层。保护涂层包括由所公开的方法制备的一份重量的有机硅烷改性二氧化硅纳米颗粒，并且还包括0.3至3重量份的（1）包含多胺的化合物的反应产物，其中多个胺基与至少一种选自烃和烃醚基团的基团键合，所述烃基和烃醚基团将所述胺基团的氮原子分成链中至少四个中间原子，和（2）硅烷，其携带多个硅键合可水解基团和与所述胺基共价反应并与其结合的硅键合的有机基团，所述硅烷还包含可水解基团，以提供包含平均每分子2.5至3.5个硅烷基团的反应产物分子。

8. 发明授权

US08003707B2 Metal-rich siliceous compositions and methods of producing same 有权
标题翻译：富含金属的硅质组合物及其制备方法
公开(公告)号：US08003707B2
公开(公告)日：2011-08-23
申请号：US12628472
申请日：2009-12-01
申请人： Brian T. Holland
发明人： Brian T. Holland
IPC分类号： B01F3/12
CPC分类号： B01J20/103 , B01J20/16 , B01J20/3236 , B01J23/44 , B01J23/66 , B01J23/70 , B01J27/13 , B01J29/049 , B01J35/0013 , B01J37/031 , B01J37/04 , B82Y30/00 , C01B33/141 , C01B33/151 , C01G55/00 , C01P2002/72 , C01P2004/64 , C01P2006/12 , C01P2006/14
摘要： A modified sol-gel method to create metal-rich siliceous material, such as colloidal silica or aluminosilicate particles is disclosed. Initially, the metal salt of choice is added to a silicic acid solution or a silicic acid solution containing aluminum salt. The aluminum is added to vary the metal-support interaction as it forms Al—O—Si linkages within the silica matrix. Besides aluminum, other metals can be added that form M—O—Si (M=Ti, B, etc.) linkages, which do not become reduced when treated with a reducing agent. Once the metal, silicic acid and/or aluminum salt is generated, it is subjected to colloidal growth by addition to a basic heel. Upon colloidal synthesis, the metal salt containing colloidal particle is left as is to maximize colloidal stability or is reduced with hydrazine to produce the zero valence metal-containing colloidal particle. Keeping a particle colloidal before use may be an effective method of forming a catalyst material as it can be easily spray-dried or mixed with other materials for extruded catalyst particles.
摘要翻译：公开了一种改进的溶胶 - 凝胶法制备富含硅的硅质材料，例如胶体二氧化硅或硅铝酸盐颗粒。首先，将所选择的金属盐加入到含有铝盐的硅酸溶液或硅酸溶液中。添加铝以改变金属 - 载体相互作用，因为它在二氧化硅基体内形成Al-O-Si键。除了铝之外，可以加入形成M-O-Si（M = Ti，B等）键的其它金属，当用还原剂处理时，其不会降低。一旦生成了金属，硅酸和/或铝盐，则通过加入到基础鞋跟中进行胶体生长。在胶体合成时，含有胶体颗粒的金属盐保持原样以最大化胶体稳定性，或者用肼还原以产生含零价金属的胶体颗粒。在使用前保持颗粒胶体可能是形成催化剂材料的有效方法，因为它可以容易地喷雾干燥或与挤出的催化剂颗粒的其它材料混合。

9. 发明申请

US20080108497A1 METAL-RICH SILICEOUS COMPOSITIONS AND METHODS OF PRODUCING SAME 审中-公开
标题翻译：金属矿物质组合物及其生产方法
公开(公告)号：US20080108497A1
公开(公告)日：2008-05-08
申请号：US11557548
申请日：2006-11-08
申请人： Brian T. Holland
发明人： Brian T. Holland
IPC分类号： C09K13/04 , B01J20/10 , C04B35/14 , B24D3/34
CPC分类号： B01J20/103 , B01J20/16 , B01J20/3236 , B01J23/44 , B01J23/66 , B01J23/70 , B01J27/13 , B01J29/049 , B01J35/0013 , B01J37/031 , B01J37/04 , B82Y30/00 , C01B33/141 , C01B33/151 , C01G55/00 , C01P2002/72 , C01P2004/64 , C01P2006/12 , C01P2006/14
摘要： A modified sol-gel method to create metal-rich siliceous material, such as colloidal silica or aluminosilicate particles is disclosed. Initially, the metal salt of choice is added to a silicic acid solution or a silicic acid solution containing aluminum salt. The aluminum is added to vary the metal-support interaction as it forms Al—O—Si linkages within the silica matrix. Besides aluminum, other metals can be added that form M-O—Si (M=Ti, B, etc.) linkages, which do not become reduced when treated with a reducing agent. Once the metal, silicic acid and/or aluminum salt is generated, it is subjected to colloidal growth by addition to a basic heel. Upon colloidal synthesis, the metal salt containing colloidal particle is left as is to maximize colloidal stability or is reduced with hydrazine to produce the zero valence metal-containing colloidal particle. Keeping a particle colloidal before use may be an effective method of forming a catalyst material as it can be easily spray-dried or mixed with other materials for extruded catalyst particles.
摘要翻译：公开了一种改进的溶胶 - 凝胶法制备富含硅的硅质材料，例如胶体二氧化硅或硅铝酸盐颗粒。首先，将所选择的金属盐加入到含有铝盐的硅酸溶液或硅酸溶液中。添加铝以改变金属 - 载体相互作用，因为它在二氧化硅基体内形成Al-O-Si键。除了铝之外，可以加入形成M-O-Si（M = Ti，B等）键的其它金属，当用还原剂处理时，其不会降低。一旦生成了金属，硅酸和/或铝盐，则通过加入到基础鞋跟中进行胶体生长。在胶体合成时，含有胶体颗粒的金属盐保持原样以使胶体稳定性最大化，或者用肼还原以产生含零价金属的胶体颗粒。在使用前保持颗粒胶体可能是形成催化剂材料的有效方法，因为它可以容易地喷雾干燥或与挤出的催化剂颗粒的其它材料混合。

10. 发明申请

US20100166692A1 METHOD FOR TREATING DAMAGED HAIR IN CONJUNCTION WITH THE RELAXING PROCESS 审中-公开
标题翻译：用于处理与松弛过程相关的损伤头发的方法
公开(公告)号：US20100166692A1
公开(公告)日：2010-07-01
申请号：US12346310
申请日：2008-12-30
申请人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Weiz , Xiaojin Harry Li , Virginie Kompalitch
发明人： Yin Z. Hessefort , Brian T. Holland , Jeffery M. Atkins , Sascha Weiz , Xiaojin Harry Li , Virginie Kompalitch
IPC分类号： A61K8/81 , A61Q5/04
CPC分类号： A61K8/8147 , A61K8/8158 , A61K2800/5424 , A61Q5/04 , A61Q5/12
摘要： A method of treating one or more damaged hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said anionic polymers to said hair shafts.
摘要翻译：公开了一种处理一个或多个受损发根的方法，每个毛轴包括角质层和包围在角质层中的皮层。该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述阴离子聚合物的组合物施用到所述毛干来处理毛干。

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