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1. 发明申请

US20070299189A1 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 失效
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：US20070299189A1
公开(公告)日：2007-12-27
申请号：US11766850
申请日：2007-06-22
申请人： Feng Cao , Kwok Chan , Erik Hagberg , Farid Khouri , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
发明人： Feng Cao , Kwok Chan , Erik Hagberg , Farid Khouri , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
IPC分类号： C08K9/04
CPC分类号： C08F2/44
摘要： In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition comprising (a) contacting under condensation polymerization conditions a first monomer, a second monomer, a solvent, and an organoclay composition, said organoclay composition comprising alternating inorganic silicate layers and organic layers, to provide a first polymerization reaction mixture, wherein one of said first monomer and second monomers is a diamine and the other is an dianhydride; (b) carrying out a stoichiometry verification step on the first polymerization reaction mixture; (c) optionally adding additional reactant (monomer 1, monomer 2, or chainstopper) to the first polymerization reaction mixture to provide a second polymerization reaction mixture; and (d) removing solvent from the first polymerization reaction mixture or the second polymerization reaction mixture to provide a first polymer-organoclay composite composition comprising a polymer component and an organoclay component wherein the organoclay component is at least 10% exfoliated.
摘要翻译：在一个实施方案中，本发明提供制备聚合物 - 有机粘土复合组合物的方法，其包含（a）在缩聚条件下使第一单体，第二单体，溶剂和有机粘土组合物接触，所述有机粘土组合物包含交替的无机硅酸盐层和有机层，以提供第一聚合反应混合物，其中所述第一单体和第二单体之一是二胺，另一个是二酐; （b）在第一聚合反应混合物上进行化学计量验证步骤; （c）任选地向第一聚合反应混合物中加入另外的反应物（单体1，单体2或链截止剂）以提供第二聚合反应混合物; 和（d）从第一聚合反应混合物或第二聚合反应混合物中除去溶剂以提供包含聚合物组分和有机粘土组分的第一聚合物 - 有机粘土复合组合物，其中有机粘土组分至少10％剥离。

2. 发明申请

US20070299188A1 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：US20070299188A1
公开(公告)日：2007-12-27
申请号：US11766423
申请日：2007-06-21
申请人： Kwok Chan , Erik Hagberg , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
发明人： Kwok Chan , Erik Hagberg , Tara Mullen , Roy Odle , James White , Norimitsu Yamaguchi
IPC分类号： C08K9/04 , C08K5/50
CPC分类号： C08J3/201 , B82Y30/00 , C01B33/44 , C08J5/005 , C08K3/346 , C08K5/50 , C08K9/04
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition, said method comprising melt mixing a quaternary organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary organic cation with a polymeric resin comprising at least one polymer selected from the group consisting of polyamides, polyesters, polyarylene sulfides, polyarylene ethers, polyether sulfones, polyether ketones, polyether ether ketones, polyphenylenes, and polycarbonates, said polymeric resin being substantially free of polyetherimides; said melt mixing being carried out at a temperature in a range between about 300° C. and about 450° C. to provide a polymer-organoclay composite composition, said polymer-organoclay composite composition being characterized by a percent exfoliation of at least 10 percent.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了制备聚合物 - 有机粘土复合材料组合物的方法，所述方法包括熔融混合包含交替的无机硅酸盐层和有机层的季有机粘土组合物，所述有机层包含季铵有机阳离子与聚合树脂，选自聚酰胺，聚酯，聚亚芳基硫醚，聚亚芳基醚，聚醚砜，聚醚酮，聚醚醚酮，聚苯基和聚碳酸酯的至少一种聚合物，所述聚合物树脂基本上不含聚醚酰亚胺; 所述熔体混合在约300℃至约450℃之间的温度下进行，以提供聚合物 - 有机粘土复合材料组合物，所述聚合物 - 有机粘土复合组合物的特征在于至少10％的剥离百分比。

3. 发明申请

US20080004391A1 METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 失效
标题翻译：制备聚合物 - 组织复合材料的方法及其衍生物
公开(公告)号：US20080004391A1
公开(公告)日：2008-01-03
申请号：US11766456
申请日：2007-06-21
申请人： Kwok Chan , Sarah Genovese , Erik Hagberg , David Hall , John Maxam , Tara Mullen , Roy Odle , Albert Stella , James White
发明人： Kwok Chan , Sarah Genovese , Erik Hagberg , David Hall , John Maxam , Tara Mullen , Roy Odle , Albert Stella , James White
IPC分类号： C08K9/04
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：一种制备聚合物 - 有机粘土复合材料组合物的方法，包括将溶剂和未剥离的有机粘土组合以提供第一混合物，其中未剥离的有机粘土包含交替的无机硅酸盐层和有机层，并且在硅酸盐层之间具有初始间隔; 将第一混合物暴露于足够强度和持续时间的通电状态以增加无机硅酸盐层的初始间隔，以提供第二混合物; 使所述第二混合物与聚合物组合物接触，使得所述聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中所述聚合物组合物至少部分地可溶于所述溶剂中; 以及从所述第二混合物中除去至少一部分所述溶剂，其中在去除所述溶剂之后，所述无机硅酸盐层保持被所述聚合物分离。

4. 发明申请

US20070299187A1 COMPOSITIONS AND METHODS FOR POLYMER COMPOSITES 审中-公开
标题翻译：聚合物复合材料的组合物和方法
公开(公告)号：US20070299187A1
公开(公告)日：2007-12-27
申请号：US11766382
申请日：2007-06-21
申请人： Kwok Chan , Erik Hagberg , John Maxam , Tara Mullen , Roy Odle , James White
发明人： Kwok Chan , Erik Hagberg , John Maxam , Tara Mullen , Roy Odle , James White
IPC分类号： C08K9/04 , C08K5/50
CPC分类号： C08F2/44 , C01P2002/72 , C01P2004/04 , C08K9/04 , C08L79/08 , C09C1/42
摘要： This invention relates to organic salt compositions useful in the preparation of organoclay compositions, polymer-organoclay composite compositions, and methods for the preparation of polymer nanocomposites. In one embodiment, the present invention provides a polymer-organoclay composite composition comprising (a) a polymeric resin; and (b) an organoclay composition comprising alternating inorganic silicate layers and organic layers, said organic layers comprising a quaternary phosphonium cation having structure XXXIII wherein Ar12, Ar13, Ar14 and Ar15 are independently C2-C50 aromatic radicals; and Ar16 is a C2-C200 aromatic radical, or a polymer chain comprising at least one aromatic group.
摘要翻译：本发明涉及可用于制备有机粘土组合物，聚合物 - 有机粘土复合材料组合物和制备聚合物纳米复合材料的方法的有机盐组合物。在一个实施方案中，本发明提供了一种聚合物 - 有机粘土复合材料组合物，其包含（a）聚合物树脂; 和（b）有机粘土组合物，其包含交替的无机硅酸盐层和有机层，所述有机层包含具有结构XXXIII的季鏻阳离子，其中Ar 12，Ar 13，Ar， SUP> 14和Ar 15独立地为C 2 -C 50芳族基团; 和Ar 16是C 2 -C 20芳族基团，或包含至少一个芳族基团的聚合物链。

5. 发明申请

US20080119610A1 METHODS OF MAKING POLYMER BLEND COMPOSITIONS 有权
标题翻译：制备聚合物混合组合物的方法
公开(公告)号：US20080119610A1
公开(公告)日：2008-05-22
申请号：US11562628
申请日：2006-11-22
申请人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
发明人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
IPC分类号： C08G63/91
CPC分类号： C08G73/1007 , C08L67/02 , C08L71/00 , C08L77/00 , C08L79/04 , C08L79/08 , C08L81/06 , C08L85/02 , C08L2666/20 , C08L2666/22 , C08L81/00 , C08L2666/02 , C08L2666/14
摘要： Methods of making miscible and compatible immiscible polymer blends are disclosed. The polymer blends have a polyimide as a component. The miscible polymer blends have a single glass transition temperature. The compatible polymer blends have two glass transition temperatures.
摘要翻译：公开了制备可混溶和相容的不混溶聚合物共混物的方法。聚合物共混物具有聚酰亚胺作为组分。可混溶的聚合物共混物具有单一的玻璃化转变温度。相容的聚合物共混物具有两个玻璃化转变温度。

6. 发明授权

US08399573B2 Polymer blend compositions 有权
公开(公告)号：US08399573B2
公开(公告)日：2013-03-19
申请号：US11562625
申请日：2006-11-22
申请人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
发明人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
IPC分类号： C08L67/00 , C08L71/02 , C08L77/00 , C08L77/12 , C08L79/06 , C08L81/04 , C08L81/06
CPC分类号： C08L79/08 , C08L65/02 , C08L67/02 , C08L77/00 , C08L81/06 , C08L2205/02 , Y10T428/1352 , Y10T428/2913 , C08L2666/20 , C08L2666/18 , C08L2666/14 , C08L2666/02 , C08L81/00 , C08L2666/22
摘要： Thermoplastic compositions having miscible and compatible immiscible polymer blends are disclosed. The miscible polymer blends have a single glass transition temperature. The compatible polymer blends have two glass transition temperatures.

7. 发明授权

US08268934B2 Methods of making polymer blend compositions 有权
标题翻译：制备聚合物共混组合物的方法
公开(公告)号：US08268934B2
公开(公告)日：2012-09-18
申请号：US11562628
申请日：2006-11-22
申请人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
发明人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
IPC分类号： C08L67/00 , C08L71/02 , C08L77/00 , C08L77/12 , C08L79/06 , C08L81/04 , C08L81/06
CPC分类号： C08G73/1007 , C08L67/02 , C08L71/00 , C08L77/00 , C08L79/04 , C08L79/08 , C08L81/06 , C08L85/02 , C08L2666/20 , C08L2666/22 , C08L81/00 , C08L2666/02 , C08L2666/14
摘要： Methods of making miscible and compatible immiscible polymer blends are disclosed. The polymer blends have a polyimide as a component. The miscible polymer blends have a single glass transition temperature. The compatible polymer blends have two glass transition temperatures.
摘要翻译：公开了制备可混溶和相容的不混溶聚合物共混物的方法。聚合物共混物具有聚酰亚胺作为组分。可混溶的聚合物共混物具有单一的玻璃化转变温度。相容的聚合物共混物具有两个玻璃化转变温度。

8. 发明申请

US20080119615A1 POLYMER BLEND COMPOSITIONS 有权
标题翻译：聚合物混合组合物
公开(公告)号：US20080119615A1
公开(公告)日：2008-05-22
申请号：US11562625
申请日：2006-11-22
申请人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
发明人： Robert Russell Gallucci , Tara Mullen , Roy Odle , Kapil Chandrakant Sheth , James M. White
IPC分类号： C08L67/00
CPC分类号： C08L79/08 , C08L65/02 , C08L67/02 , C08L77/00 , C08L81/06 , C08L2205/02 , Y10T428/1352 , Y10T428/2913 , C08L2666/20 , C08L2666/18 , C08L2666/14 , C08L2666/02 , C08L81/00 , C08L2666/22
摘要： Thermoplastic compositions having miscible and compatible immiscible polymer blends are disclosed. The miscible polymer blends have a single glass transition temperature. The compatible polymer blends have two glass transition temperatures.
摘要翻译：公开了具有可混溶和相容的不混溶的聚合物共混物的热塑性组合物。可混溶的聚合物共混物具有单一的玻璃化转变温度。相容的聚合物共混物具有两个玻璃化转变温度。

9. 发明申请

US20060270825A1 Precipitative process to prepare polyimides 有权
公开(公告)号：US20060270825A1
公开(公告)日：2006-11-30
申请号：US11137082
申请日：2005-05-25
申请人： Philip Angermeier , Robert Colborn , Robert Gallucci , Paul Howson , Tara Mullen , Roy Odle , Albert Stella , John Whitney
发明人： Philip Angermeier , Robert Colborn , Robert Gallucci , Paul Howson , Tara Mullen , Roy Odle , Albert Stella , John Whitney
IPC分类号： C08G69/08
CPC分类号： C08G69/28 , C08G69/04
摘要： A process for preparing polyimide resins comprises stirring a diamine and a dianhydride in a solvent to form a slurry; heating the slurry to a temperature sufficient for the diamine and dianhydride to react wherein the temperature is below the melting point of the dianhydride, below the melting point of the diamine, or below the melting points of the dianhydride and diamine; and reacting the diamine and dianhydride to form a polyimide having sufficient molecular weight to precipitate from the solvent.

10. 发明申请

US20090258991A1 Polyetherimide and Polyetherimide Sulfone Blends Having Automotive Lighting Applications 有权
标题翻译：具有汽车照明应用的聚醚酰亚胺和聚醚酰亚胺砜共混物
公开(公告)号：US20090258991A1
公开(公告)日：2009-10-15
申请号：US12347542
申请日：2008-12-31
申请人： Norimitsu Yamaguchi , Roy Odle , Sanjay Mishra
发明人： Norimitsu Yamaguchi , Roy Odle , Sanjay Mishra
IPC分类号： C08L77/00
CPC分类号： C08L79/08 , C08L2205/02 , Y10T428/3163 , Y10T428/31681 , Y10T428/31721 , C08L2666/20
摘要： Compositions and articles of manufacture made therefrom for use in high temperature application, such as automotive reflectors, have a minimum haze onset temperature of about 205° C. and are made from a transparent, miscible blend of from about 30 to about 70 weight percent of a polyetherimide sulfone comprising greater than or equal to 50 mole percent of the polymer linkages have an aryl sulfone group and from about 70 to about 30 weight percent of a polyetherimide or polyimide.
摘要翻译：由用于高温应用的组合物和制品，例如汽车反射器，具有约205℃的最小雾度起始温度，并且由透明的，可混溶的约30至约70重量％的共混物制成包含大于或等于50摩尔％的聚合物键的聚醚酰亚胺砜具有芳基砜基团和约70至约30重量％的聚醚酰亚胺或聚酰亚胺。

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