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    • 7. 发明申请
    • EXFOLIATION OF LAYERED MATERIALS BY WET-JET MILLING TECHNIQUES
    • 采用湿法喷射技术去除层状材料
    • WO2017089987A1
    • 2017-06-01
    • PCT/IB2016/057108
    • 2016-11-24
    • FONDAZIONE ISTITUTO ITALIANO DI TECNOLOGIA
    • DEL RIO CASTILLO, Antonio EsauANSALDO, AlbertoPELLEGRINI, VittorioBONACCORSO, Francesco
    • C01B32/20C01B21/064C01G39/06C01G41/00C01B19/00
    • C01B32/19C01B19/007C01B21/0648C01G39/06C01G41/00C01P2002/82C01P2004/04
    • A system for the exfoliation of a layered material is described, comprising in combination: an exfoliation station (14-22) operating on a volume of a dispersion of a layered precursor material, including a wet-jet milling device (10); and a collecting station (30, 40), located downstream of the exfoliation station (14-22), operating on a volume of a dispersion of the at least partly exfoliated material, in which the exfoliation station (14-22) and the collecting station (30, 40) are connected to each other through a fluid communication path (20) along which there are interposed flow regulating means (50) adapted to assume a first operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is discontinued, where the exfoliation station (14-22) is adapted to subject a volume of dispersion of layered precursor material to a predetermined number of wet-jet milling cycles; and a second operating configuration in which the communication path (20) between the exfoliation station (14-22) and the collecting station (30, 40) is continuous, where the exfoliation station (14-22) is adapted to convey a volume of previously milled dispersion including at least partly exfoliated material to the collecting station (30, 40) and is placed in communication with a supply chamber (12) to be fed with a further volume of a dispersion of layered precursor material that has to be exfoliated.
    • 描述了一种用于层状材料的剥落的系统,其包括以下组合:在一定体积的分层前体材料的分散体上操作的剥离台(14-22),其包括湿喷射 铣削装置(10); 和位于所述剥落台(14-22)下游的收集台(30,40),所述收集台在所述至少部分剥落的材料的一定体积的分散体上操作,其中所述剥离台(14-22)和所述收集台 (30,40)通过流体连通路径(20)相互连接,沿着流体连通路径插入有流动调节装置(50),该流动调节装置适于采取第一操作配置,其中在剥离站(30,40)之间的连通路径(20) 剥离台(14-22)适于使层状前体材料的一定体积的分散体经受预定数量的湿式喷射研磨循环;其中,剥离台(14-22) 和第二操作配置,其中剥落台(14-22)和收集台(30,40)之间的通信路径(20)是连续的,其中剥离台(14-22)适于传送一定体积的 预先研磨的分散体,其包括至少部分剥落的材料到收集站(30,40)并且与供应腔室(12)连通以供应另一体积的必须剥落的分层前体材料的分散体。