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    • 7. 发明申请
    • METHOD OF MANUFACTURING M41S FAMILY MOLECULAR SIEVE
    • 制备M41S家族分子筛的方法
    • WO2008097481A1
    • 2008-08-14
    • PCT/US2008/001388
    • 2008-02-01
    • EXXONMOBIL RESEARCH AND ENGINEERING COMPANYLAI, Wenyih, FrankMCCARTHY, Stephen, J.ELLIS, Robert, E.
    • LAI, Wenyih, FrankMCCARTHY, Stephen, J.ELLIS, Robert, E.
    • C01B37/00C01B37/02C01B37/04C01B37/08C01B39/00
    • C01B37/00C01B37/02C01B37/04C01B37/08C01B39/00
    • This disclosure relates to method for synthesizing a composition of matter comprising an inorganic, porous crystalline phase material having, after calcination, a substantially hexagonal arrangement of substantially uniformly- sized pores having mean diameters of at least about 13 Angstrom Units and exhibiting a substantially hexagonal electron diffraction pattern that can be indexed with a d1Oo value greater than about 18 Angstrom Units, the method comprising: preparing a mixture capable of forming the composition of matter, the mixture comprising sources of one or a combination of oxides of elements selected from the group consisting of divalent element W, trivalent element X, tetravalent element Y and pentavalent element Z, an organic directing agent (R) and a solvent, wherein at least a portion of the solvent comprises at least one recycle liquid produced during at least one previous process for the manufacture of the composition of matter; (a) maintaining the mixture under sufficient conditions of pH, temperature and time for formation of the composition of matter; (b) separating the composition of matter.
    • 本公开涉及用于合成物质组合物的方法,其包含无机多孔结晶相材料,其在煅烧之后具有基本上六边形的基本上均匀尺寸的孔,其平均直径为至少约13埃单位并且显示出基本上六边形的电子 衍射图案,其可以用大于约18埃单位的d1Oo值进行索引,所述方法包括:制备能够形成物质组合物的混合物,所述混合物包含一种或多种元素的氧化物的组合,所述氧化物选自 的二价元素W,三价元素X,四价元素Y和五价元素Z,有机导向剂(R)和溶剂,其中至少一部分溶剂包含至少一种在至少一个先前的方法中产生的再循环液体 物质组成的制造; (a)将混合物保持在足以形成物质组成的pH值,温度和时间的条件下; (b)分离物质的组成。