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1. 发明申请

WO2020261217A1 MIXTURE CONTAINING CALIXARENES, PROCESS FOR THE PRODUCTION THEREOF AND USE THEREOF FOR PREPARING DETERGENT COMPOSITIONS FOR LUBRICANTS 审中-公开
公开(公告)号：WO2020261217A1
公开(公告)日：2020-12-30
申请号：PCT/IB2020/056083
申请日：2020-06-26
申请人： ENI S.P.A.
发明人： NOTARI, Marcello , ASSANELLI, Giulio , CASNATI, Alessandro , SANSONE, Francesco , MAGINI, Andrea
IPC分类号： C10M159/22 , C11D3/00 , C10N10/04 , C10N20/02 , C10N30/02 , C10N30/04 , C10N30/00 , C10N40/25
摘要： The present invention relates to mixtures containing calixarenes of formula (I) with a reduced alkyl phenol and linear oligomer content and the preparation process thereof, wherein: a. R is selected between a linear or branched alkyl having a number of carbon atoms comprised between 4 and 40, more preferably between 4 and 24, even more preferably comprised between 8 and 18; b. n is the number of units of the calixarene cycle and is comprised in the range from 4 to 16, preferably between 4 and 12. Furthermore, the present invention relates to detergent compositions containing overbased metal salts of calixarenes, the preparation process thereof and the use thereof in lubricant compositions.

2. 发明申请

WO2014125416A1 INTEGRATED PROCESS FOR THE PREPARATION OF COMPOUNDS USEFUL AS FUEL COMPONENTS 审中-公开
标题翻译：用于制备作为燃料组分的化合物的综合方法
公开(公告)号：WO2014125416A1
公开(公告)日：2014-08-21
申请号：PCT/IB2014/058912
申请日：2014-02-11
申请人： ENI S.P.A.
发明人： BELLUSSI, Giuseppe , DE ANGELIS, Alberto, Renato , ASSANELLI, Giulio , POLLESEL, Paolo
IPC分类号： C10L1/02 , C10L1/185
CPC分类号： C10L1/18 , C07C29/60 , C07C41/09 , C07C45/52 , C07C67/44 , C07D317/22 , C10L1/02 , C10L1/023 , C10L1/026 , C10L1/1855 , C10L1/19 , C10L10/02 , C10L10/04 , C10L10/10 , C10L10/12 , C10L10/16 , C10L2200/0469 , C10L2270/023 , C10L2270/026 , Y02P20/125 , C07C43/13 , C07C31/205 , C07C47/02 , C07C69/24
摘要： The invention relates to an integrated process for the production of fuel components starting from materials of a biological origin which comprises: (A) transformation of glycerine into an alkoxy- propanediol having formula RO-CH 2 -CHOH-CH 2 OH, wherein R is a linear or branched C 1 -C 8 alkyl, (B) transformation of glycerine into 1, 2-propanediol CH 3 -CHOH-CH 2 OH, (C) dehydration of the 1, 2-propanediol obtained in (B) to propionic aldehyde, (D) reaction of part of the propionic aldehyde obtained in (C) with the alkoxy-propanediol having formula RO-CH 2 -CHOH-CH 2 OH obtained in (A) to give an acetal having formula (a) wherein R is a linear or branched C 1 -C 8 alkyl, (E) transformation of part of the propionic aldehyde obtained in (C) to a propionate having formula CH 3 -CH 2 -COOR ', wherein R' is a linear or branched C 1 -C 8 alkyl. Particular components for gasolines and/or diesel are also described.
摘要翻译：本发明涉及从生物来源的材料开始生产燃料成分的综合方法，其包括：（A）将甘油转化为具有式RO-CH 2 -CHOH-CH 2 OH的烷氧基丙二醇，其中R是直链或（B）将甘油转化为1,2-丙二醇CH 3 -CHOH-CH 2 OH，（C）将（B）中得到的1,2-丙二醇脱水为丙醛，（D）将部分（C）中得到的丙醛与式（A）中得到的具有式RO-CH2-CHOH-CH2OH的烷氧基 - 丙二醇反应得到式（a）的缩醛，其中R是直链或支链C 1 -C 8烷基（ E）将（C）中得到的丙醛的一部分转化为具有式CH 3 -CH 2 -COROR'的丙酸酯，其中R'是直链或支链C 1 -C 8烷基。还描述了汽油和/或柴油的特定组分。

3. 发明申请

WO2013046132A1 PROCESS FOR THE PREPARATION OF DIALKYL CARBONATE COMPOUNDS 审中-公开
标题翻译：制备碳酸二乙酯化合物的方法
公开(公告)号：WO2013046132A1
公开(公告)日：2013-04-04
申请号：PCT/IB2012/055124
申请日：2012-09-26
申请人： ENI S.P.A
发明人： DE ANGELIS, Alberto Renato , RIZZO, Caterina , ASSANELLI, Giulio
IPC分类号： C07C68/06 , C07C69/96 , C07D317/38 , C07D317/36 , B01J23/00 , B01J27/236
CPC分类号： C07C68/065 , B01J23/007 , B01J27/236 , C07D317/36 , C07D317/38 , C07C69/96
摘要： The present invention relates to a process for the preparation of dialkyl carbonate compounds starting from urea and reagents selected from ethylene glycol and propylene glycol. Said process comprises the following steps: • carrying out a glycolysis reaction, in the presence of a first catalyst in heterogeneous phase, between urea and a reagent selected from ethylene glycol, propylene glycol and linear alcohols with a number of carbon atoms in the chain ranging from 1 to 20, so as to form an alkenyl carbonate; • carrying out a transesterification reaction, in the presence of a second catalyst in heterogeneous phase, between the alkenyl carbonate thus obtained and an aliphatic alcohol having a number of carbon atoms within the range of 1-22, so as to form dialkyl carbonate compounds.
摘要翻译：本发明涉及从尿素和选自乙二醇和丙二醇的试剂制备碳酸二烷基酯化合物的方法。所述方法包括以下步骤：在非均相阶段的第一催化剂存在下，尿素与选自乙二醇，丙二醇和链中碳原子数为1〜20的直链醇的试剂进行糖酵解反应，从而进行糖酵解反应形成烯基碳酸酯; 。在非均相中的第二催化剂的存在下进行酯交换反应，在如此获得的链烯基碳酸酯与碳原子数为1-22的脂族醇之间进行酯交换反应，以形成碳酸二烷基酯化合物。

4. 发明申请

WO2022043891A1 FRICTION REDUCING ADDITIVES AND PROCESS FOR PREPARING THE SAME 审中-公开
公开(公告)号：WO2022043891A1
公开(公告)日：2022-03-03
申请号：PCT/IB2021/057788
申请日：2021-08-25
申请人： ENI S.P.A.
发明人： ASSANELLI, Giulio , NOTARI, Marcello , CAMBISE, Paolo , PUCCI, Andrea , IASILLI, Giuseppe
IPC分类号： C10L1/22 , C10L10/08 , C10M133/00 , C10M133/02 , C10L1/222 , C10L1/224 , C10L1/233 , C10N20/00 , C10N30/06 , C10N30/00 , C10N40/04 , C10N40/25
摘要： A friction reducing additive is described formed by a mixture that can be obtained by autocatalytic condensation reaction of fatty acids with alkanolamines, said mixture comprising an amide, one or more esters of carboxylic acids, and an oxazoline in an amount greater than 7% by weight with respect to the total weight of the mixture, wherein said additive can be used both in lubricants and in fuels.

5. 发明申请

WO2015107487A1 PROCESS FOR THE PRODUCTION OF HYDROCARBON FRACTIONS FROM MIXTURES OF A BIOLOGICAL ORIGIN 审中-公开
标题翻译：生物原料混合物生产烃类的方法
公开(公告)号：WO2015107487A1
公开(公告)日：2015-07-23
申请号：PCT/IB2015/050336
申请日：2015-01-16
申请人： ENI S.P.A.
发明人： BELLUSSI, Giuseppe , MOLINARI, Daniele , ASSANELLI, Giulio , DE ANGELIS, Alberto Renato
IPC分类号： C10G45/58 , C10G3/00 , C07C1/20 , C11B3/00 , C11C3/12
CPC分类号： C10G3/50 , C10G45/58 , C11C1/04 , C11C1/08 , C11C1/10 , C11C3/003 , C11C3/12 , C11C3/14 , Y02E50/13 , Y02P30/20
摘要： A process is described for the production of hydrocarbon fractions which can be used as diesel fuel or as components of diesel fuel, starting from a mixture of a biological origin containing fatty acid esters with glycerine, and possibly containing aliquots of free fatty acids and/or phosphoglycerides, wherein said process comprises the following steps: - subjecting the mixture of a biological origin to hydrolysis, obtaining a mixture containing glycerine and a mixture of fatty acids, - neutralizing the mixture of fatty acids with ammonia, - subjecting the neutralized mixture to hydrodeoxygenation, - subjecting the mixture resulting from the hydrodeoxygenation to hydroisomerization. The process of the present invention allows the triglycerides. This aspect, in addition to allowing the recovery of glycerine, which can be used as precursor of fuel components, allows the hydrogen consumption to be avoided in the hydrodeoxygenation step, which occurs when glycerine is present and therefore undergoes reduction to propane. Furthermore, if the mixture of a biological origin also contains aliquots of free fatty acids, the process of the invention also avoids problems of corrosion due to said acids, during the hydrodeoxygenation treatment.
摘要翻译：描述了用于生产可用作柴油燃料或作为柴油燃料成分的烃馏分的方法，其起始于含有脂肪酸酯与甘油的生物来源的混合物，并且可能含有等分的游离脂肪酸和/或磷酸甘油酯，其中所述方法包括以下步骤： - 使生物来源的混合物进行水解，得到含有甘油和脂肪酸混合物的混合物， - 中和脂肪酸混合物与氨， - 将中和的混合物进行加氢脱氧将由加氢脱氧产生的混合物进行加氢异构化。本发明的方法允许甘油三酸酯。除了允许可用作燃料成分前体的甘油的回收之外，这一方面允许在加氢脱氧步骤中避免氢消耗，当甘油存在并因此经历还原成丙烷时，可以避免氢消耗。此外，如果生物来源的混合物还含有游离脂肪酸的等分试样，则本发明的方法还避免了在加氢脱氧处理期间由于所述酸引起的腐蚀问题。

6. 发明申请

WO2022180521A1 PROCESS FOR PREPARING AN ANTIMICROBIAL COATING COMPOSITION, ANTIMICROBIAL COATING COMPOSITION AND USE THEREOF TO CONFER ANTIMICROBIAL PROPERTIES TO THE SURFACE OF A SUBSTRATE 审中-公开
公开(公告)号：WO2022180521A1
公开(公告)日：2022-09-01
申请号：PCT/IB2022/051568
申请日：2022-02-23
申请人： ENI S.P.A.
发明人： ASSANELLI, Giulio , NOTARI, Marcello , AMICO, Antonio , PO, Riccardo , SERBOLISCA, Luca
IPC分类号： C09D5/16 , C09D5/00
摘要： The present invention relates to a process for preparing an antimicrobial coating composition comprising the following steps: a. providing an aqueous dispersion comprising graphite, at least one oxidizing agent and optionally at least one antimicrobial agent; b. subjecting the aqueous dispersion from step a to high shear homogenization mixing said dispersion at a mixing speed equal to or greater than 1000 rpm, to obtain an antibacterial aqueous dispersion comprising graphene oxide; c. mixing the aqueous antimicrobial dispersion with at least one film-forming agent to obtain the antimicrobial coating composition. The invention further relates to the composition obtainable by the above process and use thereof to impart antimicrobial properties to the surface of a substrate.

7. 发明申请

WO2016185392A1 PROCESS AND APPARATUS FOR THE PRODUCTION OF ALDEHYDES STARTING FROM 1,2-DIOLS 审中-公开
标题翻译：用于生产从1,2-二醇开始的醛类的方法和装置
公开(公告)号：WO2016185392A1
公开(公告)日：2016-11-24
申请号：PCT/IB2016/052888
申请日：2016-05-18
申请人： ENI S.P.A.
发明人： ASSANELLI, Giulio , CALEMMA, Vincenzo , DE ANGELIS, Alberto Renato , GAMBAROTTA, Enrico Francesco , MOLINARI, Daniele
IPC分类号： C07C45/59 , C07C47/02 , C07D317/12 , C07C45/57 , B01J19/18 , B01J19/24
CPC分类号： B01J8/0442 , B01J8/0496 , B01J8/26 , B01J2208/00176 , B01J2208/003 , C07C45/59 , C07C45/82 , C07D317/12 , C07C47/02
摘要： The present invention relates to a process for preparing aliphatic aldehydes starting from 1,2-diols. Said aldehydes can be advantageously used for the synthesis of fuel components. In particular, the present invention relates to a process wherein said aldehydes can be produced starting from 1,2-diol intermediates of a biological origin. In addition, the present invention relates to an apparatus for performing said process for preparing aliphatic aldehydes starting from 1,2-diols.
摘要翻译：本发明涉及从1,2-二醇开始制备脂族醛的方法。所述醛可有利地用于燃料组分的合成。特别地，本发明涉及一种方法，其中所述醛可以从生物来源的1,2-二醇中间体开始制备。此外，本发明涉及一种用于从1,2-二醇开始制备脂族醛的方法的装置。

8. 发明申请

WO2022180524A1 GRAPHENE OXIDE HAVING ANTIMICROBIAL PROPERTIES, PREPARATION PROCESS AND USE THEREOF TO CONFER ANTIMICROBIAL PROPERTIES TO RUBBER ARTICLES 审中-公开
公开(公告)号：WO2022180524A1
公开(公告)日：2022-09-01
申请号：PCT/IB2022/051572
申请日：2022-02-23
申请人： ENI S.P.A.
发明人： ASSANELLI, Giulio , NOTARI, Marcello , SERBOLISCA, Luca , GALIMBERTI, Maurizio Stefano , CANDIANI, Gabriele
IPC分类号： C01B32/198
摘要： The present invention relates to a process for preparing graphene oxide which comprises subjecting an aqueous dispersion of a graphite to an exfoliation step by high shear mixing at a mixing speed equal to or greater than 3000 rpm and to an oxidation step with an oxidizing agent selected from hydrogen peroxide, potassium hydroxide and mixtures thereof, wherein the graphite exfoliation step can precede, follow or be conducted together with the oxidation step. The invention also relates to the use of the graphene oxide thus obtained to impart antimicrobial properties to rubber articles.

9. 发明申请

WO2018178130A1 INTEGRATED PROCESS FOR THE PRODUCTION OF FUEL COMPONENTS FROM GLYCERIN 审中-公开
公开(公告)号：WO2018178130A1
公开(公告)日：2018-10-04
申请号：PCT/EP2018/057870
申请日：2018-03-28
申请人： ENI S.P.A.
发明人： CALEMMA, Vincenzo , ASSANELLI, Giulio
IPC分类号： C07D317/22 , C10L1/185 , C10L1/02
CPC分类号： C07D317/22 , C10L1/02 , C10L1/1855 , C10L2200/0446 , Y02P20/125 , Y02P20/582
摘要： The present invention relates to a versatile process for the simultaneous production of biocomponents for fuels such as gasoline and diesel, essentially starting from glycerol of biological origin only, comprising a multiplicity of interconnected steps related to hydrogenation, condensation and etherification.

10. 发明申请

WO2015181749A1 PROCESS FOR PRODUCING A DIESEL HYDROCARBON FRACTION STARTING FROM A RENEWABLE FEEDSTOCK 审中-公开
标题翻译：生产从可再生饲料开始的柴油机油分离方法
公开(公告)号：WO2015181749A1
公开(公告)日：2015-12-03
申请号：PCT/IB2015/053977
申请日：2015-05-27
申请人： ENI S.P.A.
发明人： CALEMMA, Vincenzo , DE ANGELIS, Alberto Renato , ASSANELLI, Giulio
IPC分类号： C11B7/00 , C11C1/00 , C10G45/02 , C10G45/06 , C10G45/12 , C10G45/58 , C10G45/62 , C10G45/64 , C10G3/00 , C11B3/06 , C11B13/00
CPC分类号： C10G45/02 , C10G3/42 , C10G3/50 , C10G45/06 , C10G45/12 , C10G45/58 , C10G45/62 , C10G45/64 , C10G2300/1011 , C10G2300/1014 , C10G2400/04 , C11C1/04 , C11C3/00 , Y02E50/13 , Y02P30/20
摘要： The present invention relates to a process for preparing a diesel hydrocarbon fraction, comprising the following steps: (a) reacting at least a renewable feedstock comprising glycerides with water at a temperature within the range of 150–400°C and a pressure within the range of 1-20 MPa, forming at least one mixture of fatty acids and glycerine; (b) separating said glycerine from said mixture of fatty acids; (c) subjecting said mixture of fatty acids to catalytic hydrotreatment in the presence of hydrogen, obtaining a reaction product comprising: (i) at least one gaseous effluent comprising hydrogen, water vapour and CO 2 and possibly CO, (ii) at least one diesel hydrocarbon fraction comprising branched paraffins in a prevalent quantity with respect to the linear paraffins, said catalytic hydrotreatment being carried out in the presence of a catalytic composition comprising at least one metal of group VIIIB dispersed on at least one acid carrier for catalyzing a hydroisomerization reaction of linear paraffins to branched paraffins; (d) separating said diesel hydrocarbon fraction from said reaction product.
摘要翻译：本发明涉及一种制备柴油烃馏分的方法，包括以下步骤：（a）使至少包含甘油酯的可再生原料与水在150-400℃范围内的温度和在该范围内的压力下反应 1-20MPa，形成脂肪酸和甘油的至少一种混合物; （b）从所述脂肪酸混合物中分离出所述甘油; （c）使所述脂肪酸混合物在氢的存在下进行催化加氢处理，得到反应产物，其包含：（i）至少一种气态流出物，其包含氢气，水蒸汽和CO 2以及可能的CO，（ii）至少一种柴油所述催化加氢处理是在催化剂组合物存在下进行的，所述催化剂组合物包含至少一种分散在至少一种酸性载体上的ⅦB族金属的催化剂组合物，用于催化加氢异构化反应直链烷烃至支链烷烃; （d）从所述反应产物中分离所述柴油烃馏分。

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