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1. 发明申请

US20100311567A1 REGENERATION OF ZEOLITE CARBONYLATION CATALYSTS 有权
标题翻译： ZEOLITE CARBONYLATION催化剂的再生
公开(公告)号：US20100311567A1
公开(公告)日：2010-12-09
申请号：US12735122
申请日：2008-12-16
申请人： Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephen Andreas Schunk , Martin Smit , John Glenn Sunley
发明人： Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephen Andreas Schunk , Martin Smit , John Glenn Sunley
IPC分类号： B01J38/10
CPC分类号： B01J29/06 , B01J29/20 , B01J29/50 , B01J29/65 , B01J29/86 , B01J29/87 , B01J29/88 , B01J29/90 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
摘要： A process for the in-situ regeneration of a zeolite catalyst in a carbonylation process for the production of at least one of methyl acetate and acetic acid by contacting methanol, dimethyl ethyl or dimethyl carbonate with carbon monoxide in the presence of a zeolite catalyst, ceasing contact of the catalyst with the reactant, regenerating the catalyst with a regenerating gas selected from hydrogen or a mixture of hydrogen and carbon monoxide at a temperature in the range 250 to 600° C., terminating the hydrogen regenerating step and resuming contact of the catalyst with the reactant and carbon monoxide.
摘要翻译：一种用于在羰基化方法中原位再生沸石催化剂的方法，用于通过在沸石催化剂存在下使甲醇，二甲基乙基或碳酸二甲酯与一氧化碳接触来制备乙酸甲酯和乙酸中的至少一种，停止催化剂与反应物的接触，用选自氢或氢和一氧化碳的混合物的再生气体在250-600℃的温度下再生催化剂，终止氢再生步骤并恢复催化剂的接触与反应物和一氧化碳。

2. 发明授权

US08329606B2 Regeneration of zeolite carbonylation catalysts 有权
标题翻译：沸石羰基化催化剂的再生
公开(公告)号：US08329606B2
公开(公告)日：2012-12-11
申请号：US12735122
申请日：2008-12-16
申请人： Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
发明人： Edo Johann Becker , Evert Jan Ditzel , Harry Kaiser , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
IPC分类号： B01J38/10 , C07C51/12
CPC分类号： B01J29/06 , B01J29/20 , B01J29/50 , B01J29/65 , B01J29/86 , B01J29/87 , B01J29/88 , B01J29/90 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
摘要： Process for the in-situ regeneration of a zeolite catalyst in a carbonylation process for the production of at least one of methyl acetate and acetic acid. The process is carried out by (a) contacting a carbonylatable reactant selected from methanol, dimethyl ether and dimethyl carbonate and carbon monoxide in a reactor with a zeolite catalyst and recovering a product stream containing at least one of methyl acetate and acetic acid from the reactor, (b) ceasing contact of the catalyst with the carbonylatable reactant, (c) regenerating the catalyst with a regenerating gas selected from hydrogen or a mixture of hydrogen and carbon monoxide at a temperature in the range 250 to 600 C, and (d) terminating the hydrogen regenerating step and resuming contact of the catalyst with the carbonylatable reactant and carbon monoxide.
摘要翻译：用于在羰基化方法中原位再生沸石催化剂以生产乙酸甲酯和乙酸中的至少一种的方法。该方法通过以下步骤进行：（a）在反应器中使沸石催化剂使选自甲醇，二甲醚和碳酸二甲酯的羰基化反应物与一氧化碳接触，并从反应器中回收含有至少一种乙酸甲酯和乙酸的产物流（b）停止催化剂与可羰基化反应物的接触，（c）在选自氢气或氢气和一氧化碳的混合物中的再生气体在250至600℃的温度范围内再生催化剂，和（d）终止氢再生步骤并恢复催化剂与可羰基化反应物和一氧化碳的接触。

3. 发明授权

US08158815B2 Carbonylation process with in situ regeneration of mordenite catalyst 有权
标题翻译：羰基化过程与丝光沸石催化剂的原位再生
公开(公告)号：US08158815B2
公开(公告)日：2012-04-17
申请号：US12735123
申请日：2008-12-16
申请人： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
发明人： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
IPC分类号： C07C67/36 , C07C51/12 , C07C53/08
CPC分类号： B01J29/90 , B01J29/20 , B01J38/14 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
摘要： A process for the carbonylation of dimethyl ether, dimethyl carbonate and/or methanol with carbon monoxide and hydrogen in the presence of a mordenite catalyst to produce at least one of acetic acid and methyl acetate in which process the mordenite catalyst is regenerated in-situ by contacting the catalyst with a regenerating gas comprising a molecular oxygen-containing gas and an inert diluent at a total pressure in the range 1 to 100 bar and wherein the partial pressure of the molecular oxygen-containing gas is such that the temperature of the catalyst is maintained within the range 225 to 325° C.
摘要翻译：一种在丝光沸石催化剂存在下用一氧化碳和氢气二甲醚，二甲基碳酸酯和/或甲醇羰基化的方法，以产生乙酸和乙酸甲酯中的至少一种，其中丝光沸石催化剂原位再生使催化剂与包含含分子氧的气体和惰性稀释剂的再生气体在1至100巴的总压下接触，并且其中分子氧气体的分压使得催化剂的温度为维持在225至325℃的范围内

4. 发明申请

US20100317888A1 CARBONYLATION PROCESS WITH IN SITU REGENERATION OF MORDENITE CATALYST 有权
标题翻译：在原位催化剂再生过程中的碳化过程
公开(公告)号：US20100317888A1
公开(公告)日：2010-12-16
申请号：US12735123
申请日：2008-12-16
申请人： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
发明人： Evert Jan Ditzel , David John Law , George Ernest Morris , Mark Stephen Roberts , Stephan Andreas Schunk , Martin Smit , John Glenn Sunley
IPC分类号： C07C67/36 , C07C67/37 , C07C51/12
CPC分类号： B01J29/90 , B01J29/20 , B01J38/14 , C07C51/12 , C07C67/37 , Y02P20/584 , C07C53/08 , C07C69/14
摘要： A process for the carbonylation of dimethyl ether, dimethyl carbonate and/or methanol with carbon monoxide and hydrogen in the presence of a mordenite catalyst to produce at least one of acetic acid and methyl acetate in which process the mordenite catalyst is regenerated in-situ by contacting the catalyst with a regenerating gas comprising a molecular oxygen-containing gas and an inert diluent at a total pressure in the range 1 to 100 bar and wherein the partial pressure of the molecular oxygen-containing gas is such that the temperature of the catalyst is maintained within the range 225 to 325° C.
摘要翻译：一种在丝光沸石催化剂存在下用一氧化碳和氢气二甲醚，二甲基碳酸酯和/或甲醇羰基化的方法，以产生乙酸和乙酸甲酯中的至少一种，其中丝光沸石催化剂原位再生使催化剂与包含含分子氧的气体和惰性稀释剂的再生气体在1至100巴的总压力下接触，并且其中分子氧气体的分压使得催化剂的温度为维持在225至325℃的范围内

5. 发明申请

US20080159927A1 System And Method For Performing A Chemical Experiment 有权
标题翻译：用于进行化学实验的系统和方法
公开(公告)号：US20080159927A1
公开(公告)日：2008-07-03
申请号：US11910493
申请日：2005-04-04
申请人： Martin Smit , Gerardus Johannes Maria Gruter
发明人： Martin Smit , Gerardus Johannes Maria Gruter
IPC分类号： B01J19/00 , G05D16/00 , G05D7/00 , B01J4/00
CPC分类号： B01J19/0046 , B01J2219/00286 , B01J2219/00391 , B01J2219/004 , B01J2219/00477 , B01J2219/00585 , B01J2219/00601 , B01J2219/00707 , B01J2219/00747 , Y10T137/7358 , Y10T137/7374 , Y10T137/7771 , Y10T137/7781 , Y10T137/7836
摘要： The invention relates to a system for performing parallel chemical experiments. The system comprises an array of parallel flow through reactors each comprising a reaction chamber, a reactor inlet and a reactor outlet connected to the reactor chamber. Downstream of each reactor a corresponding active pressure regulating arrangement is provided for actively regulating the reactor pressure. The pressure regulating arrangement comprises a passage for reactor effluent with an inlet connected to the reactor outlet and an outlet for discharging reactor effluent at a reduced pressure with respect to the reactor pressure.
摘要翻译：本发明涉及一种用于进行平行化学实验的系统。该系统包括平行流通反应器的阵列，每个反应器包括反应室，反应器入口和连接到反应器室的反应器出口。每个反应器的下游提供相应的主动压力调节装置，用于主动调节反应器压力。压力调节装置包括用于反应器流出物的通道，其具有连接到反应器出口的入口和用于相对于反应器压力在减压下排放反应器流出物的出口。

6. 发明申请

US20050169815A1 System for chemical experiments 审中-公开
标题翻译：化学实验系统
公开(公告)号：US20050169815A1
公开(公告)日：2005-08-04
申请号：US10988070
申请日：2004-11-12
申请人： Peter van den Brink , Martin Smit , Gerardus Johannes Gruter , Rene de Ruiter , Jan van der Waal
发明人： Peter van den Brink , Martin Smit , Gerardus Johannes Gruter , Rene de Ruiter , Jan van der Waal
IPC分类号： B01J19/00 , B01L99/00 , C40B60/14 , G01N35/10
CPC分类号： G01N35/1095 , B01J19/0046 , B01J2219/00283 , B01J2219/00286 , B01J2219/00308 , B01J2219/00369 , B01J2219/00389 , B01J2219/00418 , B01J2219/00423 , B01J2219/00481 , B01J2219/00495 , B01J2219/00585 , B01J2219/00707 , B01J2219/0072 , B01J2219/00745 , B01J2219/00747 , B01L3/0293 , B01L2400/086 , C40B60/14
摘要： A system for performing a chemical experiment comprises a reactor vessel having a wall defining a reaction chamber for receiving one or more fluids performing a chemical reaction. An analysis apparatus is located remote from said reactor vessel for analysing samples of said one or more fluids removed from said reaction chamber. Sampling means and transfer means are provided which are adapted for removing samples of said one or more fluids from said reaction chamber and transferring said samples to said analysis apparatus. The sampling and transfer means comprise a sample removal passage in communication with said reaction chamber and a sample transfer passage connected to said sample removal passage and extending to said analysis apparatus. The sample removal passage establishes an open communication between said reaction chamber and said sample transfer passage and the sample removal passage contains a flow restrictor. A pressure drop over said flow restrictor causes the removal of said samples from the reaction chamber.
摘要翻译：用于执行化学实验的系统包括反应器容器，其具有限定用于接收执行化学反应的一种或多种流体的反应室的壁。分析装置位于远离所述反应器容器的位置，用于分析从所述反应室移除的所述一种或多种流体的样品。提供了采样装置和传送装置，其适于从所述反应室中移除所述一种或多种流体的样品并将所述样品转移到所述分析装置。采样和传送装置包括与所述反应室连通的样品移除通道和连接到所述样品移除通道并延伸到所述分析设备的样品传送通道。样品移除通道建立在所述反应室和所述样品传送通道之间的开放连通，并且样品移除通道包含限流器。所述限流器上的压降导致所述样品从反应室中移出。

7. 发明申请

US20110108132A1 REACTION ASSEMBLY AND FLOW SPLITTER 审中-公开
标题翻译：反应组件和流动分离器
公开(公告)号：US20110108132A1
公开(公告)日：2011-05-12
申请号：US12992436
申请日：2009-05-26
申请人： Roelandus Hendrikus Wilhelmus Moonen , Emilio Rene' Bodenstaff , Martin Smit
发明人： Roelandus Hendrikus Wilhelmus Moonen , Emilio Rene' Bodenstaff , Martin Smit
IPC分类号： G05D11/00
CPC分类号： G05D7/0635 , B01J19/0046 , B01J2219/00286 , B01J2219/00306 , B01J2219/00418 , B01J2219/00587 , G05D11/132 , Y10T137/2514
摘要： The invention pertains to reaction systems in which at least one capillary unit is applied. The capillary unit comprises: —a unit inlet for receiving a fluid flow, —a unit outlet for releasing said fluid flow, —a capillary, which capillary is arranged between the unit inlet and the unit outlet such that said fluid flow passes through the capillary, —a heater and/or a cooler for adjusting the temperature of the capillary and therewith influencing the flow rate of the fluid flow passing through said capillary, —a housing for accommodating at least the capillary and heater and/or cooler of said capillary unit, which housing provides thermal insulation of the capillary, —a flow sensor for measuring the flow rate of the fluid flow through the capillary unit, which flow sensor can be arranged either inside or outside the housing, A capillary unit is combined with or further has a flow adjustment unit for adjusting the flow rates of the secondary fluid flows, which flow adjustment unit comprises a temperature control device for individually controlling the heater and/or cooler of each capillary unit in response to the flow rate that is measured by the flow sensor of that capillary unit.
摘要翻译：本发明涉及应用至少一个毛细管单元的反应系统。毛细管单元包括： - 用于接收流体流的单元入口， - 用于释放所述流体流的单元出口， - 毛细管，毛细管布置在单元入口和单元出口之间，使得所述流体流通过毛细管， - 加热器和/或冷却器，用于调节毛细管的温度并因此影响通过所述毛细管的流体流的流速， - 用于至少容纳所述毛细管单元的毛细管和加热器和/或冷却器的壳体，该壳体提供毛细管的热绝缘， - 用于测量流过毛细管单元的流体流量的流量传感器，该流量传感器可以布置在壳体的内部或外部。毛细管单元与用于调节二次流体流量的流量的流量调节单元，该流量调节单元包括一个温度控制装置，用于单独控制加热器和/或响应于由该毛细管单元的流量传感器测量的流速，每个毛细管单元的冷却器。

8. 发明授权

US07997297B2 System and method for performing a chemical experiment 有权
标题翻译：用于进行化学实验的系统和方法
公开(公告)号：US07997297B2
公开(公告)日：2011-08-16
申请号：US11910493
申请日：2005-04-04
申请人： Martin Smit , Gerardus Johannes Maria Gruter
发明人： Martin Smit , Gerardus Johannes Maria Gruter
IPC分类号： B01J19/00 , F16K7/04
CPC分类号： B01J19/0046 , B01J2219/00286 , B01J2219/00391 , B01J2219/004 , B01J2219/00477 , B01J2219/00585 , B01J2219/00601 , B01J2219/00707 , B01J2219/00747 , Y10T137/7358 , Y10T137/7374 , Y10T137/7771 , Y10T137/7781 , Y10T137/7836
摘要： The invention relates to a system for performing parallel chemical experiments. The system comprises an array of parallel flow through reactors each comprising a reaction chamber, a reactor inlet and a reactor outlet connected to the reactor chamber. Downstream of each reactor a corresponding active pressure regulating arrangement is provided for actively regulating the reactor pressure. The pressure regulating arrangement comprises a passage for reactor effluent with an inlet connected to the reactor outlet and an outlet for discharging reactor effluent at a reduced pressure with respect to the reactor pressure.
摘要翻译：本发明涉及一种用于进行平行化学实验的系统。该系统包括平行流通反应器的阵列，每个反应器包括反应室，反应器入口和连接到反应器室的反应器出口。每个反应器的下游提供相应的主动压力调节装置，用于主动调节反应器压力。压力调节装置包括用于反应器流出物的通道，其具有连接到反应器出口的入口和用于相对于反应器压力在减压下排放反应器流出物的出口。

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