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1. 发明授权

US06399740B1 Process for reducing mono-functional and non-functional by-products during aralkylation of phenolics 失效
标题翻译：在酚醛芳族化合反应中降低单功能和非功能性副产物的方法
公开(公告)号：US06399740B1
公开(公告)日：2002-06-04
申请号：US09347265
申请日：1999-07-06
申请人： Edward Lucas, Jr. , David A. Hutchings , Rajan Hariharan , Syed A. Elahi , David J. Bir
发明人： Edward Lucas, Jr. , David A. Hutchings , Rajan Hariharan , Syed A. Elahi , David J. Bir
IPC分类号： C08G6378
CPC分类号： C08G61/02
摘要： Phenol aralkyistion polymers can be prepared by reaction among a phenolic monomer, at least one styrenic monomer and an aryl diolefin. A phenolic monomer can be initially aralkylated in the presence of an acid catalyst with a first portion of at least one styrenic monomer to obtain an aralkylated phenol. The aralkylated phenol thereafter can be reacted with an aryl diolefin to obtain a phenol aralkylation polymer. Optionally, (though preferably) the phenol aralkylation polymer is further aralkylated with a second portion of at least one styrenic monomer. By employing specific catalyst concentrations, reactant concentrations, reaction temperatures, and reaction times, the formation of mono-functional and non-functional by-products is substantially reduced.
摘要翻译：苯酚芳基聚合物可以通过酚单体，至少一种苯乙烯类单体和芳基二烯烃之间的反应来制备。酚类单体最初可以在酸催化剂存在下与第一部分至少一种苯乙烯类单体进行芳烷基化，得到芳烷基化苯酚。其后的芳烷基化苯酚可以与芳基二烯烃反应得到苯酚芳烷基化聚合物。任选地，（尽管优选）苯酚芳烷基化聚合物进一步用至少一种苯乙烯类单体的第二部分进行芳烷基化。通过使用特定的催化剂浓度，反应物浓度，反应温度和反应时间，单功能和非功能副产物的形成显着降低。

2. 发明授权

US5770750A Alkyd and aralkyd derivatives of phenolic polymers 失效
标题翻译：酚醛聚合物的醇酸和芳烃衍生物
公开(公告)号：US5770750A
公开(公告)日：1998-06-23
申请号：US781669
申请日：1997-01-10
申请人： David A. Hutchings , Rajan Hariharan , Edward Lucas, Jr. , Syed A. Elahi , Alan K. Randall , Kenneth Bourlier
发明人： David A. Hutchings , Rajan Hariharan , Edward Lucas, Jr. , Syed A. Elahi , Alan K. Randall , Kenneth Bourlier
IPC分类号： C07D317/36 , C07C69/52 , C07C69/54 , C07C233/00 , C07C271/00 , C08G61/10 , C09D163/00 , C09D165/00 , C09D175/04 , C07C53/00
CPC分类号： C07C69/54 , C07C69/52
摘要： Phenolic aralkylation polymers modified by esterification with fatty acids, transesterification with glyceride oils, or other modifications to reactive hydroxyl moieties to improve the characteristics and properties of coating systems in which the modified materials are incorporated. At least a portion of the hydroxyl moieties of the polyol is esterified or otherwise modified. The hydroxyl moieties include those that have been "chain-extended," if desired.
摘要翻译：通过用脂肪酸酯化改性的酚芳基烷基化聚合物，与甘油酯油的酯交换或对反应性羟基部分的其它改性，以改善其中掺入改性材料的涂料体系的特性和性质。多元醇的羟基部分的至少一部分被酯化或以其它方式改性。如果需要，羟基部分包括那些被“链延长”的部分。

3. 发明授权

US06291077B1 Lactone chain-extended phenolic polyester polyols 失效
标题翻译：内酯链延伸酚醛聚酯多元醇
公开(公告)号：US06291077B1
公开(公告)日：2001-09-18
申请号：US09649002
申请日：2000-08-28
申请人： Rajan Hariharan , David A. Hutchings , Kenneth A. Bourlier , Ellen V. Nagy
发明人： Rajan Hariharan , David A. Hutchings , Kenneth A. Bourlier , Ellen V. Nagy
IPC分类号： B32B2706
CPC分类号： C08G18/4277 , C08F283/00 , C08F283/02 , C08F283/04 , C08G61/02 , C08G69/44 , Y10T428/31786
摘要： A lactone chain-extended polyester polyol of the present invention comprises the reaction product of a lactone and a previously chain-extended phenolic-based hydroxyl compound. The previously chain-extended phenolic-based hydroxyl compound may comprise the reaction product of (i) a lactone or an alkoxylating agent selected from the group consisting of alkylene oxides and alkylene carbonates, and (ii) a phenolic aralkylation polymer comprising the reaction product of a phenolic monomer having at least two free reactive positions; a styrene derivative; and a coupling agent. The previously chain-extended phenolic-based hydroxyl compound also may be chain-extended by reacting with a lactam to produce a lactam chain-extended polyester polyamide. The polyols and polyamides of the present invention provide unique combinations of hard and soft functionalities, which translates into materials exhibiting a unique combination of toughness and hardness. These materials are especially suitable for use in high solids coatings and in the development of resins which can be readily processed into thermoset resins. The materials also may function as compatibilizers for thermoplastics.
摘要翻译：本发明的内酯链延长聚酯多元醇包括内酯与先前扩链的酚基羟基化合物的反应产物。先前扩链的酚基羟基化合物可以包含（i）内酯或选自环氧烷烃和碳酸亚烷基酯的烷氧基化剂的反应产物，和（ii）包含以下的反应产物的酚芳烷基化聚合物：具有至少两个自由反应位置的酚单体; 苯乙烯衍生物; 和偶联剂。先前的链延长的酚基羟基化合物也可以通过与内酰胺反应来产生内酰胺链延长的聚酯聚酰胺来延伸。本发明的多元醇和聚酰胺提供硬和软功能的独特组合，其转化为显示韧性和硬度的独特组合的材料。这些材料特别适用于高固含量涂料和开发可以容易地加工成热固性树脂的树脂。这些材料也可用作热塑性塑料的增容剂。

4. 发明授权

US6166151A Lactone chain-extended phenolic polyester polyols 有权
标题翻译：内酯链延伸酚醛聚酯多元醇
公开(公告)号：US6166151A
公开(公告)日：2000-12-26
申请号：US337496
申请日：1999-06-22
申请人： Rajan Hariharan , David A. Hutchings , Kenneth A. Bourlier , Ellen V. Nagy
发明人： Rajan Hariharan , David A. Hutchings , Kenneth A. Bourlier , Ellen V. Nagy
IPC分类号： C08F283/00 , C08F283/02 , C08F283/04 , C08G18/42 , C08G61/02 , C08G69/44
CPC分类号： C08G18/4277 , C08F283/00 , C08F283/02 , C08F283/04 , C08G61/02 , C08G69/44 , Y10T428/31786
摘要： A lactone chain-extended polyester polyol of the present invention comprises the reaction product of a lactone and a previously chain-extended phenolic-based hydroxyl compound. The previously chain-extended phenolic-based hydroxyl compound may comprise the reaction product of (i) a lactone or an alkoxylating agent selected from the group consisting of alkylene oxides and alkylene carbonates, and (ii) a phenolic aralkylation polymer comprising the reaction product of a phenolic monomer having at least two free reactive positions; a styrene derivative; and a coupling agent. The previously chain-extended phenolic-based hydroxyl compound also may be chain-extended by reacting with a lactam to produce a lactam chain-extended polyester polyamide. The polyols and polyamides of the present invention provide unique combinations of hard and soft functionalities, which translates into materials exhibiting a unique combination of toughness and hardness. These materials are especially suitable for use in high solids coatings and in the development of resins which can be readily processed into thermoset resins. The materials also may function as compatibilizers for thermoplastics.
摘要翻译：本发明的内酯链延长聚酯多元醇包括内酯与先前扩链的酚基羟基化合物的反应产物。先前扩链的酚基羟基化合物可以包含（i）内酯或选自环氧烷烃和碳酸亚烷基酯的烷氧基化剂的反应产物，和（ii）包含以下的反应产物的酚芳烷基化聚合物：具有至少两个自由反应位置的酚醛单体; 苯乙烯衍生物; 和偶联剂。先前的链延长的酚基羟基化合物也可以通过与内酰胺反应来产生内酰胺链延长的聚酯聚酰胺来延伸。本发明的多元醇和聚酰胺提供硬和软功能的独特组合，其转化为显示韧性和硬度的独特组合的材料。这些材料特别适用于高固含量涂料和开发可以容易地加工成热固性树脂的树脂。这些材料也可用作热塑性塑料的增容剂。

5. 发明授权

US5371171A Poly(methylene oxalate) and precursors thereto 失效
标题翻译：聚（亚甲基草酸盐）及其前体
公开(公告)号：US5371171A
公开(公告)日：1994-12-06
申请号：US27134
申请日：1993-03-05
申请人： A. G. Pinkus , Rajan Hariharan
发明人： A. G. Pinkus , Rajan Hariharan
IPC分类号： B32B15/04 , B32B17/10 , C03C27/04 , C03C27/10 , C08G63/18 , C08G63/40 , C08G63/02
CPC分类号： C03C27/10 , B32B15/04 , B32B17/10779 , C03C27/048 , C08G63/18 , C08G63/40
摘要： A poly(methylene oxalate) polymer [poly(oxy(1,2-dioxo-1,2-ethanediyl)oxymethylene)], a bis(tetrabutylammonium) oxalate salt, methods of synthesis thereof and methods of use. Poly(methylene oxalate) is insoluble in all common organic solvents, does not melt and is resistant to fire. Applications are as a light-weight material for use at high temperatures, e.g. as a structural material in aircraft and space vehicles, as a binder for brake systems, and as an insulator for microelectronic components.
摘要翻译：聚（亚甲基草酸盐）聚合物[聚（氧基（1,2-二氧代-1,2-乙二基）甲醛）]，双（四丁基铵）草酸盐，其合成方法和使用方法。聚（亚甲基草酸盐）不溶于所有常见的有机溶剂，不熔化并耐火。应用是作为在高温下使用的轻质材料，例如。作为飞机和太空车辆中的结构材料，作为制动系统的粘合剂，以及作为微电子部件的绝缘体。

6. 发明申请

US20100084757A1 CONDUCTIVE COMPOSITIONS AND METHODS OF USING THEM 有权
标题翻译：导电组合物及其使用方法
公开(公告)号：US20100084757A1
公开(公告)日：2010-04-08
申请号：US12567523
申请日：2009-09-25
申请人： Rajan Hariharan , James Hurley , Senthil Kanagavel , Jose Quinones , Martin Sobczak , Deborah Makita
发明人： Rajan Hariharan , James Hurley , Senthil Kanagavel , Jose Quinones , Martin Sobczak , Deborah Makita
IPC分类号： H01L23/48 , B05D5/12 , H01L23/498
CPC分类号： C08K5/09 , B23K35/3612 , B23K2101/36 , C08K3/08 , C08K2003/0806 , C08K2003/0837 , C08K2003/085 , H01B1/22 , H01L23/04 , H01L23/3178 , H01L23/4928 , H01L23/49883 , H01L24/80 , H01L2224/03332 , H01L2224/03442 , H01L2224/80011 , H01L2924/0002 , H05K7/02 , H01L2924/00
摘要： A conductive composition includes a mono-acid hybrid that includes an unprotected, single reactive group. The mono-acid hybrid may include substantially non-reactive groups elsewhere such that the mono-acid hybrid is functional as a chain terminator. Methods and devices using the compositions are also disclosed.
摘要翻译：导电组合物包括单酸混合物，其包含未被保护的单个反应性基团。单酸杂化物可以在其他地方包括基本上非反应性基团，使得单酸杂合物作为链终止剂起作用。还公开了使用该组合物的方法和装置。

7. 发明申请

US20060079050A1 Capacitor structure 失效
标题翻译：电容结构
公开(公告)号：US20060079050A1
公开(公告)日：2006-04-13
申请号：US11243890
申请日：2005-10-05
申请人： John Cahalen , Maria Rzeznik , John Schemenaur , Rajan Hariharan
发明人： John Cahalen , Maria Rzeznik , John Schemenaur , Rajan Hariharan
IPC分类号： H01L21/8242
CPC分类号： H05K1/162 , H01G4/005 , H01L28/75 , H05K3/384 , H05K2201/0355 , H05K2201/09509 , H05K2203/0723
摘要： Structures including a capacitor dielectric material disposed on the surface of an electrode suitable for use in forming capacitors are disclosed. Methods of forming such structures are also disclosed.
摘要翻译：公开了包括设置在适合用于形成电容器的电极的表面上的电容器电介质材料的结构。还公开了形成这种结构的方法。

8. 发明授权

US07190016B2 Capacitor structure 失效
标题翻译：电容结构
公开(公告)号：US07190016B2
公开(公告)日：2007-03-13
申请号：US11243890
申请日：2005-10-05
申请人： John P. Cahalen , Maria Anna Rzeznik , John E. Schemenaur , Rajan Hariharan
发明人： John P. Cahalen , Maria Anna Rzeznik , John E. Schemenaur , Rajan Hariharan
IPC分类号： H01L27/108 , H01L29/76 , H01L29/94 , H01L31/119
CPC分类号： H05K1/162 , H01G4/005 , H01L28/75 , H05K3/384 , H05K2201/0355 , H05K2201/09509 , H05K2203/0723
摘要： Structures including a capacitor dielectric material disposed on the surface of an electrode suitable for use in forming capacitors are disclosed. Methods of forming such structures are also disclosed.
摘要翻译：公开了包括设置在适合用于形成电容器的电极的表面上的电容器电介质材料的结构。还公开了形成这种结构的方法。

9. 发明授权

US06700006B2 Internally plasticizing and crosslinkable monomers and applications thereof 失效
标题翻译：内部增塑和可交联的单体及其应用
公开(公告)号：US06700006B2
公开(公告)日：2004-03-02
申请号：US09832266
申请日：2001-04-10
申请人： Shelby Freland Thames , Kamlesh Gopichand Panjnani , Rajan Hariharan , Zhiyu Wang
发明人： Shelby Freland Thames , Kamlesh Gopichand Panjnani , Rajan Hariharan , Zhiyu Wang
IPC分类号： C07C5900
CPC分类号： C08F220/18 , C07C69/73 , C08F218/08 , Y10S977/788
摘要： Novel compounds derived from traditional semi- drying and non-drying oils featuring internally plasticizing and crosslinkable properties are disclosed and claimed. Preferred embodiments include acrylate or methacrylate esters of hydroxy long-chain olefinic compounds derived from castor oil or lesquerella oil. A process for the preparation of the novel compounds is also disclosed, which involves esterification reaction of ethylenically unsaturated carboxylic acids or its derivatives with substituted hydroxy long-chain olefinic compounds. These compounds are suitable for forming latices, which form films at low minimum film forming temperatures (MFT) ranging from −5 to 10° C. and cure to above ambient glass transition (Tg) polymers without the use of traditional organic cosolvents which contribute to environmental pollution via volatile organic compounds (VOCs) emissions. These latices are therefore useful in waterborne coatings, contact and pressure sensitive adhesives, and inks.
摘要翻译：公开并要求保护具有内部增塑和交联性能的传统半干燥和非干燥油衍生的新型化合物。优选的实施方案包括衍生自蓖麻油或莱斯特雷拉油的羟基长链烯烃化合物的丙烯酸酯或甲基丙烯酸酯。还公开了制备新化合物的方法，其涉及烯键式不饱和羧酸或其衍生物与取代的羟基长链烯烃化合物的酯化反应。这些化合物适用于形成胶乳，其在低至最低成膜温度（MFT）为-5至10℃下形成薄膜，并固化至高于环境的玻璃化转变（Tg）聚合物，而不使用传统的有机共溶剂，其有助于通过挥发性有机化合物（VOCs）排放的环境污染。因此，这些胶乳可用于水性涂料，接触和压敏粘合剂以及油墨。

10. 发明授权

US06011133A Laminates of glass or metal and poly(alkylene dicarboxylates) and syntheses thereof 失效
标题翻译：玻璃或金属和聚（亚烷基二羧酸酯）的层合物及其合成
公开(公告)号：US06011133A
公开(公告)日：2000-01-04
申请号：US192825
申请日：1998-11-16
申请人： A. G. Pinkus , Rajan Hariharan
发明人： A. G. Pinkus , Rajan Hariharan
IPC分类号： B32B15/04 , B32B17/06 , B32B17/10 , C03C27/04 , C03C27/10 , C08G63/18 , C08G63/40 , C08G63/44
CPC分类号： B32B17/06 , B32B15/04 , B32B17/10036 , B32B17/10779 , C03C27/048 , C03C27/10 , C08G63/18 , C08G63/40 , Y10T428/31681 , Y10T428/31786
摘要： Poly(alkylene dicarboxylate) polymers and copolymers having tetraalkyl- or trialkylammonium ion end groups and methods of synthesis, thereof. The methylene-containing copolymers, in general, adhere to glass and metals, including aluminum, iron, and copper. Poly(methylene-co-ethylene terephthalate) is a clear film useful in the protection of metals or glass from corrosion or scratching. Glass may be bound to glass or to metal using the polymers of the present invention or metal to metal seals may be made.
摘要翻译：具有四烷基 - 或三烷基铵离子端基的聚（亚烷基二羧酸酯）聚合物和共聚物及其合成方法。通常，含亚甲基的共聚物粘附在玻璃和金属上，包括铝，铁和铜。聚（亚甲基 - 对苯二甲酸乙二醇酯）是一种透明膜，可用于保护金属或玻璃免受腐蚀或划伤。可以使用本发明的聚合物或金属与金属密封来制造玻璃与金属结合。

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