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1. 发明授权

US06262099B1 3-(substituted phenyl)-5-(substituted cyclopropyl)-1,2,4-triazole compounds 有权
标题翻译： 3-（取代的苯基）-5-（取代的环丙基）-1,2,4-三唑化合物
公开(公告)号：US06262099B1
公开(公告)日：2001-07-17
申请号：US09426077
申请日：1999-10-22
申请人： Francis E. Tisdell , Joe R. Schoonover, Jr. , James T. Pechacek , Perry V. Ripa , Leonard P. Dintenfass , Timothy P. Martin , Donald H. DeVries , Mary L. Ash , James M. Gifford , Maurice C. Yap
发明人： Francis E. Tisdell , Joe R. Schoonover, Jr. , James T. Pechacek , Perry V. Ripa , Leonard P. Dintenfass , Timothy P. Martin , Donald H. DeVries , Mary L. Ash , James M. Gifford , Maurice C. Yap
IPC分类号： A01N43653
CPC分类号： C07D249/08 , A01N43/653 , C07C327/58
摘要： 3-(Substituted phenyl)-5-(substituted cyclopropyl)-1,2,4-triazole compounds are useful as insecticides and acaricides. New synthetic procedures and intermediates for preparing the compounds, pesticide compositions containing the compounds, and methods of controlling insects and mites using the compounds are also provided.
摘要翻译： 3-（取代的苯基）-5-（取代的环丙基）-1,2,4-三唑化合物可用作杀虫剂和杀螨剂。还提供了用于制备化合物的新合成方法和中间体，含有该化合物的农药组合物，以及使用该化合物控制昆虫和螨虫的方法。

2. 发明授权

US06265424B1 3-(substituted phenyl)-5-thienyl-1,2,4-triazole compounds with activity against whitefly 有权
标题翻译：具有抗粉虱活性的3-（取代苯基）-5-噻吩基-1,2,4-三唑化合物
公开(公告)号：US06265424B1
公开(公告)日：2001-07-24
申请号：US09426078
申请日：1999-10-22
申请人： Francis E. Tisdell , James T. Pechacek , Vidyadhar B. Hegde , Joe R. Schoonover, Jr. , Leonard P. Dintenfass , James M. Gifford , Maurice C. Yap , Donald H. DeVries , Christopher T. Hamilton , Norman R. Pearson , Mary L. Ash
发明人： Francis E. Tisdell , James T. Pechacek , Vidyadhar B. Hegde , Joe R. Schoonover, Jr. , Leonard P. Dintenfass , James M. Gifford , Maurice C. Yap , Donald H. DeVries , Christopher T. Hamilton , Norman R. Pearson , Mary L. Ash
IPC分类号： A01N43653
CPC分类号： C07D409/04 , A01N43/653
摘要： 3-(Substituted phenyl)-5-(thienyl)-1,2,4-triazole compounds are useful as insecticides and acaricides.
摘要翻译： 3-（取代的苯基）-5-（噻吩基）-1,2,4-三唑化合物可用作杀虫剂和杀螨剂。

3. 发明授权

US06413997B1 3-(substituted phenyl)-5-(substituted heterocyclyl)-1,2,4-triazole compounds 有权
标题翻译： 3-（取代的苯基）-5-（取代的杂环基）-1,2,4-三唑化合物
公开(公告)号：US06413997B1
公开(公告)日：2002-07-02
申请号：US09426930
申请日：1999-10-22
申请人： Francis E. Tisdell , Peter L. Johnson , James T. Pechacek , Robert G. Suhr , Donald H. DeVries , Carl P. Denny , Mary L. Ash
发明人： Francis E. Tisdell , Peter L. Johnson , James T. Pechacek , Robert G. Suhr , Donald H. DeVries , Carl P. Denny , Mary L. Ash
IPC分类号： A01N4378
CPC分类号： C07D403/04 , A01N43/653 , A01N43/76 , A01N43/78 , A01N43/80 , A01N43/82 , C07D403/14 , C07D413/04 , C07D417/04 , C07D417/14
摘要： 3-(Substituted phenyl)-5-(substituted heterocyclyl)-1,2,4-triazole compounds are useful as insecticides and acaricides. New synthetic procedures and intermediates for preparing the compounds, pesticide compositions containing the compounds, and methods of controlling insects and mites using the compounds are also provided.
摘要翻译： 3-（取代的苯基）-5-（取代的杂环基）-1,2,4-三唑化合物可用作杀虫剂和杀螨剂。还提供了用于制备化合物的新合成方法和中间体，含有该化合物的农药组合物，以及使用该化合物控制昆虫和螨虫的方法。

4. 发明授权

US06329528B1 Process for preparing 3-(substituted phenyl)-5-thienyl or furyl)-1,2,4-triazoles and novel intermediates utilized therein 失效
标题翻译：制备3-（取代苯基）-5-噻吩基或呋喃基）-1,2,4-三唑的方法及其中使用的新型中间体
公开(公告)号：US06329528B1
公开(公告)日：2001-12-11
申请号：US09426076
申请日：1999-10-22
申请人： Mary L. Ash , Mark W. Zettler , Norman R. Pearson , Duane R. Romer , John W. Hull, Jr. , David E. Podhorez
发明人： Mary L. Ash , Mark W. Zettler , Norman R. Pearson , Duane R. Romer , John W. Hull, Jr. , David E. Podhorez
IPC分类号： C07D40904
CPC分类号： C07D409/04 , C07C327/58 , C07D307/68 , C07D333/38
摘要： New synthetic procedures for preparing insecticidal 3-(substituted phenyl)-5-(thienyl or furyl)-1,2,4-triazoles utilizing thioimidate intermediate.
摘要翻译：使用硫代亚氨酸酯中间体制备杀虫剂3-（取代苯基）-5-（噻吩基或呋喃基）-1,2,4-三唑的新合成方法。

5. 发明授权

US5138081A Process for purifying vinylically-unsaturated organosilicon compounds 失效
标题翻译：乙烯基不饱和有机硅化合物的纯化方法
公开(公告)号：US5138081A
公开(公告)日：1992-08-11
申请号：US694521
申请日：1991-04-30
申请人： Robert A. DeVries , Mary L. Ash , Hughie R. Frick, deceased
发明人： Robert A. DeVries , Mary L. Ash , Hughie R. Frick, deceased
IPC分类号： C07F7/08 , C07F7/18 , C07F7/20
CPC分类号： C07F7/1896 , C07F7/0889 , C07F7/089 , C07F7/1892 , C07F7/20
摘要： A process for purifying an impure vinylically-unsaturated organosilicon product compound prepared by reaction between a vinylically-unsaturated organosilicon precursor and a halogenated organic compound in the presence of a homogeneous zerovalent palladium catalyst complex, the catalyst complex including an organophosphine or organoarsine ligand, in the presence of a hydrogen halide acceptor in an essentially anhydrous diluent, comprising treating a mixture containing the impure vinylically-unsaturated organosilicon product compound with a peroxide for a time sufficient to oxidize organophosphine or organoarsine impurities present in a mixture being treated. The peroxide can be selected from aqueous hydrogen peroxide or organic peroxides. The thus-treated mixture can be further treated by chromatography over silica gel or alumina. In optional embodiments, chromatography over silica gel or alumina can precede treatment with the peroxide.
摘要翻译：一种在均相的零价钯催化剂络合物（包括有机膦或有机砷配体）的催化剂络合物的存在下，通过在乙烯基不饱和有机硅前体和卤代有机化合物之间的反应制备的不纯的乙烯基不饱和有机硅产物化合物的方法，在基本上无水的稀释剂中存在卤化氢受体，包括用过氧化物处理含有不纯的乙烯基不饱和有机硅产物化合物的混合物足以氧化存在于待处理的混合物中的有机膦或有机砷杂质。过氧化物可以选自过氧化氢水溶液或有机过氧化物。这样处理的混合物可以通过硅胶或氧化铝上的色谱进一步处理。在任选的实施方案中，硅胶或氧化铝上的色谱可以在用过氧化物处理之前进行。

6. 发明授权

US4666777A Structured latex core-shell polymer particles suitable for use in the preparation of composite sheets 失效
标题翻译：适用于制备复合片材的结构化乳胶核 - 壳聚合物颗粒
公开(公告)号：US4666777A
公开(公告)日：1987-05-19
申请号：US812615
申请日：1985-12-23
申请人： Mary L. Ash , Do I. Lee , Carl H. Frick
发明人： Mary L. Ash , Do I. Lee , Carl H. Frick
IPC分类号： C08L9/10 , C08F257/02 , C08F259/02 , C08F291/00 , C08L21/02 , C08L51/00 , C08K5/34 , B32B27/08 , C08K5/13
CPC分类号： C08F259/02 , C08F257/02 , Y10S525/902 , Y10T428/2998
摘要： A structured latex polymer particle suitable for use in the preparation of a wet-laid composite sheet having good wet-end and end-use properties. The structured latex particle has a core region comprising from about 10 to about 40 percent of the total polymer particle volume and a shell region comprising from about 60 to about 90 percent of the total polymer particle volume and comprising a vinyl acid. The core region is prepared to have good end-use properties as measured by tensile and elongation and the shell region is prepared to have good wet-end properties as measured by deposition and drainage time. The subject structured latex polymer particles are thus advantageously employed in the preparation of composite sheets of all types to thus form an economical and high quality composite sheet.
摘要翻译：一种结构化的胶乳聚合物颗粒，适用于制备具有良好的湿端和终端用途的湿法复合片材。结构化胶乳颗粒具有包含总聚合物颗粒体积的约10至约40％的芯区域和包含总聚合物颗粒体积的约60至约90％并包含乙烯基酸的壳区域。核心区域被制备为具有通过拉伸和伸长率测量的良好的最终用途性质，并且通过沉积和排出时间测定壳壳区域具有良好的湿端性能。因此，本发明的结构化胶乳聚合物颗粒有利地用于制备所有类型的复合片材，从而形成经济且高质量的复合片材。

7. 发明授权

US4423222A Pyridinyl fungicides and herbicides 失效
标题翻译：吡啶类杀真菌剂和除草剂
公开(公告)号：US4423222A
公开(公告)日：1983-12-27
申请号：US380644
申请日：1982-05-21
申请人： Mary L. Ash , Richard G. Pews
发明人： Mary L. Ash , Richard G. Pews
IPC分类号： A01N53/00 , C07C51/09 , C07C51/60 , C07D213/30 , C07D213/40 , C07D213/61
CPC分类号： C07D213/30 , A01N53/00 , C07C51/09 , C07C51/60 , C07D213/40
摘要： Suitably substituted 2-aminomethyl pyridines and suitably substituted 2-pyridinylcarbinols are reacted with 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxoyl chloride in an inert solvent to form a group of biologically active organic compounds. These compounds are active as fungicides, herbicides, or both.
摘要翻译：将适当取代的2-氨基甲基吡啶和适当取代的2-吡啶基甲醇与3-（2,2-二氯乙烯基）-2,2-二甲基环丙烷甲酰氯在惰性溶剂中反应，形成一组生物活性有机化合物。这些化合物作为杀真菌剂，除草剂或两者都是有活性的。

8. 发明授权

US4414422A Purification of 4,4-dihydroxybiphenyl 失效
标题翻译： 4,4-二羟基联苯的纯化
公开(公告)号：US4414422A
公开(公告)日：1983-11-08
申请号：US376867
申请日：1982-05-10
申请人： Mary L. Ash , Timothy R. Diephouse , Robert M. Strom
发明人： Mary L. Ash , Timothy R. Diephouse , Robert M. Strom
IPC分类号： C07C37/70
CPC分类号： C07C37/70
摘要： 4,4'-Dihydroxybiphenyl is purified to remove sulfur-containing impurities, color bodies and/or phenyl-substituted phenol compounds by heating in the presence of a mixture of water and a water-miscible organic compound selected from acetone and C.sub.1-6 alkanols or diols for a time sufficient to remove substantial quantities of the sulfur-containing impurity, color bodies and/or phenyl-substituted phenol compound and thereafter recovering the purified 4,4'-dihydroxybiphenyl.
摘要翻译：通过在水和可与水混合的有机化合物的混合物存在下加热选择丙酮和C 1-6链烷醇，纯化4,4'-二羟基联苯以除去含硫杂质，着色体和/或苯基取代的酚化合物或二醇的时间足以除去大量的含硫杂质，着色体和/或苯基取代的酚化合物，然后回收纯化的4,4'-二羟基联苯。

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