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1. 发明授权

US06197276B1 Hydrated aluminum compounds, their preparation and use thereof 失效
标题翻译：水合铝化合物，其制备和用途
公开(公告)号：US06197276B1
公开(公告)日：2001-03-06
申请号：US09249077
申请日：1999-02-12
申请人： Frédéric Kolenda , Jean-Louis Guth , Sabine Valange , Zelimir Gabelica , Eric Benazzi
发明人： Frédéric Kolenda , Jean-Louis Guth , Sabine Valange , Zelimir Gabelica , Eric Benazzi
IPC分类号： C01F702
CPC分类号： C01F7/34 , C01B37/00 , C01P2002/72 , C01P2002/78 , C01P2002/86
摘要： Hydrated aluminium compounds of the present invention are represented by the general formula nS, mM, Al2O3, xH2O where S is a surfactant or a group of surfactants, n is the number of moles of S, M is an alkaline cation, preferably selected from the group formed by Na+, K+, NH4+, m is the number of moles of M and x is the number of moles of water. The hydrated compounds are obtained from inorganic aluminium sources which are in the form of cation-monomers and/or cation-oligomers. The surfactants are anionic and/or non-ionic surfactants. When the group of surfactants comprises at least one anionic surfactant, at least one cationic surfactant can optionally be added.
摘要翻译：本发明的水合铝化合物由通式nS，mM，Al 2 O 3，xH 2 O表示，其中S是表面活性剂或一组表面活性剂，n是S的摩尔数，M是碱性阳离子，优选选自由Na +，K +，NH 4 +，m形成的基团是M的摩尔数，x是水的摩尔数。水合化合物由阳离子单体和/或阳离子低聚物形式的无机铝源获得。表面活性剂是阴离子和/或非离子表面活性剂。当该组表面活性剂包含至少一种阴离子表面活性剂时，可以任选地加入至少一种阳离子表面活性剂。

2. 发明授权

US06548040B1 Process for preparing a zeolite with structure type MTT using specific template precursors 有权
标题翻译：使用特定模板前体制备具有MTT结构类型的沸石的方法
公开(公告)号：US06548040B1
公开(公告)日：2003-04-15
申请号：US09672053
申请日：2000-09-29
申请人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
发明人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
IPC分类号： C01B3948
CPC分类号： B01J20/18 , B01J29/04 , C01B39/48 , C10G45/64 , Y10S423/36
摘要： The present invention concerns a process for synthesising a zeolite with structure type MTT comprising at least one element X selected from silicon and germanium and at least one element T selected from aluminium, iron gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, comprising reacting an aqueous mixture comprising at least one source of at least one element X, at least one source of at least one element T, and at least one precursor of an organic compound comprising at least one alkylated polymethylene &agr;-&ohgr; diammonium derivative, characterized in that at least one precursor is selected from monoamines. The present invention also concerns the use of the zeolite obtained as a catalyst in a process for converting hydrocarbon-containing feeds, as an adsorbent to control pollution and as a molecular sieve for separation.
摘要翻译：本发明涉及合成具有结构类型MTT的沸石的方法，该方法包括至少一种选自硅和锗的元素X和至少一种选自铝，铁镓，硼，钛，钒，锆，钼，砷，锑，铬和锰，包括使包含至少一种元素X的至少一种源，至少一种元素T的至少一种源的至少一种含有至少一种烷基化聚亚甲基α - 大豆二铵衍生物，其特征在于至少一种前体选自单胺。本发明还涉及在用于转化含烃原料作为吸附剂以控制污染和分离分子筛的方法中作为催化剂获得的沸石的用途。

3. 发明授权

US06692723B2 MTT zeolite comprising crystals and crystal aggregates with specific granulometries, and its use as a catalyst for isomerizing straight chain paraffins 有权
标题翻译：包含晶体和具有特定粒度的晶体聚集体的MTT沸石及其作为直链烷烃异构化催化剂的用途
公开(公告)号：US06692723B2
公开(公告)日：2004-02-17
申请号：US09788480
申请日：2001-02-21
申请人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
发明人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
IPC分类号： C01B3904
CPC分类号： C10G45/64 , B01J20/18 , B01J29/70 , B01J29/74 , B01J35/023 , B01J2229/26 , B01J2229/42 , C01B39/48 , Y10S423/36
摘要： The invention concerns a zeolite with structure type MTT comprising MTT zeolite crystals with a size of less than 5 &mgr;m, at least a portion of the MTT zeolite crystals being in the form of MTT zeolite crystal aggregates, said zeolite being characterized in that the granulometry of the aggregates is such that the dimension Dv,90 is in the range 40 nm to 100 &mgr;m. The invention also concerns the preparation of the zeolite and the use of the zeolite as a catalyst in a process for converting hydrocarbon feeds, and in particular in a process for isomerizing straight chain paraffins.
摘要翻译：本发明涉及结构类型为MTT的沸石，其包含尺寸小于5um的MTT沸石晶体，至少一部分MTT沸石晶体为MTT沸石晶体聚集体形式，所述沸石的特征在于，粒度测定聚集体使得尺寸Dv，90在40nm至100μm的范围内。本发明还涉及沸石的制备以及沸石作为转化烃原料的方法中的催化剂的用途，特别是在使直链烷烃异构化的方法中。

4. 发明授权

US06475464B1 Process for preparing a zeolite with structure type MTT using zeolitic material seeds 有权
标题翻译：使用沸石材料种子制备具有MTT结构型沸石的沸石的方法
公开(公告)号：US06475464B1
公开(公告)日：2002-11-05
申请号：US09672052
申请日：2000-09-29
申请人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
发明人： Loïc Rouleau , Frédéric Kolenda , Eric Benazzi
IPC分类号： C01B3948
CPC分类号： C10G45/64 , B01J20/18 , B01J29/04 , C01B39/48 , Y10S423/36
摘要： The present invention concerns a process for preparing a zeolite with structure type MTT comprising at least one element X selected from silicon and germanium and at least one element T selected from iron, aluminium, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, characterized in that seeds of at least one zeolitic material are used comprising at least one element X′ selected from silicon and germanium and at least one element T′ selected from iron, aluminium, gallium, boron, titanium, vanadium, zirconium, molybdenum, arsenic, antimony, chromium and manganese, said seeds being different from the zeolite with structure type MTT being synthesised. The present invention also concerns the use of the zeolite obtained as a catalyst in a process for converting hydrocarbon-containing feeds, as an adsorbent to control pollution and as a molecular sieve for separation.
摘要翻译：本发明涉及一种制备具有结构类型MTT的沸石的方法，该方法包括至少一种选自硅和锗的元素X以及选自铁，铝，镓，硼，钛，钒，锆，钼，砷中的至少一种元素T. ，锑，铬和锰，其特征在于使用至少一种沸石材料的种子，其包含至少一种选自硅和锗的元素X'和至少一种选自铁，铝，镓，硼，钛，钒，锆，钼，砷，锑，铬和锰，所述种子不同于合成结构型MTT的沸石。本发明还涉及在用于转化含烃原料作为吸附剂以控制污染和分离分子筛的方法中作为催化剂获得的沸石的用途。

5. 发明授权

US6136290A IM-5 zeolite, a process for its preparation and catalytic applications thereof 失效
标题翻译： IM-5沸石，其制备方法和催化应用
公开(公告)号：US6136290A
公开(公告)日：2000-10-24
申请号：US955117
申请日：1997-10-21
申请人： Eric Benazzi , Jean-Louis Guth , Loic Rouleau
发明人： Eric Benazzi , Jean-Louis Guth , Loic Rouleau
IPC分类号： B01J29/70 , B01J29/00 , B01J29/04 , C01B39/46 , C01B39/48 , C10G49/08 , B01J29/06 , C10G11/05
CPC分类号： C10G49/08 , B01J29/04 , C01B39/48
摘要： The invention concerns IM-5 zeolite with a chemical composition with the following formula, expressed in terms of the mole ratios of the oxides for the anhydrous state: 100XO.sub.2,mY.sub.2 O.sub.3, pR.sub.2/n O where m is 10 or less; p is in the range 0 to 20; R represents one or more cations with valency n; X represents silicon and/or germanium; Y represents one or more of the following elements: aluminum, iron, gallium, boron and titanium. The zeolite is characterized by an Xray diffraction diagram, in its as synthesized state, which comprises the results shown in Table 1 of the description. The invention also concerns the preparation of the zeolite, any catalyst containing the zeolite and any catalytic process using such a catalyst.
摘要翻译：本发明涉及具有下式的化学组成的IM-5沸石，以无水状态的氧化物的摩尔比表示：100XO2，mY2O3，pR2 / nO，其中m为10或更小; p在0到20之间; R表示一个或多个价数为n的阳离子; X表示硅和/或锗; Y表示以下元素中的一种或多种：铝，铁，镓，硼和钛。沸石的特征在于XRD衍射图，其合成状态包括说明书的表1所示的结果。本发明还涉及沸石的制备，含有沸石的任何催化剂以及使用这种催化剂的任何催化方法。

6. 发明授权

US5695735A Process for the synthesis of zeolites and mesoporous solids from a homogeneous solution in a semi-open system 失效
标题翻译：在半开放系统中从均相溶液合成沸石和介孔固体的方法
公开(公告)号：US5695735A
公开(公告)日：1997-12-09
申请号：US565399
申请日：1995-11-30
申请人： Eric Benazzi , Pierre-Yves Legoff , Philippe Caullet , Jean-Louis Guth
发明人： Eric Benazzi , Pierre-Yves Legoff , Philippe Caullet , Jean-Louis Guth
IPC分类号： C01B37/02 , C01B39/02 , C01B39/04 , C01B39/24 , C01B39/30 , C01B39/38 , C01B39/40 , C01B39/48
CPC分类号： C01B39/02 , C01B37/02 , C01B39/04 , C01B39/24 , C01B39/305 , C01B39/40 , C01B39/48 , Y10S423/21 , Y10S423/22 , Y10S423/27 , Y10S423/32 , Y10S423/38
摘要： The invention concerns a process for the synthesis of zeolites based on element(s) T and mesoporous solids based on element(s) T, T being silicon and/or aluminium, comprising the following sequence of steps: i) synthesizing a reaction medium which is a homogeneous source of element(s) T containing: a) at least one source of element(s) T selected from the group formed by aqueous basic solutions of silica or silica and alumina and alcoholic solutions of alkyl tetraorthosilicate and trialkoxyaluminium; b) optionally, at least one structuring agent; c) optionally, seeds of the desired crystalline phase; ii) heating the reaction medium to a temperature in the range 20.degree. C. to 220.degree. C. for a period in the range several minutes and several days; iii) injecting at least one chemical agent at a controlled rate to generate polycondensable species in said medium.
摘要翻译：本发明涉及一种基于元素T和介孔固体的基于元素T，T为硅和/或铝的合成沸石的方法，其包括以下步骤顺序：i）合成反应介质，其中是元素T的均匀源，其含有：a）选自由二氧化硅或二氧化硅和氧化铝的碱性水溶液形成的基团中的至少一种元素T，以及四原硅酸烷基酯和三烷氧基铝的烷基醇溶液; b）任选地，至少一种结构剂; c）任选地，所需结晶相的种子; ii）将反应介质加热至20℃至220℃的温度，持续数分钟和数天的时间; iii）以受控的速率注射至少一种化学试剂以在所述介质中产生可缩聚物质。

7. 发明授权

US07390393B2 Process for converting heavy petroleum fractions including an ebulliated bed for producing middle distillates with a low sulfur content 有权
$Process for converting heavy petroleum fractions including an ebulliated bed for producing middle distillates with a low sulfur content$
标题翻译：用于转化重质石油馏分的方法，包括用于生产低硫含量的中间馏分的沸腾床
公开(公告)号：US07390393B2
公开(公告)日：2008-06-24
申请号：US11505285
申请日：2006-08-17
申请人： Christophe Gueret , Pierre Marion , Cecile Plain , Jerome Bonnardot , Eric Benazzi , Olivier Martin
发明人： Christophe Gueret , Pierre Marion , Cecile Plain , Jerome Bonnardot , Eric Benazzi , Olivier Martin
IPC分类号： C10G45/00
CPC分类号： C10G49/007 , C10G2400/06
摘要： The invention relates to a process for treating heavy petroleum feedstocks for producing a gas oil fraction that has a sulfur content of less than 50 ppm and most often 10 ppm that includes the following stages: a) ebulliated-bed catalytic hydrocracking, b) separation from hydrogen sulfide of a distillate fraction that includes a gas oil fraction and a heavier fraction than the gas oil, c) hydrotreatment of said distillate fraction, and d) separation of a gas oil fraction with less than 50 ppm of sulfur. Make-up hydrogen, preferably all make-up hydrogen, is to stage c). Advantageously, the heavier fraction from step (b) is subjected to catalytic cracking. The invention also relates to an installation that can be used for implementing this process.
摘要翻译：本发明涉及一种处理重质石油原料的方法，用于生产硫含量小于50ppm，最常为10ppm的瓦斯油馏分，其包括以下步骤：a）沸腾床催化加氢裂化，b）馏出物馏分的硫化氢，其包含粗柴油馏分和比瓦斯油更重的馏分，c）加氢处理所述馏出物馏分，以及d）分离具有小于50ppm硫的粗柴油馏分。补充氢，优选所有化妆氢，都是阶段c）。有利地，来自步骤（b）的较重馏分经受催化裂化。本发明还涉及可用于实现该过程的安装。

8. 发明授权

US07270738B2 Catalyst and process for hydrocracking hydrocarbon-containing feedstocks 有权
标题翻译：用于加氢裂化含烃原料的催化剂和方法
公开(公告)号：US07270738B2
公开(公告)日：2007-09-18
申请号：US10696561
申请日：2003-10-30
申请人： Patrick Euzen , Carole Bobin , Magalie Roy-Auberger , Eric Benazzi , Patrick Bourges , Christophe Gueret
发明人： Patrick Euzen , Carole Bobin , Magalie Roy-Auberger , Eric Benazzi , Patrick Bourges , Christophe Gueret
IPC分类号： C01G47/00 , C01G45/00 , C01G17/00 , B01J23/00 , B01J21/00
CPC分类号： B01J35/10 , B01J21/12 , B01J23/24 , B01J23/42 , B01J23/74 , B01J23/85 , B01J23/888 , B01J35/002 , B01J35/1019 , B01J35/1038 , B01J35/1061 , B01J35/108 , B01J37/0009 , C10G47/12 , C10G47/14 , C10G47/16 , C10G47/20 , C10G65/12 , C10G2300/107 , C10G2300/1074 , C10G2300/1077 , C10G2300/4018 , C10G2300/70
摘要： This invention relates to silico-aluminum substrates, catalysts, and the hydrocracking and hydrotreatment processes that use them. The catalyst comprises at least one hydro-dehydrogenating element that is selected from the group that is formed by elements of group VIB and group VIII of the periodic table and a non-zeolitic silica-alumina-based substrate that contains an amount of more than 5% by weight and less than or equal to 95% by weight of silica (SiO2) and has the following characteristics: A mean pore diameter, measured by mercury porosimetry, encompassed between 20 and 140 Å, a total pore volume, measured by mercury porosimetry, encompassed between 0.1 ml/g and 0.6 ml/g, a total pore volume, measured by nitrogen porosimetry, encompassed between 0.1 ml/g and 0.6 ml/g, a BET specific surface area encompassed between 100 and 550 m2/g, a pore volume, measured by mercury porosimetry, encompassed in the pores with diameters of more than 140 Å, of less than 0.1 ml/g, a pore volume, measured by mercury porosimetry, encompassed in the pores with diameters of more than 160 Å, of less than 0.1 ml/g, a pore volume, measured by mercury porosimetry, encompassed in the pores with diameters of more than 200 Å, of less than 0.1 ml/g, a pore volume, measured by mercury porosimetry, encompassed in the pores with diameters of more than 500 Å, of less than 0.01 ml/g, an X diffraction diagram contains at least the main lines that are characteristic of at least one of the transition aluminas contained in the group that consists of the alpha, rho, chi, eta, gamma, kappa, theta and delta aluminas.
摘要翻译：本发明涉及硅铝基板，催化剂以及使用它们的加氢裂化和加氢处理方法。该催化剂包含至少一种选自由元素周期表VIB族和VIII族的元素形成的基团和非沸石二氧化硅 - 氧化铝基底物的含氢量超过5的氢脱氢元件重量百分比和小于或等于95重量％的二氧化硅（SiO 2/2），并具有以下特征：通过水银孔率法测量的平均孔径包含在20和140之间，a 通过水银孔率法测量的总孔体积在0.1ml / g至0.6ml / g之间，通过氮气孔率法测量的总孔体积在0.1ml / g至0.6ml / g之间，包括在 100和550m 2 / g，通过水银孔率法测量的孔体积包含在直径大于140埃，小于0.1ml / g的孔中，孔体积由包含在直径大于160埃，小于0的孔中的水银孔率法。 1毫升/克，通过水银孔率测定法测量的孔体积，直径大于200埃，小于0.1毫升/克，通过水银孔率法测定的孔体积，包含在直径为大于500埃，小于0.01ml / g，X衍射图至少包含由α，rho，chi，eta等组成的组中包含的至少一种过渡氧化铝的特征的主线， γ，κ，θ和δ氧化铝。

9. 发明授权

US06884339B2 Flexible method for producing oil bases with a ZSM-48 zeolite 有权
标题翻译：用ZSM-48沸石生产油基的灵活方法
公开(公告)号：US06884339B2
公开(公告)日：2005-04-26
申请号：US10018526
申请日：2001-04-20
申请人： Eric Benazzi , Pierre Marion , Alain Billon , Christophe Gueret , Jean-Claude Hipeaux , Jean Paul Gouzard
发明人： Eric Benazzi , Pierre Marion , Alain Billon , Christophe Gueret , Jean-Claude Hipeaux , Jean Paul Gouzard
IPC分类号： C10G45/08 , C10G45/50 , C10G45/52 , C10G45/62 , C10G45/64 , C10G47/20 , C10G65/08 , C10G65/12 , C10G67/04 , C10M101/02 , C10N70/00 , C10G69/02
CPC分类号： C10G65/12 , C10G2400/10
摘要： A process for the production of very high quality base oils optionally with simultaneous production of high quality middle distillates comprises the stages for hydrotreatment, preferably hydrocracking, on Y or beta zeolite, and atmospheric distillation. The effluent is subjected to a catalytic dewaxing on the ZSM-48 catalyst. The process then comprises a hydrofinishing stage for hydrogenating the aromatic compounds, preferably on a catalyst that comprises at least one noble metal of group VIII, chlorine and fluorine, and the stages of atmospheric and vacuum distillation. The hydrofinishing stage is conducted at a temperature lower by 20-200° C. than the catalytic dewaxing stage.
摘要翻译：任选地同时生产高品质中间馏分的生产非常高质量的基础油的方法包括在Y或β沸石上进行加氢处理，优选加氢裂化的阶段和常压蒸馏。流出物在ZSM-48催化剂上进行催化脱蜡。该方法然后包括用于氢化芳族化合物的加氢精制阶段，优选在包含至少一种VIII族的贵金属，氯和氟的催化剂上，以及大气压和真空蒸馏阶段。加氢精制阶段在比催化脱蜡阶段低20-200℃的温度下进行。

10. 发明授权

US06583330B1 Catalysts containing heteropolyanions usable in processes for conversion of paraffins 失效
标题翻译：含有可用于石蜡转化方法的杂多阴离子的催化剂
公开(公告)号：US06583330B1
公开(公告)日：2003-06-24
申请号：US09604055
申请日：2000-06-26
申请人： Christine Travers , Maryline Delage , Eric Benazzi , Jean-François Joly
发明人： Christine Travers , Maryline Delage , Eric Benazzi , Jean-François Joly
IPC分类号： C07C258
CPC分类号： B01J21/066 , B01J27/188 , C07C2/58 , C07C5/2791 , C07C2521/06 , C07C2523/44 , C07C2523/46 , C07C2523/755 , C07C2523/88 , C07C2523/888 , C07C2527/18 , C07C9/00
摘要： New catalysts that contain heteropolyanions of the 12-tungstophosphoric acid or the 12-tungstomolybdic acid, and, for some of these, at least one metal of group VIII, and that are deposited on substrates that develop a specific surface area and a high pore volume, such as zirconium oxide (ZrO2), silicas, silica-aluminas or aluminas, are used in particular in isomerization of paraffinic fractions that contain in large part n-paraffins that have, for example, 4 to 8 carbon atoms per molecule and in aliphatic alkylation of isoparaffins (for example isobutane and/or isopentane) by at least one olefin that comprises, for example, 2 to 6 carbon atoms per molecule (C2 to C6).
摘要翻译：含有12-钨磷酸或12-钨钼酸杂多糖的新型催化剂，以及其中一些这些至少一种第VIII族金属，并且沉积在形成比表面积和高孔体积的基材上，例如氧化锆（ZrO 2），二氧化硅，二氧化硅 - 氧化铝或氧化铝，特别是用于大部分含有例如每分子4至8个碳原子的正链烷烃和脂族的链烷烃级分的异构化通过至少一种包含例如每分子2至6个碳原子（C 2至C 6）的烯烃烷基化异链烷烃（例如异丁烷和/或异戊烷）。

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