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1. 发明授权

US06337384B1 Method of making thermally removable epoxies 有权
标题翻译：制造热可去除环氧树脂的方法
公开(公告)号：US06337384B1
公开(公告)日：2002-01-08
申请号：US09484839
申请日：2000-01-18
申请人： Douglas A. Loy , David R. Wheeler , Edward M. Russick , James R. McElhanon , Randall S. Saunders
发明人： Douglas A. Loy , David R. Wheeler , Edward M. Russick , James R. McElhanon , Randall S. Saunders
IPC分类号： C08G5926
CPC分类号： C08L63/00 , C08G59/26 , C08G59/302 , C08G59/306 , C08G59/50 , C08G65/22 , H05K3/285 , H05K3/288
摘要： A method of making a thermally-removable epoxy by mixing a bis(maleimide) compound to a monomeric furan compound containing an oxirane group to form a di-epoxy mixture and then adding a curing agent at temperatures from approximately room temperature to less than approximately 90° C. to form a thermally-removable epoxy. The thermally-removable epoxy can be easily removed within approximately an hour by heating to temperatures greater than approximately 90° C. in a polar solvent. The epoxy material can be used in protecting electronic components that may require subsequent removal of the solid material for component repair, modification or quality control.
摘要翻译：通过将双（马来酰亚胺）化合物与含有环氧乙烷基团的单体呋喃化合物混合以形成二环氧混合物，然后在约室温至小于约90℃的温度下加入固化剂来制备热可除去环氧树脂的方法 ℃以形成可热去除的环氧树脂。通过在极性溶剂中加热至大约90℃的温度，可以在大约1小时内容易地除去热可去除的环氧树脂。环氧树脂材料可用于保护可能需要随后除去固体材料以进行部件修理，改性或质量控制的电子部件。

2. 发明授权

US6110982A Epoxy foams using multiple resins and curing agents 失效
标题翻译：环氧泡沫使用多种树脂和固化剂
公开(公告)号：US6110982A
公开(公告)日：2000-08-29
申请号：US229512
申请日：1999-01-13
申请人： Edward M. Russick , Peter B. Rand
发明人： Edward M. Russick , Peter B. Rand
IPC分类号： C08J9/04 , H05K3/28 , C08J9/00
CPC分类号： C08J9/04 , C08J2363/00 , H05K3/284 , H05K3/285
摘要： An epoxy foam comprising a plurality of resins, a plurality of curing agents, at least one blowing agent, at least one surfactant and optionally at least one filler and the process for making. Preferred is an epoxy foam comprising two resins of different reactivities, two curing agents, a blowing agent, a surfactant, and a filler. According to the present invention, an epoxy foam is prepared with tailorable reactivity, exotherm, and pore size by a process of admixing a plurality of resins with a plurality of curing agents, a surfactant and blowing agent, whereby a foamable mixture is formed and heating said foamable mixture at a temperature greater than the boiling temperature of the blowing agent whereby said mixture is foamed and cured.
摘要翻译：包含多种树脂，多种固化剂，至少一种发泡剂，至少一种表面活性剂和任选的至少一种填料的环氧泡沫及其制备方法。优选的是包含两种不同反应性的树脂的环氧泡沫，两种固化剂，发泡剂，表面活性剂和填料。根据本发明，通过将多种树脂与多种固化剂，表面活性剂和发泡剂混合的方法制备具有可调节反应性，放热和孔径的环氧泡沫体，由此形成可发泡混合物并加热所述可发泡混合物的温度大于发泡剂的沸点温度，由此所述混合物发泡并固化。

3. 发明授权

US4673695A Low density microcellular foams 失效
标题翻译：低密度微孔泡沫
公开(公告)号：US4673695A
公开(公告)日：1987-06-16
申请号：US785436
申请日：1985-10-08
申请人： James H. Aubert , Roger L. Clough , John G. Curro , Carlos A. Quintana , Edward M. Russick , Montgomery T. Shaw
发明人： James H. Aubert , Roger L. Clough , John G. Curro , Carlos A. Quintana , Edward M. Russick , Montgomery T. Shaw
IPC分类号： B01D39/16 , B01D67/00 , B01D71/28 , C08J9/26 , C08J9/28
CPC分类号： C08J9/28 , B01D39/1676 , B01D67/003 , B01D71/28 , C08J9/26 , C08J2201/0482 , C08J2201/0484 , C08J2201/052 , C08J2325/06
摘要： Low density, microporous polymer foams are provided by a process which comprises forming a solution of polymer and a suitable solvent followed by rapid cooling of the solution to form a phase-separated system and freeze the phase-separated system. The phase-separated system comprises a polymer phase and a solvent phase, each of which is substantially continuous within the other. The morphology of the polymer phase prior to and subsequent to freezing determine the morphology of the resultant foam.Both isotropic and anisotropic foams can be produced. If isotropic foams are produced, the polymer and solvent are tailored such that the solution spontaneously phase-separates prior to the point at which any component freezes. The morphology of the resultant polymer phase determines the morphology of the resultant foam and the morphology of the polymer phase is retained by cooling the system at a rate sufficient to freeze one or both components of the system before a change in morphology can occur. Anisotropic foams are produced by forming a solution of polymer and solvent that will not phase separate prior to freezing of one or both components of the solution. In such a process, the solvent typically freezes before phase separation occurs. The morphology of the resultant frozen two-phase system determines the morphology of the resultant foam.The process involves subjecting the solution to essentially one-dimensional cooling. Means for subjecting such a solvent to one-dimensional cooling are also provided.Foams having a density of less than 0.1 g/cc and a uniform cell size of less than 10 .mu.m and a volume such that the foams have a length greater than 1 cm are provided.
摘要翻译：通过包括形成聚合物溶液和合适溶剂的方法提供低密度，微孔聚合物泡沫，然后快速冷却溶液以形成相分离系统并冷冻相分离系统。相分离系统包括聚合物相和溶剂相，其各自在另一个内基本连续。在冷冻之前和之后的聚合物相的形态决定所得泡沫的形态。可以生产各向同性和各向异性泡沫。如果产生各向同性泡沫，则定制聚合物和溶剂使得溶液在任何组分冻结的点之前自发相分离。所得聚合物相的形态决定了所得泡沫体的形态，并且通过以足以在形态变化发生之前冻结体系的一个或两个组分的速率冷却系统来保留聚合物相的形态。通过形成聚合物和溶剂的溶液来产生各向异性泡沫，该溶液在溶液的一个或两个组分冷冻之前不会相分离。在这种过程中，溶剂通常在相分离发生之前冻结。所得冷冻两相体系的形态决定所得泡沫的形态。该方法包括使溶液基本上进行一维冷却。还提供了使这种溶剂进行一维冷却的方法。具有小于0.1g / cc的密度和小于10μm的均匀泡孔尺寸的泡沫和具有长度大于1cm的泡沫的体积。

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