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    • 4. 发明专利
    • Bonzotriazole compound, pigment microparticle, pigment microparticle dispersion, and near-infrared-absorbing material containing the pigment microparticle
    • BONZOTRIAZOLE化合物,颜料微粒,颜料微粒分散体和含有色素微粒的近红外吸收材料
    • JP2008105958A
    • 2008-05-08
    • JP2006287501
    • 2006-10-23
    • Fujifilm Corp富士フイルム株式会社
    • KIMURA KEIZOMASAKI TOMOHITOUCHIDA OSAMUYAMAKAWA KAZUYOSHI
    • C07D249/20C09B67/20C09B67/46G02B5/22
    • PROBLEM TO BE SOLVED: To provide a novel vinylethynylarylcarboxylic acid compound useful as an intermediate for pharmaceuticals and agrichemicals and as a raw material for functional materials such as liquid crystal and electronic materials and high-durability resins, to provide a production method capable of stably obtaining the compound in a high-purity form, and to provide a thermally crosslinkable compound made from the compound. SOLUTION: The benzotriazole compound is represented by formula (I). In formula (I), R 11 to R 19 are each independently a hydrogen atom or a substituent; provided that at least one of them is a substituent represented by formula (II), and the total number of carbon atoms constituting the substituents other than the substituent represented by formula (II) is 8 or larger. In formula (II), X 11 is SO 2 -O or CO-O and M 11 is a hydrogen atom or an n 11 -valent metal atom; and n 11 is an integer of 1-6. COPYRIGHT: (C)2008,JPO&INPIT
    • 待解决的问题:提供一种用作药物和农药中间体的新型乙烯基乙炔基芳基羧酸化合物,以及作为液晶和电子材料等功能材料和高耐久性树脂的原料,提供一种能够 稳定地获得高纯度形式的化合物,并提供由该化合物制成的热交联性化合物。 解决方案:苯并三唑化合物由式(I)表示。 在式(I)中,R 11和R 16各自独立地为氢原子或取代基; 条件是它们中的至少一个是由式(II)表示的取代基,构成除式(II)表示的取代基以外的取代基的碳原子总数为8以上。 在式(II)中,X 11 为SO 2,或者CO-O,M 11为氢原子或n 11价金属原子; 并且n 11 是1-6的整数。 版权所有(C)2008,JPO&INPIT
    • 5. 发明专利
    • Method for preparing near infrared ray absorption coloring matter compound
    • 用于制备近红外辐射吸收颜料的化合物的方法
    • JP2007070476A
    • 2007-03-22
    • JP2005259243
    • 2005-09-07
    • Fujifilm Corp富士フイルム株式会社
    • KIMURA KEIZOMASAKI TOMOHITOYAMAKAWA KAZUYOSHI
    • C09B53/00C09K3/00
    • C07C249/02C09B57/008C07C251/22C07C251/30
    • PROBLEM TO BE SOLVED: To provide a method for preparing a near infrared ray absorption coloring matter compound useful as an image-forming material, an infrared ray heat sensitive type recording material, an optical recording device, an optical film material and the like, particularly an aminium salt and a diimonium salt at a low cost with ease in high yield.
      SOLUTION: The method for preparing a near infrared ray absorption cloring matter compound comprises a step of reacting a compound represented by formula (I) (wherein R
      111 , R
      112 , R
      121 , R
      122 , R
      131 , R
      132 , R
      141 , and R
      142 are each independently hydrogen, an aliphatic group or an aromatic group; n
      103 , n
      113 , n
      123 , n
      133 , and n
      143 are each independently a substituent; and n
      103 , n
      113 , n
      123 , n
      133 , and n
      143 are each independently an integer of 0-4) with a halogenating agent.
      COPYRIGHT: (C)2007,JPO&INPIT
    • 要解决的问题:提供一种制备用作成像材料的近红外线吸收色素化合物的方法,红外线热敏型记录材料,光学记录装置,光学膜材料和 特别是铵盐和二亚铵盐,成本低廉,产率高。 解决方案:用于制备近红外线吸收沉淀物质化合物的方法包括使式(I)表示的化合物(其中R 111 ,R 112 ,R 121 ,R 122 ,R< SP> 131< SP> >和R 142 各自独立地为氢,脂族基团或芳族基团; n 103 ,n 123 ,n 133 和n 143 各自独立地为取代基; n 103 >,n 123 ,n 133 和n 各自独立地为0-4的整数)与卤化剂。 版权所有(C)2007,JPO&INPIT
    • 6. 发明专利
    • Method of production of azo compound
    • 制备AZO化合物的方法
    • JP2010248290A
    • 2010-11-04
    • JP2009096225
    • 2009-04-10
    • Fujifilm Corp富士フイルム株式会社
    • MASAKI TOMOHITOGOTO TAKEOGOTO HARUYOSHI
    • C09B29/50C07B61/00
    • PROBLEM TO BE SOLVED: To provide a method of producing an azo compound represented by formula (III) by stabilizing a diazonium salt.
      SOLUTION: This method of producing an azo compound comprises: subjecting an amino group of a diazole derivative having the amino group as a substituent to a diazotization reaction to convert the diazole derivative into a corresponding diazonium salt compound; and reacting the compound with a pyrazolone compound in the presence of an acid having pKa of 3 or less to obtain a compound represented by formula (III), where R
      1 , R
      2 , R
      3 , R
      4 , and R
      5 individually represent a substituent.
      COPYRIGHT: (C)2011,JPO&INPIT
    • 待解决的问题:提供通过稳定重氮盐来制备由式(III)表示的偶氮化合物的方法。 解决方案:这种制备偶氮化合物的方法包括:将具有氨基的二唑衍生物的氨基作为取代基进行重氮化反应,将二唑衍生物转化成相应的重氮盐化合物; 并在pKa为3以下的酸的存在下,使该化合物与吡唑啉酮化合物反应,得到式(III)所示的化合物,式中,R 1, >,R 3 ,R 4 和R 5 分别表示取代基。 版权所有(C)2011,JPO&INPIT
    • 10. 发明专利
    • Method for producing 2,6-diaminopyridine compound
    • 2,6-二氨基吡啶化合物的制备方法
    • JP2010235527A
    • 2010-10-21
    • JP2009086113
    • 2009-03-31
    • Fujifilm Corp富士フイルム株式会社
    • MASAKI TOMOHITO
    • C07D213/85B01J21/10B01J23/06C07B61/00
    • C07D213/85
    • PROBLEM TO BE SOLVED: To provide a method capable of producing a 2,6-diaminopyridine compound under mild reaction conditions.
      SOLUTION: The method for producing a 2,6-diaminopyridine compound represented by formula (III) includes reacting a compound such as dibutylamine with a compound such as 2,6-dichloro-3-cyano-4-methylpyridine in the presence of a metal catalyst. In formula (III), R
      11 , R
      12 , and R
      13 , which are each independently a hydrogen atom or a substituent; X is a leaving group; R
      1 and R
      2 are each independently a hydrogen atom, an aliphatic group, an aromatic group, or a heterocyclic group; provided that these groups may be further substituted, and R
      1 and R
      2 may be bonded together to form a nitrogen-containing ring.
      COPYRIGHT: (C)2011,JPO&INPIT
    • 待解决的问题:提供一种能够在温和的反应条件下生产2,6-二氨基吡啶化合物的方法。 解决方案:由式(III)表示的2,6-二氨基吡啶化合物的制备方法包括使化合物如二丁胺与2,6-二氯-3-氰基-4-甲基吡啶等化合物在存在下反应 的金属催化剂。 在式(III)中,R 11和R 12各自独立地为氢原子或取代基; X是离职团体 R 1 和R 2 各自独立地为氢原子,脂族基团,芳族基团或杂环基团; 条件是这些基团可以进一步被取代,并且R 1和R 2彼此可以结合在一起形成含氮环。 版权所有(C)2011,JPO&INPIT