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1. 发明授权

US5952095A Intercalates and exfoliates formed with long chain (C.sub.10 +) monomeric organic intercalant compounds; and composite materials containing same 失效
标题翻译：由长链（C10 +）单体有机插层剂形成的插层和去角质; 和含有它们的复合材料
公开(公告)号：US5952095A
公开(公告)日：1999-09-14
申请号：US758740
申请日：1996-12-06
申请人： Gary W. Beall , Fernando Serrano , Semeon Tsipursky , Steven J. Engman
发明人： Gary W. Beall , Fernando Serrano , Semeon Tsipursky , Steven J. Engman
IPC分类号： C01B33/44 , C08K7/00 , C08K9/04 , C08L101/00 , C09C1/42 , C09C3/10 , B32B7/00
CPC分类号： C09C1/42 , C01B33/44 , C08K9/04 , C09C3/10 , C01P2002/08 , C01P2002/72 , C01P2002/77 , C01P2004/54 , Y10T428/26
摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer including an alkyl radical having at least 10 carbon atoms and having a dipole moment greater than the dipole moment of water, to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix.
摘要翻译：通过使层状材料例如页硅酸盐与包含具有至少10个碳原子的烷基并且具有大于偶极矩的偶极矩的插层单体接触形成的插层，以吸附或插入相邻片晶之间的插入剂单体的分层材料。在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在约10-45安士，使得插入物容易被剥离成单独的血小板。插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。

2. 发明授权

US5844032A Intercalates and exfoliates formed with non-EVOH monomers, oligomers and polymers; and EVOH composite materials containing same 失效
标题翻译：用非EVOH单体，低聚物和聚合物形成的插层和去角质; 和含有它的EVOH复合材料
公开(公告)号：US5844032A
公开(公告)日：1998-12-01
申请号：US761444
申请日：1996-12-06
申请人： Fernando Serrano , Steven J. Engman , Gary W. Beall
发明人： Fernando Serrano , Steven J. Engman , Gary W. Beall
IPC分类号： C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C08L29/02 , C08L29/04 , C08L39/06 , C08L71/00 , C08L71/02 , C11C5/00
CPC分类号： C08K9/08 , B82Y30/00 , C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C11C5/002 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Nanocomposites are manufactured by combining an EVOH matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with a non-EVOH intercalant to adsorb or intercalate the intercalant between adjacent phyllosilicate platelets. Sufficient intercalant is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG., preferably at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with the EVOH matrix polymer melt, to provide an EVOH matrix polymer/platelet composite (nanocomposite) material that does not degrade the EVOH matrix polymer.
摘要翻译：通过组合EVOH基质聚合物和通过使页硅酸盐与非EVOH插入剂接触形成的剥离的嵌入物来吸附或插入相邻的页硅酸盐片晶之间的插入剂来制造纳米复合材料。在相邻的页硅酸盐血小板之间吸附足够的嵌入剂以将相邻的血小板膨胀至至少约5 ANGSTROM，优选至少约10 ANGSTROM（在除水后测量）的间隔，高达约100安培，优选在约30 -40 ANGSTROM，使得嵌入物容易被剥离，例如当与EVOH基质聚合物熔体混合时，提供不会降解EVOH基质聚合物的EVOH基质聚合物/片晶复合材料（纳米复合材料）材料。

3. 发明授权

US06228903B1 Exfoliated layered materials and nanocomposites comprising said exfoliated layered materials having water-insoluble oligomers or polymers adhered thereto 有权
标题翻译：剥离的层状材料和纳米复合材料，其包含粘附有水不溶性低聚物或聚合物的所述剥离层状材料
公开(公告)号：US06228903B1
公开(公告)日：2001-05-08
申请号：US09283954
申请日：1999-04-01
申请人： Gary W. Beall , Fernando Serrano , Hannah Cruz
发明人： Gary W. Beall , Fernando Serrano , Hannah Cruz
IPC分类号： C08K904
CPC分类号： B82Y30/00 , C01B33/44 , C01P2002/70 , C01P2002/74 , C01P2002/88 , C01P2004/20 , C01P2004/54 , C01P2004/64 , C01P2006/22 , C01P2006/80 , C08K7/00 , C08K9/04 , C08K9/08 , C09C1/42 , C11C5/002
摘要： A phyllosilicate material is exfoliated by admixture of the phyllosilicate with water, and a solvent for a water-insoluble oligomer or polymer that is sorbed or electrostatically bonded to the inner surfaces of the phyllosilicate platelets after exfoliation of the phyllosilicate. Intercalation and exfoliation can be achieved via contact of the phyllosilicate with an organic solvent and water to electrostatically bond one or more polar moieties from the organic solvent to a metal cation on the platelet inner surfaces, so that after evaporation of the water used for intercalation of the organic solvent between phyllosilicate platelets, the platelets do not then collapse together, but remain exfoliated. After exfoliation of the phyllosilicate, the exfoliated platelets are contacted with a polymer/carrier composition that includes a water-insoluble polymer or water-insoluble oligomer, and a solvent for the water-insoluble polymer or oligomer. After exfoliating the phyllosilicate and prior to polymer contact, the individual phyllosilicate platelets are contacted with the polymer/carrier composition to sorb the water-insoluble polymer or water-insoluble oligomer onto one or both surfaces of the exfoliated phyllosilicate platelets and drive off the adhered solvent.
摘要翻译：页硅酸盐材料通过页硅酸盐与水的混合物的剥离，以及在剥离页硅酸盐之后被吸附或静电粘合到页硅酸盐片的内表面的水不溶性低聚物或聚合物的溶剂。插层和剥离可以通过页硅酸盐与有机溶剂和水的接触来实现，以将一个或多个极性部分从有机溶剂静电粘结到血小板内表面上的金属阳离子上，使得在用于插入页硅酸盐血小板之间的有机溶剂，血小板不会一起塌陷，而是保持剥离。在剥离页硅酸盐之后，将剥离的血小板与包含水不溶性聚合物或水不溶性低聚物的聚合物/载体组合物和水不溶性聚合物或低聚物的溶剂接触。在剥离页硅酸盐并且在聚合物接触之前，使单独的页硅酸盐血小板与聚合物/载体组合物接触以将不溶于水的聚合物或水不溶性低聚物吸附到剥离的页硅酸盐血小板的一个或两个表面上并驱除粘附的溶剂。

4. 发明申请

US20130112925A1 METHOD AND SYSTEM FOR PRODUCING GRAPHENE AND GRAPHENOL 失效
标题翻译：用于生产石墨和石墨烯的方法和系统
公开(公告)号：US20130112925A1
公开(公告)日：2013-05-09
申请号：US13659570
申请日：2012-10-24
申请人： Gary W. Beall
发明人： Gary W. Beall
IPC分类号： C07C37/00
CPC分类号： C07C37/002 , B82Y30/00 , B82Y40/00 , C01B32/184 , C07C2603/54 , C08K5/053 , C07C39/12
摘要： This disclosure includes a process that unexpectedly can produce very inexpensive graphene and a new compound called graphenol in particulate or dispersions in solvents. The process can also produce graphene layers on metallic and nonmetallic substrates. Further, the graphenol and graphene can be utilized to form nanocomposites that yield property improvements exceeding anything reported previously.
摘要翻译：该公开内容包括意外地可以生产非常便宜的石墨烯和称为石墨烯的新化合物的方法，其在溶剂中的颗粒或分散体中。该工艺还可以在金属和非金属基底上生产石墨烯层。此外，可以利用石墨烯和石墨烯来形成纳米复合材料，其产生超过以前报道的任何物质改进。

5. 发明授权

US08362134B2 Film comprising silicate platelets of exfoliated from phospolipid-intercalated layered silicate 有权
公开(公告)号：US08362134B2
公开(公告)日：2013-01-29
申请号：US11990614
申请日：2006-08-15
申请人： Michael D. Grah , Gary W. Beall
发明人： Michael D. Grah , Gary W. Beall
IPC分类号： C01B33/44 , B65D65/40 , C08K5/52
CPC分类号： C01B33/44 , C08K5/10 , C08K9/04 , Y10T428/261
摘要： A packaging film comprises a dispersed-particle composition, which comprises a plurality of particles dispersed in a matrix medium of thermoplastic polymer. The particles comprise silicate platelets. Intercalating agent of one or more phospholipids is sorbed to the silicate platelets.

6. 发明授权

US07772362B2 Treatment method for imparting self-healing and shape memory properties to certain CBDO copolymers 有权
标题翻译：赋予某些CBDO共聚物自我修复和形状记忆性能的处理方法
公开(公告)号：US07772362B2
公开(公告)日：2010-08-10
申请号：US12173186
申请日：2008-07-15
申请人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
发明人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
IPC分类号： C08F6/00
CPC分类号： C08G63/88 , C08G63/199
摘要： A method of treating an amorphous CBDO polymer to impart self healing and shape memory properties by heat treatment, and products resulting from such method are described. An amorphous CBDO copolymer may include a copolyester prepared by reacting an aromatic dicarboxylic acid or ester or anhydride thereof, a 2,2,4,4-tetraalkyl-1,3-cyclobutanediol and 1,3-propanediol, 1,4-butanediol, or mixture thereof. The method may include heating said copolymer to a temperature above its glass transition temperature to impart self healing and shape memory properties.
摘要翻译：描述了通过热处理处理无定形CBDO聚合物以赋予自愈和形状记忆特性的方法，并且描述了由这种方法产生的产品。无定形CBDO共聚物可以包括通过使芳族二羧酸或其酯或酸酐，2,2,4,4-四烷基-1,3-环丁二醇和1,3-丙二醇，1,4-丁二醇，或其混合物。该方法可以包括将所述共聚物加热至高于其玻璃化转变温度的温度以赋予自愈合和形状记忆性能。

7. 发明申请

US20090023885A1 TREATMENT METHOD FOR IMPARTING HIGH IMPACT RESISTANCE IN CERTAIN CBDO COPOLYMERS 审中-公开
标题翻译：在某些CBDO共聚物中阻止高抗冲击性的处理方法
公开(公告)号：US20090023885A1
公开(公告)日：2009-01-22
申请号：US12173314
申请日：2008-07-15
申请人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
发明人： Gary W. Beall , Jesse R. Hancock , Chad J. Booth
IPC分类号： C08G63/16
CPC分类号： C08G63/88 , C08G63/199
摘要： According to the invention, an amorphous CBDO copolymer (as described in U.S. Pat. No. 5,705,575, issued Jan. 6, 1998, which U.S. patent is incorporated herein by reference in its entirety) is treated to impart high impact resistance, also called impact strength.
摘要翻译：根据本发明，处理无定形CBDO共聚物（如美国专利5,705,575（1998年1月6日授权，其全部内容通过引用并入本文作为参考）中所述）以赋予高抗冲击性，也称为冲击强度。

8. 发明授权

US06235533B1 Method of determining the composition of clay deposit 失效
标题翻译：确定粘土沉积物组成的方法
公开(公告)号：US06235533B1
公开(公告)日：2001-05-22
申请号：US09040633
申请日：1998-03-18
申请人： Semeon J. Tsipursky , Don D. Eisenhour , Gary W. Beall , Mark Clarey , James Edwards
发明人： Semeon J. Tsipursky , Don D. Eisenhour , Gary W. Beall , Mark Clarey , James Edwards
IPC分类号： G01N3300
CPC分类号： G01N33/24 , G01N33/383
摘要： A method of determining a quantity of amorphous SiC2-containing impurities in a montmorillonite clay sample comprising the steps of: (a) analyzing the clay sample to determine the weight percent of SiO2 contained in the clay sample; (b) analyzing the clay sample for non-montmorillonite SiO2-containing crystalline components; (c) calculating the weight percent of SiO2 from step (a) that is derived from the montmorillonite and amorphous SiQ2-containing impurities by lowering the weight percent of SiO2 in step (a) based on the non-montmorillonite SiO2-containing crystalline impurities found in step (b); and (d) determining the amorphous SiO2-containing impurity portion of the SiO2 calculated in step (c) by further lowering the amount of SiO2 from step (c) until the amount of montmorillonite-derived SiO2 is consistent with one or more properties of the clay sample, the amount of further lowering being proportional to an amount of amorphous SiO2-containing impurities contained in the clay sample.
摘要翻译：一种测定蒙脱石粘土样品中含无定形SiC 2的杂质的量的方法，包括以下步骤：（a）分析粘土样品以确定粘土样品中所含的SiO 2的重量百分比;（b）分析粘土样品非蒙脱土SiO 2的结晶成分;（c）通过降低步骤（a）中SiO 2的重量百分比来计算源自蒙脱土和含有无定形SiQ 2的杂质的步骤（a）中SiO 2的重量百分比，基于在步骤（b）中发现的非蒙脱石SiO 2结晶杂质; 和（d）通过进一步降低步骤（c）中的SiO 2的量直到由蒙脱石衍生的SiO 2的量与所述SiO 2的一个或多个性质一致来确定在步骤（c）中计算出的SiO 2的无定形SiO 2杂质部分粘土样品，进一步降低的量与粘土样品中所含的无定形SiO 2杂质的量成比例。

9. 发明授权

US5877248A Intercalates and exfoliates formed with oligomers and polymers and composite materials containing same 失效
标题翻译：用低聚物和聚合物形成的插层物和去角质物以及含有它们的复合材料
公开(公告)号：US5877248A
公开(公告)日：1999-03-02
申请号：US968408
申请日：1997-11-12
申请人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
发明人： Gary W. Beall , Semeon Tsipursky , Anatoliy Sorokin , Anatoliy Goldman
IPC分类号： C01B33/44 , C08K3/00 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C08L101/00 , C11C5/00 , C08J5/10 , C08L39/06
CPC分类号： B82Y30/00 , A61K8/26 , A61K8/27 , A61K8/8176 , A61Q5/04 , C01B33/44 , C08K3/34 , C08K7/00 , C08K9/04 , C08K9/08 , C11C5/002 , A61K2800/56 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/64
摘要： Nanocomposites are manufactured by combining a host material, such as an organic solvent or a matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with a polymer to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG., preferably at least about 10 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with an organic solvent or a polymer melt, to provide a carrier material for drugs and the like, or to provide a matrix polymer/platelet composite (nanocomposite) material--the platelets being exfoliated from the intercalate.
摘要翻译：纳米复合材料通过将主体材料如有机溶剂或基质聚合物和通过使页硅酸盐与聚合物接触形成的剥离的嵌入物组合而制造，以在相邻的页硅酸盐片剂之间吸附或嵌入聚合物。在相邻的页硅酸盐片晶之间吸附足够的聚合物以将相邻的血小板膨胀至至少约5安培的间隔，优选至少约10安培（在除水后测量），高达约100安培，优选在约30约 -40 ANGSTROM，使得嵌入物容易被剥离，例如当与有机溶剂或聚合物熔体混合时，提供用于药物等的载体材料，或提供基质聚合物/血小板复合材料（纳米复合材料） - 血小板从插层中剥离。

10. 发明授权

US5452684A Method of agglomerating a smectite clay litter 失效
标题翻译：挤出的蒙脱石粘土结块动物垃圾具有改善的团块强度
公开(公告)号：US5452684A
公开(公告)日：1995-09-26
申请号：US248304
申请日：1994-05-24
申请人： Carol Elazier-Davis , Gary W. Beall , John Hughes
发明人： Carol Elazier-Davis , Gary W. Beall , John Hughes
IPC分类号： A01K1/015 , B01J2/20 , B01J20/12 , C09K3/00
CPC分类号： A01K1/0155 , A01K1/0154
摘要： An animal litter including an extruded smectite clay that forms stronger clumps, when wetted with animal urine, due to the extrusion process. In a preferred embodiment, the extruded smectite clay is mixed, before or after extrusion, with a small percentage, preferably at least about 0.025% to less than 0.1%, based on the dry weight of the smectite clay, of a water-soluble adhesive that forms improved, stronger, more cohesive clumps that can be essentially completely removed from a litter box leaving the remaining litter box contents odor-free.
摘要翻译：一种动物垃圾，包括挤压蒙脱石粘土，由于挤出过程而形成较强的团块，当用动物尿液润湿时。在优选的实施方案中，将挤出的蒙脱石粘土在挤出之前或之后以基于蒙脱石粘土的干重为基础的小百分比，优选至少约0.025％至小于0.1％的水溶性粘合剂其形成改进的，更强的，更具凝聚力的团块，其可以从垃圾箱基本上完全去除，使得剩余的垃圾箱内容物不含气味。

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