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    • 2. 发明申请
    • METHOD FOR PRODUCING MONO-ALKALI METAL ZINC ALKOXIDE CUBANES
    • 用于生产MONO-碱金属 - 锌醇盐立方烷
    • WO2009141416A3
    • 2010-01-21
    • PCT/EP2009056207
    • 2009-05-22
    • GRILLO ZINKOXID GMBHJANA SURAJITDRIESS MATTHIASAKSU YILMAZ
    • JANA SURAJITDRIESS MATTHIASAKSU YILMAZ
    • C07F3/06
    • C07F3/06
    • The invention relates to a method for producing alkali metal zinc alkoxide compounds, characterised in that: a) an alkali metal alkoxide is dissolved in a solvent; b) an organometallic zinc compound is added to this compound; c) this mixture is heated for at least 5 min, in particular at least 15 min, to a temperature between 20 °C and the boiling point of the solvent, d) the mixture is cooled, e) a polar-protic solvent such as an alcohol or water is added, f) this mixture is heated for at least 5 min, in particular at least 15 min, to a temperature between 20 °C and the boiling point of the solvent, g) the mixture is cooled and the resultant alkali metal zinc alkoxide compound is isolated.
    • 一种制备碱金属 - 锌醇盐化合物的,其特征在于:a)处理溶解在溶剂中的碱金属醇盐,b)一种有机金属锌化合物加入到该溶液中,c)中分钟,该混合物至少5,尤其是至少15分钟,以一 20℃和溶剂的沸点之间的温度被加热时,D)将混合物冷却,e)是极性质子溶剂如醇或加入水,F)分钟该混合物至少5,尤其是至少15分钟,以一 20℃和溶剂的沸点之间的温度被加热,克),将混合物冷却,将所得碱金属锌醇盐化合物中分离。