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1. 发明申请

WO2015177009A3 MEMBRANE-ASSISTED CATALYST SEPARATION DURING EPOXIDATION OF FATTY ACID METHYL ESTERS 审中-公开
标题翻译：基于膜的催化剂分离IN的脂肪酸环氧化
公开(公告)号：WO2015177009A3
公开(公告)日：2016-01-14
申请号：PCT/EP2015060543
申请日：2015-05-13
申请人： EVONIK DEGUSSA GMBH , WIEDERHOLD HOLGER , GRASS MICHAEL , WOLDT BENJAMIN , BOECK FLORIAN SEBASTIAN , PRISKE MARKUS , BOAM ANDREW , KREIS PETER
发明人： WIEDERHOLD HOLGER , GRASS MICHAEL , WOLDT BENJAMIN , BOECK FLORIAN SEBASTIAN , PRISKE MARKUS , BOAM ANDREW , KREIS PETER
IPC分类号： B01J31/40 , C07D301/12
CPC分类号： B01J31/4061 , B01J2231/72 , B01J2531/56 , B01J2531/64 , B01J2531/66 , B01J2531/985 , B01J2540/42
摘要： The invention relates to a method for separating homogeneous catalyst systems from organic reaction mixtures. The aim of the invention is to devise a method which is used for epoxidating fatty acid methyl ester in reaction mixtures. Said aim is achieved by using a membrane, the actively separating layer of which comprises crosslinked silicone acrylates and/or polydimethylsiloxane (PDMS) and/or polyimide.
摘要翻译：本发明涉及一种用于从有机反应混合物中分离均相催化剂体系的方法。它是基于指定的方法，其在反应混合物中用于脂肪酸烷基酯的环氧化的对象上。该目的是通过使用膜，交联的硅氧烷丙烯酸酯和/或Polydimetyl硅氧烷（PDMS）和/或包括聚酰亚胺的活性分离层来实现的。

2. 发明申请

WO2011000696A3 PRODUCING ISOBUTENE BY CRACKING MTBE 审中-公开
标题翻译：通过分解MTBE，现代制造异丁烯
公开(公告)号：WO2011000696A3
公开(公告)日：2011-06-16
申请号：PCT/EP2010058424
申请日：2010-06-16
申请人： EVONIK OXENO GMBH , WINTERBERG MARKUS , ROETTGER DIRK , RIX ARMIN , BUKOHL REINER , LUH WALTER , WIEDERHOLD HOLGER , SCHILLING GUNNAR , BOEING CHRISTIAN
发明人： WINTERBERG MARKUS , ROETTGER DIRK , RIX ARMIN , BUKOHL REINER , LUH WALTER , WIEDERHOLD HOLGER , SCHILLING GUNNAR , BOEING CHRISTIAN
IPC分类号： C07C11/09 , C07C1/20 , F28D7/00
CPC分类号： C07C11/09 , C07C1/20
摘要： The invention relates to a method for producing isobutene by cracking MTBE, wherein the following steps are carried out: a) MTBE synthesis; reacting isobutene-containing hydrocarbon mixtures (II) with methanol (III), contained in one or more methanol-containing streams (VIII, IX), on acidic ion exchangers obtaining a stream (IV) containing MTBE and TBA, b) MTBE separation; separating a stream (V) containing MTBE and TBA from stream (IV) by means of distillation, c) MTBE cracking; cracking the stream (V) on a heterogenic catalyst in the gas phase, thus obtaining a stream (VI) which contains at least isobutene, methanol, MTBE, water, and optionally TBA, d) isobutene separation; separating the stream (VI) by means of distillation, thus obtaining a stream (VII) containing more than 50 mass % of the amounts of methanol, TBA, and water contained in stream (VI), and a stream (XVII) containing isobutene, e) water separation; separating, water from the stream (VII) to below 1 mass % by means of distillation, thus obtaining a stream (VIII), f) recirculating; complete or partial recirculation of the methanol-containing stream (VIII) into the MTBE synthesis. The invention further relates to a tube bundle device comprising the following elements: i) tube bundle, ii) tube bottom, iii) deflection plates, iv) inner shell, iv) pressure bearing outer shell, comprising at least one inlet and outlet, vi) shell chamber, comprising a fluid releasing or absorbing heat, characterized in that the inner shell is connected to the deflection plates attached over the length of the tube bundle without a gap, or with a small gap, and is connected to the tube bottom, wherein the fluid present in the shell chamber encloses the inner shell on both sides.
摘要翻译：本发明涉及一种用于通过MTBE裂解制备异丁烯的方法，其特征在于，通过以下步骤：a）MTBE合成; 包含在一个或多个含甲醇的流（VIII，IX），酸性离子交换剂，以获得流含MTBE和TBA（IV）的烃混合物，（II），用甲醇（III）含异丁烯的，B）的MTBE反应分离; 含MTBE和TBA从电流（IV）中，c）MTBE裂解流（V）的蒸馏分离; 含有至少异丁烯，甲醇，MTBE和水和任选的TBA的电流（V）的裂解在在气相中，以获得一个流（VI）的非均相催化剂，D）异丁烯去除; 的电流（VI）的蒸馏分离，得到流（VII），（VI）中的功率的每个包含多于50质量％含有甲醇，TBA和水的水平，和含异丁烯的电流（XVII）， e）水分离; 蒸馏除去水从流（VII）至低于1％的质量百分比，以获得流（VIII）中，f）返回; 在MTBE合成含甲醇的流（VIII）的完全或部分再循环。本发明的下一个主题是具有下列元素的管装置：i）所述管束，ⅱ）管板，III）挡板，静脉内）内护套，ⅳ）承压外护套，其包括至少一个入口和出口，ⅵ）的壳空间包括热发射或接收流体，其特征在于，该内壳没有间隙或具有小的间隙与所述附着在管束偏转板的长度和管板连接，其中在围绕在两侧的内包层中的壳空间中的流体。

3. 发明申请

WO2011107188A3 PROCESS FOR THE MANUFACTURE OF A 1,2-EPOXIDE AND A DEVICE FOR CARRYING OUT SAID PROCESS 审中-公开
标题翻译： 1,2-环氧化物的制造方法和实施方法的装置
公开(公告)号：WO2011107188A3
公开(公告)日：2012-02-02
申请号：PCT/EP2011000320
申请日：2011-01-26
申请人： MOMENTIVE SPECIALTY CHEMICALS RES S A , MOMENTIVE SPECIALTY CHEM INC , MUPPA PRASAD , POSTMA RON , VAN DEN BERG BART , STOCK JUERGEN , WIEDERHOLD HOLGER , RAUSCH HANS , SCHALLENBERG JOERG , BERNHARDT STEFAN
发明人： MUPPA PRASAD , POSTMA RON , VAN DEN BERG BART , STOCK JUERGEN , WIEDERHOLD HOLGER , RAUSCH HANS , SCHALLENBERG JOERG , BERNHARDT STEFAN
IPC分类号： C07D301/12 , B01D17/02 , B01F5/06 , B01J19/18
CPC分类号： C07D301/14 , B01D17/0208 , B01F5/061 , B01J4/00 , B01J19/2435 , B01J2219/00094 , B01J2231/72 , C07D301/03 , C07D301/12 , Y02P20/582
摘要： Apparatus and processes are provided for forming epoxide compounds. In one embodiment, a process for the manufacture of an epoxide is provided including adding an oxidant, a water-soluble manganese complex and a terminal olefin to form a multiphasic reaction mixture, reacting the terminal olefin with the oxidant in the multiphasic reaction mixture having at least one organic phase in the presence of the water-soluble manganese complex, separating the reaction mixture into the at least one organic phase and an aqueous phase, and reusing at least part of the aqueous phase. The invention is also related to a device for performing the above process.
摘要翻译：提供了用于形成环氧化合物的装置和方法。在一个实施方案中，提供了制备环氧化物的方法，包括加入氧化剂，水溶性锰络合物和末端烯烃以形成多相反应混合物，使末端烯烃与氧化剂在多相反应混合物中反应，所述多相反应混合物具有在水溶性锰络合物的存在下的至少一个有机相，将反应混合物分离成至少一个有机相和水相，并重新使用至少部分水相。本发明还涉及用于执行上述过程的装置。

4. 发明申请

WO2010006832A3 PROCESS FOR PRODUCTION OF ISOBUTENE BY CRACKING MTBE-CONTAINING MIXTURES 审中-公开
标题翻译：通过剪切含MTBE的混合物制备异丁醇的方法
公开(公告)号：WO2010006832A3
公开(公告)日：2010-04-15
申请号：PCT/EP2009056069
申请日：2009-05-19
申请人： EVONIK OXENO GMBH , WINTERBERG MARKUS , ROETTGER DIRK , BUKOHL REINER , WIEDERHOLD HOLGER , LUH WALTER
发明人： WINTERBERG MARKUS , ROETTGER DIRK , BUKOHL REINER , WIEDERHOLD HOLGER , LUH WALTER
IPC分类号： C07C1/20 , C07C11/09
CPC分类号： C07C1/20 , C07C7/04 , C07C2521/12 , C07C2523/02 , C07C11/09
摘要： The invention relates to a process for production of isobutene from MTBE-containing mixtures which comprises the following steps a) cracking, in a reactor R, a mixture obtained from an MTBE-containing feedstock (1a) and/or an MTBE-containing stream (13, 5), delivering a stream (6) of reaction products consisting of isobutene, methanol, MTBE and also by-products, wherein these consist of a1) high boilers having a boiling range above 55°C at a pressure of 0.1 MPa; a2) medium boilers having a boiling range from 12 to 55°C at a pressure of 0.1 MPa; and a3) low boilers having a boiling range below 12°C at a pressure of 0.1 MPa; b) separation of stream (6) by distillation into a stream (7) which contains the product isobutene and low boilers and a stream (8) which contains MTBE, methanol, medium boilers and high boilers; c) separating the stream (8) by distillation obtaining an MTBE-containing stream (10, 12) and a methanol-containing high-boiler stream (9, 11); d) recirculating an MTBE-containing stream (10, 12, 13) to step a) of the process, wherein the medium-boilers are completely or partially separated off from the medium-boiler-rich streams (10, 12) upstream of step d).
摘要翻译：本发明涉及一种方法，用于从含MTBE的混合物制备异丁烯，包括：a）分离的步骤在反应器R A（从含MTBE原料1a）和/或含MTBE的流（13，5 ）由异丁烯，甲醇，MTBE和副产物组成的反应产物流（6），这些产物来自a1）高沸点化合物，沸点范围高于55℃，压力为0.1MPa; a2）在0.1MPa的压力下沸程为12-55℃的中级锅炉; 和a3）在0.1MPa的压力下具有低于12℃的沸程的低沸点物; b）将所述物流（6）蒸馏分离成含有产物异丁烯和低沸物的物流（7）和含有MTBE，甲醇，介质锅炉和高沸点物流的物流（8）; c）蒸馏分离物流（8）以获得含有MTBE的物流（10,12）和含甲醇的高沸点物流（9,11）; d）回收在步骤a的方法的含MTBE的流（10，12，13）），其中，被执行（从中间沸点组分丰富的流10，12）到步骤d）之前的介质锅炉的完全或部分分离。

5. 发明专利

AU2014204452B2 Process for the manufacture of a 1,2-epoxide and a device for carrying out said process 未知
公开(公告)号：AU2014204452B2
公开(公告)日：2016-03-03
申请号：AU2014204452
申请日：2014-07-16
申请人： EVONIK DEGUSSA GMBH
发明人： MUPPA PRASAD , POSTMA RON , VAN DEN BERG BART , STOCK JUERGEN , WIEDERHOLD HOLGER , RAUSCH HANS , SCHALLENBERG JÖRG , BERNHARDT STEFAN
IPC分类号： C07D301/12 , B01D17/02 , B01F5/06 , B01J19/18
摘要： Apparatus and processes are provided for forming epoxide compounds. In one embodiment, a process for the manufacture of an epoxide is provided including adding an oxidant, a water-soluble manganese complex and a terminal olefin to form a multiphasic reaction mixture, reacting the terminal olefin with the oxidant in the multiphasic reaction mixture having at least one organic phase in the presence of the water-soluble manganese complex, separating the reaction mixture into the at least one organic phase and an aqueous phase, and reusing at least part of the aqueous phase. The invention is also related to a device for performing the above process.

6. 发明专利

MY162533A PROCESS FOR THE MANUFACTURE OF A 1,2-EPOXIDE AND A DEVICE FOR CARRYING OUT SAID PROCESS 未知
公开(公告)号：MY162533A
公开(公告)日：2017-06-15
申请号：MYPI2012003461
申请日：2011-01-26
申请人： EVONIK DEGUSSA GMBH
发明人： MUPPA PRASAD , POSTMA RON , VAN DEN BERG BART , STOCK JUERGEN , WIEDERHOLD HOLGER , RAUSCH HANS , SCHALLENBERG JÖRG , BERNHARDT STEFAN
IPC分类号： C07D301/12 , B01D17/02 , B01F5/06 , B01J19/18
摘要： APPARATUS AND PROCESSES ARE PROVIDED FOR FORMING EPOXIDE COMPOUNDS. IN ONE EMBODIMENT, A PROCESS FOR THE MANUFACTURE OF AN EPOXIDE IS PROVIDED INCLUDING ADDING AN OXIDANT, A WATER-SOLUBLE MANGANESE COMPLEX AND A TERMINAL OLEFIN TO FORM A MULTIPHASIC REACTION MIXTURE, REACTING THE TERMINAL OLEFIN WITH THE OXIDANT IN THE MULTIPHASIC REACTION MIXTURE HAVING AT LEAST ONE ORGANIC PHASE IN THE PRESENCE OF THE WATER-SOLUBLE MANGANESE COMPLEX, SEPARATING THE REACTION MIXTURE INTO THE AT LEAST ONE ORGANIC PHASE AND AN AQUEOUS PHASE, AND REUSING AT LEAST PART OF THE AQUEOUS PHASE. THE INVENTION IS ALSO RELATED TO A DEVICE FOR PERFORMING THE ABOVE PROCESS.

7. 发明专利

ES2552154T3 Preparación de isobuteno mediante disociación de MTBE 未知
公开(公告)号：ES2552154T3
公开(公告)日：2015-11-26
申请号：ES10725455
申请日：2010-06-16
申请人： EVONIK DEGUSSA GMBH
发明人： WINTERBERG MARKUS , RÖTTGER DIRK , RIX ARMIN , BUKOHL REINER , LUH WALTER , WIEDERHOLD HOLGER , SCHILLING GUNNAR , BÖING CHRISTIAN
IPC分类号： C07C1/20 , C07C11/09
摘要： Procedimiento para la preparación de isobuteno mediante disociación de MTBE, en el que se recorren las siguientes etapas: a) síntesis de MTBE; reacción de mezclas de hidrocarburos (II) con contenido en isobuteno con metanol (III), contenido en una o varias corrientes con contenido en metanol (VIII, IX), en intercambiadores de iones de carácter ácido, obteniéndose una corriente (IV) que contiene MTBE y TBA, b) separación de MTBE; separación destilativa de una corriente (V) que contiene MTBE y TBA a partir de la corriente (IV), c) disociación de MTBE; disociación de la corriente (V) en un catalizador heterogéneo en la fase gaseosa, obteniéndose una corriente (VI) que contiene al menos isobuteno, metanol, MTBE y agua, y eventualmente TBA, d) separación de isobuteno; separación destilativa de la corriente (VI), obteniéndose una corriente (VII) que contiene en cada caso más de 50% en masa de las cantidades de metanol, TBA y agua contenidos en la corriente (VI), y una corriente (XVII) que contiene isobuteno, e) separación del agua; separación destilativa de agua a partir de la corriente (VII) hasta una porción inferior a 1% en masa, obteniéndose una corriente (VIII), f) retorno; retorno completo o parcial de la corriente (VIII) con contenido en metanol a la síntesis de MTBE.

8. 发明专利

DE102014209413A1 Membrangestützte Katalysatorabtrennung bei der Epoxidierung von Fettsäurealkylestern 未知
公开(公告)号：DE102014209413A1
公开(公告)日：2015-11-19
申请号：DE102014209413
申请日：2014-05-19
申请人： EVONIK DEGUSSA GMBH
发明人： WIEDERHOLD HOLGER , GRASS MICHAEL , WOLDT BENJAMIN , BOECK FLORIAN SEBASTIAN , PRISKE MARKUS , BOAM ANDREW , KREIS PETER
IPC分类号： C07D301/32 , B01D71/70 , C07D301/12
摘要： Die vorliegende Erfindung betrifft ein Verfahren zur Abtrennung homogener Katalysatorsystemen aus organischen Reaktionsmischungen. Ihr liegt die Aufgabe zu Grunde ein Verfahren anzugeben welches in Reaktionsgemischen zur Epoxidierung von Fettsäurealkylester eingesetzt wird. Gelöst wird diese Aufgabe durch Einsatz einer Membran, deren trennaktive Schicht vernetzte Siliconacrylate und/oder Polydimetyl-siloxan (PDMS) und/oder Polyimid umfasst.

9. 发明专利

SG11201804345RA METHOD FOR PRODUCING PROPYLENE GLYCOL FROM PROPENE AND HYDROGEN PEROXIDE 未知
公开(公告)号：SG11201804345RA
公开(公告)日：2018-06-28
申请号：SG11201804345R
申请日：2016-11-01
申请人： EVONIK DEGUSSA GMBH
发明人： WIEDERHOLD HOLGER , BOLZ DAVID , JAEGER BERND , KÖHLE HANS-JÜRGEN , IMM SEBASTIAN , THIELE GEORG FRIEDRICH
IPC分类号： C07C29/48 , C07C31/20
摘要： Method for producing propylene glycol from propene and hydrogen peroxide : The process for preparing 1,2-propanediol from propene and hydrogen peroxide comprises the steps of a) reacting propene with hydrogen peroxide in the presence of a catalyst mixture comprising a 5 phase transfer catalyst and a heteropolytungstate, wherein the reaction is carried out in a liquid mixture comprising an aqueous phase having a pH of at most 6 and an organic phase, b) separating the biphasic mixture from step a) into an aqueous phase and an organic phase comprising propene oxide, 10 c) recycling the propene oxide present in the separated organic phase into the reaction of step a) and d) separating 1,2-propanediol from the aqueous phase separated in step b). Fig. 1

10. 发明专利

HUE035587T2 Eljárás 1,2-epoxid elõállítására és eszköz az eljárás végrehajtására 未知
公开(公告)号：HUE035587T2
公开(公告)日：2018-05-28
申请号：HUE15171187
申请日：2011-01-26
申请人： EVONIK DEGUSSA GMBH
发明人： MUPPA PRASAD , POSTMA RON , VAN DEN BERG BART B , STOCK JUERGEN , WIEDERHOLD HOLGER , RAUSCH HANS-MARTIN , SCHALLENBERG JOERG , BERNHARDT STEFAN
IPC分类号： B01D17/02 , B01F5/06 , B01J4/00 , B01J19/18 , B01J19/24

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