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1. 发明授权

US06265461B1 High-solids, radiation-curable water-soluble combinations of polyester resins 有权
标题翻译：高固体，可辐射固化的聚酯树脂的水溶性组合
公开(公告)号：US06265461B1
公开(公告)日：2001-07-24
申请号：US09383091
申请日：1999-08-25
申请人： Edmund Urbano , Ulrike Kuttler , Martin Gerlitz , Rami-Raimund Awad
发明人： Edmund Urbano , Ulrike Kuttler , Martin Gerlitz , Rami-Raimund Awad
IPC分类号： C09D16707
CPC分类号： C09D167/07 , C08G63/21 , C08L67/00
摘要： Radiation curable polyester composition AB, capable of forming solutions or dispersions in water of high solid content which can be produced by mixing or pre-condensing a water soluble, radiation-curable emulsifying resin A which contains ester and acid groups and has an acid number from 20 to 300 mg/g and water-insoluble, radiation-curable polymer B containing ester and/or ether groups, wherein resin A is a reaction product of an alkoxylated polyol A1 having at least 3 hydroxyl groups and 3 to 10 oxyalkylene units per molecule, these oxyalkylene units containing 2 to 4 carbon atoms each, with an &agr;, &bgr;-unsaturated carboxylic acid A2 having each a free carboxyl group per molecule, and a carboxylic acid A3 which is at least tri-functional and wherein polymer B is a reaction product of aliphatic, linear, branched or cyclic alcohols B1 with compounds B2, selected from alkylene oxides B21, dicarboxylic acids B22 and aliphatic lactones B23 having 4 to 12 carbon atoms as well as compounds B3 selected from &agr;,&bgr;-unsaturated carboxylic acids with 1 to 2 carboxyl groups in the molecule, aqueous coating compositions made therefrom, and a method of using these for coating of heat-sensitive substrates.
摘要翻译：可辐射固化的聚酯组合物AB，其能够在高固含量的水中形成溶液或分散体，其可通过将含有酯和酸基团并具有酸值的水溶性可辐射固化的乳化树脂A混合或预冷凝来制备 20至300mg / g和含有酯和/或醚基团的水不溶性可辐射固化聚合物B，其中树脂A是每分子具有至少3个羟基和3至10个氧化烯单元的烷氧基化多元醇A1的反应产物，各自含有2至4个碳原子的这些氧化烯单元与每分子具有游离羧基的α，β-不饱和羧酸A2和至少三官能的羧酸A3，其中聚合物B是反应脂肪族，直链，支链或环状醇B1与化合物B2的选自烯化氧B21，二羧酸B22和碳原子数4〜12的脂肪族内酯B23以及组合物 ds B3选自分子中具有1至2个羧基的α，β-不饱和羧酸，由其制备的水性涂料组合物，以及使用它们来涂覆热敏性基材的方法。

2. 发明授权

US5990192A Radiation-curable water-dilutable urethane resins, preparation process and use 失效
标题翻译：可辐射固化水可稀释的聚氨酯树脂，制备方法和用途
公开(公告)号：US5990192A
公开(公告)日：1999-11-23
申请号：US57583
申请日：1998-04-09
申请人： Martin Gerlitz , Rami-Raimund Awad , Ulrike Kuttler , Thomas Fraydl , Martin Leitner , Andreas Kocsar
发明人： Martin Gerlitz , Rami-Raimund Awad , Ulrike Kuttler , Thomas Fraydl , Martin Leitner , Andreas Kocsar
IPC分类号： C08G18/67 , C09D175/14 , C08G18/62
CPC分类号： C09D175/14 , C08G18/6705 , C08G18/675 , Y10T428/31591
摘要： Radiation-curable water-dilutable urethane resins obtainable by reacting cycloaliphatic and/or aromatic diisocyanates with a mixture of a (meth)acryloyl-containing dihydroxy compound in an amount such that the amount of reactive hydroxyl groups present therein is from 0.2 to 0.6 mol, and with a tri or tetrahydric polyol which has been partly esterified with (meth)acrylic acid and has a residual average hydroxyl functionality of from 1.0 to 1.4 in the molecule, in an amount such that the amount of the reactive hydroxyl groups is from 0.4 to 0.8 mol, the sum of the amounts of the reactive hydroxyl groups always being 1.0 mol, and from 40 to 60% of the isocyanate groups being converted into urethane groups, and reacting the resulting intermediate with an aliphatic saturated monocarboxylic acid having at least two hydroxyl groups in an amount such that the amount of the reactive hydroxyl groups is from 0.6 to 1 mol, until the hydroxyl groups have undergone complete reaction and reacting this product, if desired, with further part-esterified polyol in an amount such that the amount of hydroxyl groups in the polyol is from 0 to 0.5 mol until the remaining free isocyanate groups have undergone complete reaction, the molar proportions of the components being chosen so that the ratio of the number of isocyanate groups to the number of hydroxyl groups is from 0.9:1 to 1:1 and the reaction product possesses carboxyl groups in accordance with an acid number of from 20 to 40 mg/g and has a specific double bond content of not more than 3.5 mol/kg.
摘要翻译：可通过使脂环族和/或芳族二异氰酸酯与含（甲基）丙烯酰基的二羟基化合物的混合物使其中存在的反应性羟基的量为0.2至0.6mol的量反应得到的可辐射固化水可稀释的聚氨酯树脂，和与（甲基）丙烯酸部分酯化并且在分子中具有1.0至1.4的残余平均羟基官能度的三元或四元多元醇，其量使得反应性羟基的量为0.4至 0.8mol，反应性羟基的总量总计为1.0mol，异氰酸酯基的40-60％转化为氨基甲酸酯基团，并使得到的中间体与具有至少两个羟基的脂族饱和一元羧酸反应基团的量使得反应性羟基的量为0.6至1mol，直到羟基已经完全反应并使其反应是产物，如果需要，还有部分酯化的多元醇的量使得多元醇中羟基的量为0至0.5mol，直到剩余的游离异氰酸酯基团经历了完全反应，选择的组分的摩尔比例使得异氰酸酯基数与羟基数的比例为0.9:1至1:1，并且反应产物具有根据酸值为20至40mg / g的羧基，并且具有特定的双键含量不超过3.5 mol / kg。

3. 发明申请

US20120238690A1 WATER-BORNE BINDERS FOR PRIMER-SURFACER COATING COMPOSITIONS 审中-公开
标题翻译：用于表面涂料组合物的水性粘合剂
公开(公告)号：US20120238690A1
公开(公告)日：2012-09-20
申请号：US13384798
申请日：2010-07-21
申请人： Roland Feola , Ulrike Kuttler
发明人： Roland Feola , Ulrike Kuttler
IPC分类号： C09D167/02
CPC分类号： C08G18/0823 , C08L61/28 , C08L75/04 , C09D167/00 , C09D175/04 , C08L2666/16 , C08L2666/14
摘要： The invention relates to water-borne coating binders ABC comprising a mixture of a curing agent C and a reaction product AB made by at least partial esterification of a hydroxyl group-containing polyester A and an acid groups-containing polyurethane B, characterised in that each of A and B comprise not more than 20% of the amount of substance of their educts A1, A2, B1, and B2, of molecules comprising aromatic structures, to a method of their preparation, and a method of use thereof to formulate primer-surfacer coating compositions.
摘要翻译：本发明涉及包含固化剂C和通过至少部分酯化含羟基的聚酯A和含酸性基团的聚氨酯B制成的反应产物AB的混合物的水性涂料粘合剂ABC，其特征在于每种的A和B包含不超过其包含芳族结构的分子的A1，A2，B1和B2的物质的量的20％，其制备方法及其制备方法，表面涂料组合物。

4. 发明授权

US6048936A Acrylate polymers based on polyester resins or polyester oligomers 失效
标题翻译：基于聚酯树脂或聚酯低聚物的丙烯酸酯聚合物
公开(公告)号：US6048936A
公开(公告)日：2000-04-11
申请号：US130489
申请日：1998-08-07
申请人： Ulrich Epple , Gert Dworak , Ulrike Kuttler , Claudia Pietsch
发明人： Ulrich Epple , Gert Dworak , Ulrike Kuttler , Claudia Pietsch
IPC分类号： C08F283/02 , C09D4/02 , C09D151/08 , C09D133/02 , C08L33/02 , C08L33/14 , C09D133/14
CPC分类号： C09D151/08 , C08F283/02
摘要： Acrylate copolymers AB obtainable by polymerization of a monomer mixture A in an organic solvent or in bulk, the monomer mixture A comprising proportions by mass of from 25 to 80% of C.sub.1 -C.sub.20 -alkyl (meth)acrylates whose alkyl radicals can be linear, branched or cyclic, from 1 to 28% of C.sub.2 -C.sub.20 -hydroxyalkyl (meth)acrylates whose hydroxyalkyl radicals can be linear, branched or cyclic, from 0.5 to 20% of .alpha.,.beta.-unsaturated carboxylic acids and from 0 to 55% of aromatic vinyl compounds or aliphatic vinyl esters and vinyl ethers, vinyl halides, olefinically unsaturated ketones or aldehydes, esters of glycidyl alcohol or methylglycidyl alcohol with olefinically unsaturated carboxylic acids, or nitriles of .alpha.,.beta.-unsaturated carboxylic acids, in the presence of free-radical polymerization initiators and of at least one polyester or polyester oligomer B obtaintable by polycondensation of polyoles and polycarboxylic acids and having a hydroxyl number of from 50 to 350 mg/g, an acid number of from 1 to 50 mg/g and a weight-average molar mass M.sub.w of up to 5000 g/mol, with the provisos that the polyester or the polyester oligomers are free from olefinic double bonds, that the proportion by mass of component B in the end product AB is less than 10% of its mass and that this end product has an acid number of from 5 to 45 mg/g, a hydroxyl number of from 40 to 125 mg/g and a weight-average molar mass M.sub.w of not more than 10,000 g/mol and a polydispersity (=M.sub.w /M.sub.n) of 3 or less than 3. The copolymers can be employed in coating compositions for metals, plastics, wood, leather, textiles, paper and building materials.
摘要翻译：通过单体混合物A在有机溶剂中或本体聚合获得的丙烯酸酯共聚物AB，其单体混合物A包含25至80％（C 1 -C 20烷基（甲基）丙烯酸烷基酯，其烷基可以是直链的）支链或环状的1至28％的羟烷基可以是直链，支链或环状的C 2 -C 20羟烷基（甲基）丙烯酸酯，0.5至20％的α，β-不饱和羧酸和0至55％芳族乙烯基化合物或脂族乙烯基酯和乙烯基醚，乙烯基卤化物，烯属不饱和酮或醛，缩水甘油醇或甲基缩水甘油酯与烯属不饱和羧酸的酯，或α，β-不饱和羧酸的腈，自由基聚合引发剂和至少一种聚酯或聚酯低聚物B，其通过多元醇和多元羧酸的缩聚获得，羟值为50-350mg / g，酸数量为1至50mg / g，重均摩尔质量Mw高达5000g / mol，条件是聚酯或聚酯低聚物不含烯属双键，组分B的质量比例最终产物AB小于其质量的10％，并且该最终产物的酸值为5至45mg / g，羟值为40至125mg / g，重均摩尔质量Mw 不大于10,000g / mol，多分散性（= Mw / Mn）为3或小于3。该共聚物可用于金属，塑料，木材，皮革，纺织品，纸张和建筑材料的涂料组合物中。

5. 发明授权

US06406753B2 Aqueous coating composition 失效
标题翻译：水性涂料组合物
公开(公告)号：US06406753B2
公开(公告)日：2002-06-18
申请号：US09727136
申请日：2000-11-30
申请人： Gert Dworak , Ulrike Kuttler
发明人： Gert Dworak , Ulrike Kuttler
IPC分类号： B05D302
CPC分类号： C09D201/08 , C09D175/04 , C08L2666/14
摘要： Coating composition especially for preparing automotive surfacers, comprising an anionically stabilized resin, preferably a condensation product A of a carboxyl group-containing resin A1 and a hydroxyl group-containing resin A2, and a curing agent C, which becomes active even at room temperature or slightly elevated temperature of up to not more than 120° C., and comprises a mixture of an unblocked isocyanate C1 and a hydrophilic partially etherified amino resin C2.
摘要翻译：涂料组合物特别用于制备汽车表面活性剂，其包含阴离子稳定的树脂，优选含羧基树脂A1和含羟基的树脂A2的缩合产物A和固化剂C，其即使在室温下也变得有活性，或稍高的温度高达不高于120℃，并且包含未封端的异氰酸酯C1和亲水部分醚化的氨基树脂C2的混合物。

6. 发明申请

US20130330561A1 MULTI-LAYER COATING FILMS 审中-公开
标题翻译：多层涂膜
公开(公告)号：US20130330561A1
公开(公告)日：2013-12-12
申请号：US13981189
申请日：2012-02-21
申请人： Rudolf Schipfer , Roland Feola , Ulrike Kuttler
发明人： Rudolf Schipfer , Roland Feola , Ulrike Kuttler
IPC分类号： H01B5/00
CPC分类号： H01B5/00 , B05D7/14 , B05D7/542 , C09D5/4442 , C25D13/22 , Y10T428/31554 , Y10T428/31565
摘要： The invention relates to a process for the preparation of a multi-layer coating film on an electrically conductive substrate, comprising the steps of electrodepositing on an electrically conductive substrate, a first coating composition to form an uncured electrodeposition coating film, applying an aqueous primer-surfacer coating composition to form an uncured intermediate coating film, and then simultaneously heating the substrate coated with the said coating films and curing both the uncured electrodeposition coating film and the uncured intermediate coating film to form a cured film, wherein the curing agent B is a capped isocyanate where the capping agents are selected from the group consisting of aliphatic linear or branched diols, hydroxyalkyl(meth)acrylates and >NH functional heterocyclic aliphatic or aromatic compounds, to coating films made by this process, and to substrates covered with such coating films.
摘要翻译：本发明涉及一种在导电基材上制备多层涂膜的方法，包括以下步骤：电沉积在导电基材上，第一涂料组合物形成未固化的电沉积涂膜，表面涂料组合物以形成未固化的中间涂层膜，然后同时加热涂覆有所述涂膜的基材并固化未固化的电沉积涂膜和未固化的中间涂膜以形成固化膜，其中固化剂B为封端的异氰酸酯，其中封端剂选自脂肪族直链或支链二醇，羟基烷基（甲基）丙烯酸酯和> NH官能杂环脂族或芳族化合物，通过该方法制备的涂膜以及用这种涂膜覆盖的基材。

7. 发明授权

US06824834B2 Coating composition 失效
标题翻译：涂料组成
公开(公告)号：US06824834B2
公开(公告)日：2004-11-30
申请号：US10288813
申请日：2002-11-06
申请人： Markus A. Schafheutle , Ulrike Kuttler , Anton Arzt , Julius Burkl
发明人： Markus A. Schafheutle , Ulrike Kuttler , Anton Arzt , Julius Burkl
IPC分类号： C09D17504
CPC分类号： C08G18/8061 , C08G18/0823 , C08G18/4288 , C09D175/04 , Y10T428/31551 , C08L75/04
摘要： Coating composition especially for preparing automotive surfacers, comprising a condensation product A of a carboxyl-containing resin A1 and a hydroxyl-containing resin A2, a curing agent C which becomes active only at an elevated temperature of at least 80° C., and a high molecular mass polyurethane B.
摘要翻译：包含含羧基的树脂A1和含羟基的树脂A2的缩合产物A，仅在至少80℃的升高的温度下变为活性的固化剂C的用于制备汽车表面活性剂的涂料组合物和高分子量聚氨酯B.

8. 发明授权

US06596817B2 Low molar mass aliphatic polyester polyols, their preparation and use in high performance coating compositions 有权
公开(公告)号：US06596817B2
公开(公告)日：2003-07-22
申请号：US09882665
申请日：2001-06-15
申请人： Ulrich Epple , Ulrike Kuttler , Adolf Labenbacher
发明人： Ulrich Epple , Ulrike Kuttler , Adolf Labenbacher
IPC分类号： C08L6700
CPC分类号： C08G63/00
摘要： Low molar mass polyester polyols having a weight average molar mass Mw of up to 3500 g/mol, hydroxyl numbers of from 80 to 280 mg/g and acid numbers of from 5 to 40 mg/g, comprising structural units derived from aliphatic monocyclic or polycyclic compounds containing at least two hydroxyl and/or epoxide groups and at least one heteroatom, aliphatic acyclic or cyclic polyhydroxy compounds containing three or more hydroxyl groups per molecule, linear or branched aliphatic dihydroxy compounds and aliphatic cyclic polycarboxylic acids, alone or in a mixture with low molar mass acrylate copolymers, may be processed to give coating materials which dry rapidly, and result in defect-free surfaces.

9. 发明授权

US06258897B1 Polyester polyols of low molar mass, their preparation and use in coating compositions 失效
标题翻译：低摩尔质量的聚酯多元醇，它们在涂料组合物中的制备和用途
公开(公告)号：US06258897B1
公开(公告)日：2001-07-10
申请号：US09583735
申请日：2000-05-31
申请人： Ulrich Epple , Ulrike Kuttler , Claudia Pietsch
发明人： Ulrich Epple , Ulrike Kuttler , Claudia Pietsch
IPC分类号： C08F2000
CPC分类号： C08G18/423 , C08F20/00 , C08G18/4072 , C08G63/00 , C09D175/06
摘要： Low molar mass polyester polyols having a weight-average molar mass M, of not more than 2000 g/mol, with hydroxyl numbers of from 80 to 300 mg/g and acid numbers of from 5 to 35 mg/g, comprising the stated mole fractions (in %=mol/100 mol) of structural units derived from: a) from 1 to 45% of aliphatic polycyclic polyhydroxy compounds having at least two hydroxyl groups per molecule, b) from 5 to 50% of branched aliphatic acyclic dihydroxy compounds, c) from 30 to 50% of aliphatic cyclic polycarboxylic acids, d) from 0 to 30% of aliphatic acyclic or monocyclic polyhydroxy compounds having three or more hydroxyl groups per molecule, and e) from 0 to 10% of polyfunctional compounds selected from aliphatic linear and monocyclic dihydroxy compounds, aliphatic linear and branched dicarboxylic acids, aromatic dicarboxylic acids and polycaboxylic acids having three or more carboxyl groups per molecule, and also f) from 0 to 10% of monofunctional units selected from monocarboxylic acids and monoalcohols, the mole fractions indicated in each case under a), b), c), d), e) and f) adding up to 100% and use of these low molar mass polyester polyols or mixtures thereof of copolymers in one- and two-component coating materials and also spray surfacers.
摘要翻译：羟值为80〜300mg / g，酸值为5〜35mg / g的重量平均摩尔质量M为2000g / mol以下的低摩尔质量聚酯多元醇，包含所述摩尔衍生自以下结构单元的级分（％= mol / 100mol）：a）1至45％每分子具有至少两个羟基的脂族多环多羟基化合物，b）5至50％的支链脂族无环二羟基化合物，c）30-50％的脂肪族环状多元羧酸，d）0-30％的每分子具有三个或更多个羟基的脂族无环或单环多羟基化合物，和）0至10％的多官能化合物，选自脂肪族线性和单环二羟基化合物，脂族直链和支链二羧酸，芳族二羧酸和每分子具有三个或更多个羧基的多羟基酸，还有0至10％的选自单羧酸和monoalco的单官能单元在每种情况下，在a），b），c），d），e）和f）处指示的摩尔分数分别为100％和100％，并且使用这些低摩尔质量的聚酯多元醇或其共聚物的混合物，双组分涂料和喷雾表面活性剂。

10. 发明授权

US10538613B2 Aqueously dispersible polyurethane 有权
公开(公告)号：US10538613B2
公开(公告)日：2020-01-21
申请号：US13504390
申请日：2010-10-27
申请人： Anton Arzt , Markus Schafheutle , Gerlinde Petritsch , Julius Burkl , Robert Harrer , Ulrike Kuttler
发明人： Anton Arzt , Markus Schafheutle , Gerlinde Petritsch , Julius Burkl , Robert Harrer , Ulrike Kuttler
IPC分类号： B05D1/02 , C08G18/83 , C08G18/42
摘要： The invention relates to an aqueously dispersible polyurethane having a specific amount of substance of hydroxyl groups, —OH, of at least 0.6 mol/kg, and additionally satisfying at least two of the following conditions: a) a degree of branching measured as specific amount of substance of tertiary and/or quaternary aliphatic carbon atoms of from 0.01 mol/kg to 0.5 mol/kg, b) a specific amount of urea groups >N—CO—N

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