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1. 发明授权

US06203639B1 Vehicle assembly line-side heat activation of a “ready-to-install” window fixing adhesive for attachment of a vehicle window to a vehicle 失效
公开(公告)号：US06203639B1
公开(公告)日：2001-03-20
申请号：US09244367
申请日：1999-02-04
申请人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
发明人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
IPC分类号： B32B3112
CPC分类号： F16B11/006 , B29C65/1412 , B29C65/1416 , B29C65/1422 , B29C65/1425 , B29C65/1432 , B29C65/1445 , B29C65/1464 , B29C65/1467 , B29C65/1496 , B29C65/4835 , B29C65/484 , B29C66/112 , B29C66/131 , B29C66/54 , B29C66/91411 , B29C66/91423 , B29C66/91443 , B29C66/91445 , B29C66/9161 , B29C66/919 , B29C66/91921 , B29C66/91941 , B29C66/91951 , B29C66/949 , B29C2035/0822 , B29L2031/3052 , B60J10/45 , B60J10/70 , C09J5/06
摘要： A method of preparing a vehicle panel assembly for attaching the panel to a vehicle is disclosed which provides a “ready-to-install” panel assembly. The panel assembly includes first and second spaced sides, with the bead of heat activated adhesive provided on the second side of the panel. The panel and bead are heated preferably by applying shortwave and longwave infrared radiation, with the shortwave infrared radiation being applied to an adhesive free side of the panel to heat the panel and, thereby, indirectly heat the bead of the heat activated adhesive. The longwave infrared radiation is applied to the adhesive side of the panel to directly heat the bead and thereby activate the adhesive. The ready-to-install adhesive may be applied on or adjacent to a gasket, such as a polyvinyl chloride (PVC) molding, a urethane molding, or the like. Optionally, either during or after heating, the substrate is cooled in order to ease handling of the panel assembly after the bead of adhesive is activate and ready for installation.

2. 发明授权

US06054001A Vehicle assembly line-side heat activation of a "ready-to-install" window fixing adhesive for attachment of a vehicle window to a vehicle 失效
公开(公告)号：US06054001A
公开(公告)日：2000-04-25
申请号：US24226
申请日：1998-02-17
申请人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
发明人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
IPC分类号： B29C35/08 , B29C65/00 , B29C65/14 , B29C65/48 , B60J10/00 , B60J10/02 , B32B31/26
CPC分类号： B60J10/70 , B60J10/45 , B29C2035/0822 , B29C65/14 , B29C65/1416 , B29C65/1422 , B29C65/1432 , B29C65/1445 , B29C65/1464 , B29C65/1467 , B29C65/1496 , B29C65/4835 , B29C65/484 , B29C66/80 , B29C66/91411 , B29C66/91423 , B29C66/91431 , B29C66/91645 , B29C66/919 , B29C66/91921 , B29C66/949 , Y10T156/17
摘要： A method of and apparatus for activating a ready-to-install heat activated adhesive for attaching a vehicle panel to a vehicle is disclosed which provides a "ready-to-install" panel assembly. The panel assembly includes first and second spaced apart surfaces, with the bead of heat activated adhesive provided on the second surface of the panel. The panel and bead are heated preferably by applying shortwave and longwave infrared radiation, with the shortwave infrared radiation being applied to an adhesive free side of the panel to heat the panel and, thereby, indirectly heat the bead of the heat activated adhesive. For example, where the window panel is such as a laminated windshield or side window or backlite comprising two glass sheets laminated with a polymer inner layer, such as plasticized polyvinyl butyral, or silicone or the like, it is preferable that the heat activation temperature of the adhesive be less than or equal to about 125.degree. C., more preferably less than or equal to about 115.degree. C., and most preferably less than or equal to about 105.degree. C. Also, when a ready-to-install adhesive is applied on or adjacent to a gasket such as a polyvinyl chloride (PVC) molding, a urethane molding, or the like, it is preferable that the heat activation temperature of the adhesive be about less than or equal to about 125.degree. C., more preferably less than or equal to about 115.degree. C., and most preferably less than or equal to about 105.degree. C. The longwave infrared radiation is applied to the adhesive side of the panel to directly heat the bead and thereby activate the adhesive. The apparatus includes a first heating component and a second heating component, with the first heating component including a source of shortwave infrared radiation, such as one or more lamps, which is adapted to heat the adhesive free side of the panel for indirectly heating the bead of adhesive. The second heating component includes a source of longwave radiation, for example a quartz emitter, which is applied the second side of the panel to directly heat the bead of adhesive.

3. 发明授权

US06521083B1 Vehicle assembly line-side heat activation of a “ready-to-install” window fixing adhesive for attachment of a vehicle window to a vehicle 有权
公开(公告)号：US06521083B1
公开(公告)日：2003-02-18
申请号：US09422053
申请日：1999-10-20
申请人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
发明人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
IPC分类号： B32B3126
CPC分类号： B60J10/70 , B29C65/14 , B29C65/1416 , B29C65/1422 , B29C65/1432 , B29C65/1445 , B29C65/1464 , B29C65/1467 , B29C65/1496 , B29C65/4835 , B29C65/484 , B29C66/80 , B29C66/91411 , B29C66/91423 , B29C66/91431 , B29C66/91645 , B29C66/919 , B29C66/91921 , B29C66/949 , B29C2035/0822 , B60J10/45 , Y10T156/17
摘要： A method of and apparatus for activating a ready-to-install heat activated adhesive for attaching a vehicle panel to a vehicle is disclosed which provides a “ready-to-install” panel assembly. The panel assembly includes first and second spaced apart surfaces, with the bead of heat activated adhesive provided on the second surface of the panel. The panel and bead are heated preferably by applying shortwave and longwave infrared radiation, with the shortwave infrared radiation being applied to an adhesive free side of the panel to heat the panel and, thereby, indirectly heat the bead of the heat activated adhesive. For example, where the window panel is such as a laminated windshield or side window or backlite comprising two glass sheets laminated with a polymer inner layer, such as plasticized polyvinyl butyral, or silicone or the like, it is preferable that the heat activation temperature of the adhesive be less than or equal to about 125° C., more preferably less than or equal to about 115° C., and most preferably less than or equal to about 105° C. Also, when a ready-to-install adhesive is applied on or adjacent to a gasket such as a polyvinyl chloride (PVC) molding, a urethane molding, or the like, it is preferable that the heat activation temperature of the adhesive be about less than or equal to about 125° C., more preferably less than or equal to about 115° C., and most preferably less than or equal to about 105° C. The longwave infrared radiation is applied to the adhesive side of the panel to directly heat the bead and thereby activate the adhesive. The apparatus includes a first heating component and a second heating component, with the first heating component including a source of shortwave infrared radiation, such as one or more lamps, which is adapted to heat the adhesive free side of the panel for indirectly heating the bead of adhesive. The second heating component includes a source of longwave radiation, for example a quartz emitter, which is applied the second side of the panel to directly heat the bead of adhesive.

4. 发明授权

US06599386B2 Vehicle assembly line-side heat activation of a “Ready-To-Install” window fixing adhesive for attachment of a vehicle window to a vehicle 失效
标题翻译：用于将车窗安装到车辆上的“准备安装”窗户固定粘合剂的车辆装配线侧热活化
公开(公告)号：US06599386B2
公开(公告)日：2003-07-29
申请号：US09805540
申请日：2001-03-13
申请人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
发明人： Douglas R. Swanson , David E. Nestell , Niall R. Lynam
IPC分类号： B60J100
CPC分类号： F16B11/006 , B29C65/1412 , B29C65/1416 , B29C65/1422 , B29C65/1425 , B29C65/1432 , B29C65/1445 , B29C65/1464 , B29C65/1467 , B29C65/1496 , B29C65/4835 , B29C65/484 , B29C66/112 , B29C66/131 , B29C66/54 , B29C66/91411 , B29C66/91423 , B29C66/91443 , B29C66/91445 , B29C66/9161 , B29C66/919 , B29C66/91921 , B29C66/91941 , B29C66/91951 , B29C66/949 , B29C2035/0822 , B29L2031/3052 , B60J10/45 , B60J10/70 , C09J5/06
摘要： A method of preparing a vehicle panel assembly for attaching the panel to a vehicle is disclosed which provides a “ready-to-install” panel assembly. The panel assembly includes first and second spaced sides, with the bead of heat activated adhesive provided on the second side of the panel. The panel and bead are heated preferably by applying shortwave and longwave infrared radiation, with the shortwave infrared radiation being applied to an adhesive free side of the panel to heat the panel and, thereby, indirectly heat the bead of the heat activated adhesive. The longwave infrared radiation is applied to the adhesive side of the panel to directly heat the bead and thereby activate the adhesive. The ready-to-install adhesive may be applied on or adjacent to a gasket, such as a polyvinyl chloride (PVC) molding, a urethane molding, or the like. Optionally, either during or after heating, the substrate is cooled in order to ease handling of the panel assembly after the bead of adhesive is activate and ready for installation.
摘要翻译：公开了一种制备用于将面板附接到车辆的车辆面板组件的方法，其提供了“准备安装”面板组件。面板组件包括第一和第二隔开的侧面，其中设置在面板的第二侧上的热活化粘合剂的珠。优选地通过施加短波和长波红外辐射来加热面板和珠，其中短波红外辐射被施加到面板的无粘合剂侧以加热面板，从而间接加热热活化粘合剂的珠。将长波红外辐射施加到面板的粘合剂侧，以直接加热珠，从而激活粘合剂。准备安装的粘合剂可以施加在垫圈上或附近，例如聚氯乙烯（PVC）模制件，聚氨酯模塑件等。任选地，在加热期间或之后，基板被冷却以便在粘合剂珠被激活并准备安装之后便于面板组件的处理。

5. 发明授权

US07985424B2 Dendritic polymers with enhanced amplification and interior functionality 有权
标题翻译：具有增强的扩增和内部功能的树枝状聚合物
公开(公告)号：US07985424B2
公开(公告)日：2011-07-26
申请号：US11630044
申请日：2005-12-21
申请人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam , Joseph R. Heinzelmann , Sonke Svenson , Lori A. Reyna , Michael A. Zhuravel , Abhay Singh Chauhan , Cordell R. DeMattei
发明人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam , Joseph R. Heinzelmann , Sonke Svenson , Lori A. Reyna , Michael A. Zhuravel , Abhay Singh Chauhan , Cordell R. DeMattei
IPC分类号： A61K9/14
CPC分类号： C08G63/46 , A01N25/10 , A61K8/85 , A61K9/0019 , A61K9/5146 , A61Q15/00 , A61Q17/005 , C08G83/003 , H01M4/86 , H01M8/10 , Y02P70/56
摘要： Dendritic polymers with enhanced amplification and interior functionality are disclosed. These dendritic polymers are made by use of fast, reactive ring-opening chemistry (or other fast reactions) combined with the use of branch cell reagents in a controlled way to rapidly and precisely build dendritic structures, generation by generation, with cleaner chemistry, often single products, lower excesses of reagents, lower levels of dilution, higher capacity method, more easily scaled to commercial dimensions, new ranges of materials, and lower cost. The dendritic compositions prepared have novel internal functionality, greater stability (e.g., thermal stability and less or no reverse Michael's reaction), and reach encapsulation surface densities at lower generations. Unexpectedly, these reactions of polyfunctional branch cell reagents with polyfunctional cores do not create cross-linked materials. Such dendritic polymers are useful as demulsifiers for oil/water emulsions, wet strength agents in the manufacture of paper, proton scavengers, polymers, nanoscale monomers, calibration standards for electron microscopy, making size selective membranes, and agents for modifying viscosity in aqueous formulations such as paint. When these dendritic polymers have a carried material associated with their surface and/or interior, then these dendritic polymers have additional properties for carrying materials due to the unique characteristics of the dendritic polymer, such as for drug delivery, transfection, and diagnostics.
摘要翻译：公开了具有增强的扩增和内部功能的树枝状聚合物。这些树枝状聚合物通过使用快速，反应性开环化学（或其他快速反应）结合使用分支细胞试剂以受控方式快速和精确地构建树突状结构，一代代，具有更清洁的化学，通常单一产品，较低的试剂过量，较低的稀释水平，更高的容量方法，更容易缩放到商业尺寸，新的材料范围以及更低的成本。制备的树枝状组合物具有新颖的内部功能，更高的稳定性（例如，热稳定性和较少的或没有反向的迈克尔反应），并且在较低的代次下达到包封表面密度。出乎意料的是，多官能分支细胞试剂与多官能核心的这些反应不产生交联材料。这种树枝状聚合物可用作油/水乳液的破乳剂，纸张制造中的湿强剂，质子清除剂，聚合物，纳米尺寸单体，用于电子显微镜的校准标准品，制备尺寸选择性膜，以及用于在水性制剂中改性粘度的试剂作为油漆。当这些树枝状聚合物具有与其表面和/或内部相关的载体材料时，由于树枝状聚合物的独特特征，例如用于药物递送，转染和诊断，这些树枝状聚合物具有携带材料的附加性质。

6. 发明申请

US20100086482A1 DIVERGENT SYNTHESIS OF LOOPED POLY(ESTER)-AND POLY(ETHER)-SUBSTITUTED DENDRONS AND DENDRIMERS 审中-公开
标题翻译：循环聚合（ESTER）和聚（醚） - 分散的DENDRONS和DENDRIMERS的多重合成
公开(公告)号：US20100086482A1
公开(公告)日：2010-04-08
申请号：US12448513
申请日：2007-12-28
申请人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam
发明人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam
IPC分类号： A61K49/00 , C07D487/00 , C07D491/00 , A61K31/395 , C07D245/00 , A61K31/495 , A61K31/16 , G01N33/566
CPC分类号： C08G83/003 , Y10T436/143333
摘要： The present invention describes a process for preparing new looped dendrimer and dendron compounds by controlling the molar amount of branch cell reagent monomer that is combined with various cores bearing core-XR functionalities (e.g., primary, or secondary amines, thiol, or epoxy functionalities). These looped, macrocyclic structures are more robust to various conditions, with greater resistance to acid/base hydrolysis. Alternatively, the looped, macrocyclic structure may offer new orientations that would qualify it as a better chelation ligand for metals, and other similar uses.
摘要翻译：本发明描述了通过控制与具有核-XR官能团的各种核心（例如伯，仲胺，硫醇或环氧官能团）组合的分支细胞试剂单体的摩尔量来制备新的环状树枝状聚合物和树枝状化合物的方法，。这些环状的大环结构对各种条件更加坚固，具有较强的抗酸/碱水解的能力。或者，环状的大环结构可以提供新的取向，其将其作为金属的更好的螯合配体和其它类似的用途。

7. 发明授权

US5705573A Process for preparation of water borne curing agents 失效
标题翻译：水性固化剂的制备方法
公开(公告)号：US5705573A
公开(公告)日：1998-01-06
申请号：US708677
申请日：1996-09-05
申请人： Douglas R. Swanson , Donald A. Tomalia
发明人： Douglas R. Swanson , Donald A. Tomalia
IPC分类号： C08F8/00
CPC分类号： C08F8/32
摘要： A novel process for preparing poly(2-isopropenyl-2-oxazoline or oxazine) and its methyl methacrylate copolymer, which are useful as water borne curing agents, particularly in the non-stick coating industry. The process converts commercially available poly(methyl methacrylate) into poly(2-isopropenyl-2-oxazoline or oxazine) polymers or copolymers with methyl methacrylate, while circumventing the use of the highly toxic monomer, 2-isopropenyl-2-oxazoline or oxazine. The process involves converting a poly(methacrylic ester) to the corresponding poly(.beta.-hydroxy-N-ethyl or propyl methacrylamide) and activating the ring-forming .beta.-hydroxy-N-ethyl or propyl methacrylamide moiety to form an oxazoline or oxazine ring.
摘要翻译：制备聚（2-异丙烯基-2-恶唑啉或恶嗪）及其甲基丙烯酸甲酯共聚物的新方法，其可用作水性固化剂，特别是在不粘涂料工业中。该方法将市售的聚（甲基丙烯酸甲酯）转化成聚（2-异丙烯基-2-恶唑啉或恶嗪）聚合物或与甲基丙烯酸甲酯共聚物，同时避免使用高毒性单体2-异丙烯基-2-恶唑啉或恶嗪。该方法包括将聚（甲基丙烯酸酯）转化为相应的聚（β-羟基-N-乙基或丙基甲基丙烯酰胺）并活化成环β-羟基-N-乙基或丙基甲基丙烯酰胺部分以形成恶唑啉或恶嗪环。

8. 发明授权

US07981444B2 Dendritic polymers with enhanced amplification and interior functionality 有权
标题翻译：具有增强的扩增和内部功能的树枝状聚合物
公开(公告)号：US07981444B2
公开(公告)日：2011-07-19
申请号：US10594776
申请日：2005-04-20
申请人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam
发明人： Donald A. Tomalia , Douglas R. Swanson , Baohua Huang , Veera Reddy Pulgam
IPC分类号： A61K9/14
CPC分类号： C08G83/003 , C08G59/1477 , C08G59/32 , C08G59/3227 , C08G59/5026
摘要： Poly(ester-acrylate) and poly(ester/epoxide) dendrimers. These materials can be synthesized by utilizing the so-called “sterically induced stoichiometric” principles. The preparation of the dendrimers is carried out by reacting precursor amino/polyamino-functional core materials with various branch cell reagents. The branch cell reagents are dimensionally large, relative to the amino/polyamino-initiator core and when reacted, produce generation=1 dendrimers directly in one step. There is also a method by which the dendrimers can be stabilized and that method is the reaction of the dendrimers with surface reactive molecules to pacify the reactive groups on the dendrimers.
摘要翻译：聚（酯 - 丙烯酸酯）和聚（酯/环氧化物）树枝状大分子。这些材料可以通过利用所谓的“空间诱导化学计量”原理来合成。树枝状大分子的制备通过使前体氨基/聚氨基官能的核心材料与各种分支细胞试剂反应来进行。分支细胞试剂相对于氨基/聚氨基 - 引发剂核心在尺寸上是大的，并且当反应时，在一个步骤中直接产生生成= 1个树枝状大分子。还有一种树枝状聚合物可以稳定的方法，该方法是树枝状聚合物与表面反应性分子的反应，以平衡树枝状聚合物上的反应性基团。

9. 发明申请

US20090012033A1 Delivery of Biologically Active Materials Using Core-Shell Tecto(Dendritic Polymers) 审中-公开
标题翻译：使用核 - 壳Tecto（树枝状聚合物）递送生物活性材料
公开(公告)号：US20090012033A1
公开(公告)日：2009-01-08
申请号：US12224644
申请日：2007-03-03
申请人： Cordell R. DeMattei , Baohua Huang , Lori A. Reyna , Sonke Svenson , Douglas R. Swanson , Donald A. Tomalia , Michael A. Zhuravel , Veera Reddy Pulgam
发明人： Cordell R. DeMattei , Baohua Huang , Lori A. Reyna , Sonke Svenson , Douglas R. Swanson , Donald A. Tomalia , Michael A. Zhuravel , Veera Reddy Pulgam
IPC分类号： A61K48/00 , C08G73/02 , C08G63/08 , C12Q1/68 , A61P43/00 , C12N15/63 , C08G63/91 , A61K31/7052
CPC分类号： A61K48/00 , A61K9/5146 , A61K47/59 , A61K47/595 , A61K47/60 , C08G83/003 , Y02A50/463
摘要： The present invention concerns core-shell tecto (dendritic polymers) that are associated with biologically active materials (such as nucleic acids for use for RNAi and in transfection). Also included are formulations for their use. The constructs are useful for the delivery of drugs to an animal or plant and may be in vivo, in vitro or ex vivo.
摘要翻译：本发明涉及与生物活性物质（例如用于RNAi和转染的核酸）相关的核 - 壳结构（树枝状聚合物）。还包括其使用的配方。所述构建体可用于将药物递送至动物或植物，并且可以在体内或体外进行。

10. 发明授权

US07977452B2 Janus dendrimers and dendrons 失效
标题翻译：珍珠菌树枝状大分子和树突
公开(公告)号：US07977452B2
公开(公告)日：2011-07-12
申请号：US11885244
申请日：2006-03-27
申请人： Donald A. Tomalia , Veera Reddy Pulgam , Douglas R. Swanson , Boahua Huang
发明人： Donald A. Tomalia , Veera Reddy Pulgam , Douglas R. Swanson , Boahua Huang
IPC分类号： C08G75/00
CPC分类号： C08G83/003 , C08G81/00
摘要： This invention provides a cost effective process and new Janus dendrimers where at least two dendrons are attached at the core (with or without a connector group) and where at least two of the dendrons have different functionality. Preferred are those Janus dendrimers where at least one dendron is a PEHAM dendron. Thus these Janus dendrimers are heterobifunctional in character and use unique ligation chemistry with single site functional dendrons, di-dendrons and multi-dendrons. Also included are Janus dendrons which may be used as intermediates to make the Janus dendrimers or to further react with another reactive moiety. These Janus dendrimers can provide several new dendrimer moieties, namely: combinatorial libraries of bifunctional structures; combined target director and signaling dendrimers; specific targeting entities for diagnostic and therapeutic applications, such as for example targeted MRI agents, targeted radionuclide delivery for diseases such as cancer, and targeted photosensitive or radiowave sensitive agents.
摘要翻译：本发明提供了一种成本有效的方法和新的Janus树枝状大分子，其中至少两个树突状物连接在核心处（具有或不具有连接基团），并且其中至少两个枝状突起具有不同的功能。那些Janus树枝状大分子是首选，其中至少有一个树突是PEHAM树突。因此，这些Janus树枝状大分子在性质上是异双功能的，并且使用独特的连接化学物质，其具有单位点功能性树突，二树枝状突起和多枝状突起。还包括Janus dendron，其可以用作中间体以制备Janus树枝状大分子或进一步与另一反应性部分反应。这些Janus树枝状大分子可以提供几个新的树枝状大分子部分，即：双功能结构的组合文库; 组合目标主任和信号树枝状大分子; 用于诊断和治疗应用的特异性靶向实体，例如靶向MRI剂，用于诸如癌症的疾病的靶向放射性核素递送，以及靶向感光或无线电波敏感剂。

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